Basic Engineering Package

PROJECT NO: - 876

CLIENT: M/s Gulf Stabilizers Industries Kingdom Of Saudi Arabia

Basic Engineering Package

SUPPLIED BY:

LIBRA TECHCON LTD. Head Office: 805/806, Hallmark Business Plaza, Guru Nanak Hospital Road, Bandra (East), Mumbai 400 051, India. . Phones: (91-22)-40940555 Fax: (91-22)-40940590 Email: [email protected] Website: http://www.libratechcon.com

INDEX The following documents attached here with are being released for Detailed Engineering 1) 2) 3) 4) 5) 6) 7)

Mass and Energy Balance Equipment List Process Flow Diagram Piping and Instrumentation diagram Pipe line sizing list Instrument Index Process Data sheet a. Heat Exchangers b. Pumps. c. Vacuum Pumps d. Vessels e. Distillation Column 8) Capacity Check a. Dryer DA4401 b. Centrifuge CF4301 c. Heat Exchanger ET4301 d. Heat Exchanger EC4401

# of additions of catalyst ncatalyst/nMPE

SHEET: PLANT: CLIENT :

Anox20 Mass Balance

LIBRA TECHCON LTD. MUMBAI

Anti-oxidants plant Gulf Stabilizers Industries

3.00 0.02 Charging PP Base charge (TOTAL)

MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH TOTAL

wt frac

13,662.19 37.81 13,700.00

1.00 0.00 1.00

kmol

46.72 0.16 46.88

PE charge mol frac

1.00 0.00 1.00

kg

wt frac

1,450.00 1,450.00

Catalyst kmol

1.00 1.00

10.65 10.65

mol frac

1.00 1.00

kg

23.05 23.05

wt frac

Total kmol

1.00 1.00

0.61 0.61

mol frac

1.00 1.00

kg

13,662.19 37.81 1,450.00 23.05 15,173.05

wt frac

kmol

0.90 0.00 0.10 0.00 1.00

46.72 0.16 10.65 0.61 58.14

mol frac

0.80 0.00 0.18 0.01 1.00

Reaction Crude (without catalyst) MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05

wt frac crude

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH TOTAL

0.00 0.11 0.06 0.01 0.81 1.00

kmol/1kg crude

0.00 0.00 0.00 0.00 0.00 0.00

kmol MPE/1kg crude

0.00 0.00 0.00 0.00

mol frac of MPE

kmol MPE

kg MPE

kg

66.09 1,466.46 0.09 0.02 0.89 1.00

0.96 0.17 9.52 10.65

130.80 23.40 1,295.80 1,450.00

881.25 192.77 11,208.45 13,769.59

wt frac

0.00 0.11 0.06 0.01 0.81 1.00

kmol

0.24 5.01 0.96 0.17 9.52 15.90

Crude (with catalyst) mol frac

0.01 0.32 0.06 0.01 0.60 1.00

kg

66.09 1,466.46 881.25 192.77 11,208.45 23.05 13,838.09

wt frac

0.00 0.11 0.06 0.01 0.81 0.00 1.00

kmol

0.24 5.01 0.96 0.17 9.52 0.61 16.51

MeOH mol frac

0.01 0.30 0.06 0.01 0.58 0.04 1.00

kg

92.35 22.03 1,219.86

1,334.24

wt frac

0.07 0.02 0.91 1.00

kmol

2.88 0.69 38.07

41.64

mol frac

0.07 0.02 0.91 1.00

1

Crystallization no. of crystallization batches Crude per crystallization batch

Crude MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH TOTAL

66.09 1,466.46 881.25 192.77 11,208.45 23.05 13,838.09

wt frac

0.00 0.11 0.06 0.01 0.81 0.00 1.00

kmol

mol frac

0.24 5.01

0.01 0.30

0.96 0.17 9.52 0.61 16.51

0.06 0.01 0.58 0.04 1.00

Density (kg/m3) Volume (m3)

kg

22.03 488.82 293.75 64.26 3,736.15 7.68 4,612.70

3.00 solvent(wt)/crude(wt) MeOH+water(7%) per crystallization batch

wt frac

kmol

mol frac

0.00 0.11

0.08 1.67

0.01 0.30

0.06 0.01 0.81 0.00 1.00

0.32 0.06 3.17 0.20 5.50

0.06 0.01 0.58 0.04 1.00

1,170.00 3.94

kg

wt frac

kmol

6,434.71

0.93

200.82

484.33

0.07

26.88

14.41 6,933.46

0.00 1.00

0.24 227.94

1.50 nAcAc/nLiOMe Slurry per crystallization batch mol frac

0.88 0.12 0.00 1.00

kg

22.03 488.82 293.75 64.26 3,736.15 6,441.19 484.33 13.35 2.43 11,546.32

wt frac

0.00 0.04 0.03 0.01 0.32 0.56 0.04 0.00 0.00 1.00

1.20 Slurry TOTAL kmol

0.08 1.67 0.32 0.06 3.17 201.02 26.88 0.20 0.04 233.45

mol frac

0.00 0.01 0.00 0.00 0.01 0.86 0.12 0.00 0.00 1.00

kg

66.09 1,466.46 881.25 192.77 11,208.45 19,323.58 1,453.00 40.06 7.29 34,638.96

wt frac

0.00 0.04 0.03 0.01 0.32 0.56 0.04 0.00 0.00 1.00

kmol

0.24 5.01 0.96 0.17 9.52 603.06 80.65 0.61 0.12 700.35

mol frac

0.00 0.01 0.00 0.00 0.01 0.86 0.12 0.00 0.00 1.00

804.88 8.61 Centrifuge and drying

Spec Consumpt kgPPB/kgA20 kgPPB tot/kgA20 prod

1.06 1.23 kg MeOH/kg Product

0.60

Product MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH TOTAL

34.03

wt frac

Cake washing solvent TOTAL kmol

0.00

0.12

mol frac

kg

0.02

0.26

0.03

10,856.79

0.98

9.22

0.96 6,677.50

136.28

1.00

9.59

1.00

kmol

-

0.01

238.22

11,129.16

wt frac

6,813.77

208.40 7.56 215.96

0.98 8.25 9.23

Mother liquor mol frac

0.96 0.01 0.97

kg

66.09 1,432.43 643.03 192.77 351.66 26,001.08 1,589.27 40.06 7.29 30,323.70

wt frac

0.00 0.05 0.02 0.01 0.01 0.86 0.05 0.00 0.00 1.00

kmol

0.24 4.90 0.70 0.17 0.30 811.46 88.22 0.61 0.12 906.71

mol frac

0.00 0.01 0.00 0.00 0.00 0.89 0.10 0.00 0.00 1.00

Solvent Recovery Solvent distilled MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH TOTAL

27,146.66

554.01

27,700.67

wt frac

0.98 0.02 1.00

kmol

847.21 30.75 877.96

Tars mol frac

0.96 0.04 1.00

kg

66.09 1,432.43 643.03 192.77 351.66 151.85 151.85 40.06 7.29 3,037.05

wt frac

0.02 0.47 0.21 0.06 0.12 0.05 0.05 0.01 0.00 1.00

Bottom Product of Distillation kmol

0.24 4.90 0.70 0.17 0.30 4.74 8.43 0.61 0.12 20.20

mol frac

0.01 0.24 0.03 0.01 0.01 0.23 0.42 0.03 0.01 1.00

kg

wt frac

kmol

mol frac

36.81

0.04

1.15

0.02 assuming 5% of MeOH and 5% of Water in tars

883.41

0.96

49.04

0.98 assuming 5% of MeOH and 5% of Water in tars

920.22

1.00

50.19

1.00

2

Considering total MeOH water feed to distillation column Wt Fraction of MeOH in Feed to distillation Distillate Bottom Feed

D W F

28,620.89 kg 0.95

xd= xw = xf =

0.98 0.04 0.95

F=D+W D+W = 28,620.89 xf . F = D.xd + W.xw 0.98 D + 0.04 W = 27,183.46 Solving These to equations simulanteously D= W=

27,700.67 920.22 Tars washing Tars washing (per batch of Anox)

MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05 84.16

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH CycloHexane TOTAL

wt frac

kmol

Tars Washing (total) mol frac

kg

0.02 0.47 0.21 0.06 0.12 0.05 0.05 0.01 0.00

0.24 4.90 0.70 0.17 0.30 4.74 8.43 0.61 0.12

0.01 0.24 0.03 0.01 0.01 0.23 0.42 0.03 0.01

264.38 5,729.72 2,572.14 771.10 1,406.65 607.41 607.41 160.22 29.16

0.02 0.47 0.21 0.06 0.12 0.05 0.05 0.01 0.00

3,037.05

1.00

20.20

1.00

12,148.18

1.00

Tars washing - 1st wash MW

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05 84.16

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH CycloHexane TOTAL

264.38 5,729.72 2,572.14 771.10 1,406.65 2,400.00 160.22 129.16 10,400.00 23,833.36

wt frac

kmol

0.01 0.24 0.11 0.03 0.06 0.10 0.01 0.01 0.44 1.00

0.95 19.59 2.80 0.69 1.19 133.22 2.43 2.15 123.57 286.60

278.39 292.42 236.31 656.91 917.29 1,121.56 1,177.67 396.53 32.04 136.15 37.97 18.02 65.98 60.05 84.16

kg

pp-Acid PP-Base PP-Base deal Di-A20 TriS (1st vac) Deal Anox 20 (1st vac) MonoS MeOH MPE LiOme Water CH3COOLi CH3COOH CycloHexane TOTAL

264.38 5,729.72 2,572.14 771.10 1,406.65 1,196.00 10,400.00 22,339.97

wt frac

0.01 0.26 0.12 0.03 0.06 0.05 0.47 1.00

kmol

0.95 19.59 2.80 0.69 1.19 18.96 33.72 2.43 0.49 80.82

mol frac

0.01 0.24 0.03 0.01 0.01 0.23 0.42 0.03 0.01 1.00

kg

0.00 0.07 0.01 0.00 0.00 0.46 0.01 0.01 0.43 1.00

kg

wt frac

kmol

0.95 19.59 2.80 0.69 1.19 66.39 123.57 215.19

mol frac

0.89 0.06 0.05

133.22 2.43 2.15

0.97 0.02 0.02

2,689.39

1.00

137.80

1.00

0.00 0.09 0.01 0.00 0.01 0.31 0.57 1.00

10,400.00 10,400.00

wt frac

1.00 1.00

kmol

123.57 123.57

mol frac

kg

wt frac

kmol

18.96

0.36

607.41

0.50

33.72

0.64

2,400.00

133.22

1.00

100.00 10,400.00 12,900.00

1.67 123.57 258.46

1,214.82

1.00

52.67

Tars washing - 2nd wash mol frac

2,400.00 160.22 129.16

kg

kmol

0.50

kg

264.38 5,729.72 2,572.14 771.10 1,406.65 3,596.00 10,400.00 24,739.97

Cyclohexane stripping

kmol

wt frac

Charging

607.41

Phase separation (aqueous phase) mol frac

Tars washing MW

wt frac

66.09 1,432.43 643.03 192.77 351.66 151.85 151.85 40.06 7.29

Methanol Stripping

wt frac

kmol

0.01 0.23 0.10 0.03 0.06 0.15 0.42 1.00

0.95 19.59 2.80 0.69 1.19 199.61 123.57 348.41

mol frac

Phase separation (aqueous phase) mol frac

kg

wt frac

kmol

mol frac

0.00 0.06 0.01 0.00 0.00 0.57

2,400.00

0.89

12.02

0.09

0.35 1.00

2,400.00

0.89

12.02

0.09

Washed Tars mol frac

1.00 1.00

kg

264.38 5,729.72 2,572.14 771.10 1,406.65 1,196.00 11,939.97

wt frac

0.02 0.48 0.22 0.06 0.12 0.10 1.00

kmol

0.95 19.59 2.80 0.69 1.19 66.39 91.62

mol frac

0.01 0.21 0.03 0.01 0.01 0.72 1.00

3

LIBRA TECHCON LTD. MUMBAI

MW 136.15 292.4 1177.6 32.04 37.97

Penta-erithritol PP Base ANOX20 MeOH LiOMe Hot Oil

PP Base

SHEET: PLANT: CLIENT :

Anox20 Heat Balance

Melt Point 65 -

Boil Point 177.00 64.70 -

Anti-oxidants plant Gulf Stabilizers Industries

Specific Heat 0.51

0.64

Kg 13700.00

Kmol 46.88

Specific Heat of PP Base = Heat to be supplied by Hot Oil = Rate of PP base transfer = Total Time taken to transfer = Heat to be supplied by Hot Oil =

T 0C 90

Heating PP Base ET-4101

0.51 663765.00 9000.00 1.52 436050.00

kcal/kg 0C kcal kg/hr hr kcal/hr

0.64

kcal/kg 0C

230.00

0

68669.29 81.55

kg/hr m3/hr

PP Base

Temperature difference for Hot Oil= Flow of Hot oil = Flow of Hot oil =

C

Kmol 46.88

T 0C 185

specific heat as provided by GSI, higher value is considered for appropriate sizing

PP base heating Specific Heat of Hot oil =

Kg 13700.00

220 0C Density =

specific heat as mentioned by GSI, as per data sheet of Heat Exchanger ET4101, the specific mentioned is 0.495 kcal/kg C temperature range as mentioned by GSI, as per utility details mentioned, Inlet HO temperature is 240 C 842 kg/m3

1

Penta-erithritol LiOMe PP Base

Kg 1450.00 23.05 13700.00

Kmol 10.65 0.61 46.88

T 0C 35 35 185

Kmol 10.65 0.61 46.88

T 0C

Penta-erithritol LiOMe PP Base

Kg 1450.00 23.05 13700.00

Specific Heat of Reaction Mass = Heat to be supplied by Hot Oil =

150

Charging TR-4101 Heating with Recirculation

Heating and Reaction T(max)=190 0C TR4101 Heating with Recirculation 0.60 89928.90

Reactor Heating

89928.90 0.64 230.00 14162.03 1.00 14162.03 16.82

Kmol 16.51 41.64

T 0C

Crude MeOH

Kg 13838 1334.24

150

160

kcal/kg 0C kcal

Heat to be supplied by Hot oil to raise temperature from 150 C to 160 C = Heat to be supplied by Limpet of reactor Heat to be supplied by Limpet= Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Time for complete reaction Flowrate of hot oil required Flowrate of hot oil required

Kmol 10.65 0.61 46.88

T 0C

Penta-erithritol LiOMe PP Base

Kg 1450.00 23.05 13700.00

Kcal kcal/kg 0C 0 C kg hrs kg/hr m3/hr

89928.9 Kcal

220 0C

Density =

842 kg/m3

Flow of Oil required to Maintain T-160 C Calculation for Heat required to maintain temperature at 160 C Diameter of TR4101 = 2500 mm 2.5 m Height of TR4101 = 4200 mm 4.2 m (cylindrical portion) Surface area of reactor TR4101 thru which heat loss will occur = 32.99 m2 (cylindrical portion) considering the surface area of the top and bottom dish end 19.63 m2 dish end top and bottom Total surface area of reactor 52.62 m2 As per literautre, heat transfer coefficient for heat loss thru an insulated vessel= 2.15 kcal/hr m2 C source : http://www.spiraxsarco.com/Resources/Pages/Steam-Engineering-Tutorials/steam-engineering-principles-and-heattransfer/energy-consumption-of-tanks-and-vats.aspx Temperature inside the reactor = 160 0C Ambient temperature = 35 0C Heat to be supplied to maintain 160 C = 14142.08 kcal

2

Heat to be supplied by Limpet= Endothermic heat of reaction = Total Endothermic Heat of reaction= total heat to be supplied by Hot Oil= Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flowrate of hot oil required

Maintaining Temperature & Endothermicity

14142.08 24.00 364153.25 378295.32 0.64 230.00 59574.07 70.75

Kcal/hr kcal/kg .hr kcal/hr kcal/hr kcal/kg 0C 0 C kg m3/hr

as provided by GSI

220 0C Density =

842 kg/m3

As the flow rate of hot oil to the limpet is constrained by the flow rate of the pump PC4104 which is 30 m3/hr total heat to be supplied by Hot Oil= 378295.32 kcal/hr Specific Heat of Hot oil = 0.64 kcal/kg 0C 0 Inlet temperature of hot oil = 230.00 C Flow rate of hot oil = 30.00 m3/hr Flow rate of hot oil = 25260.00 kg/hr 0 Outlet temperature of hot oil = 206.42 C Calculating Log mean temperature difference 0 Hot oil inlet 230.00 C 0 process inlet 160.00 C LMTD = 57.40 Surface area of reactor TR4101 = Heat transfer coefficient = Reaction crude heating to 180 C Specific Heat of Reaction Mass = Heat to be supplied by Hot Oil =

0

Outlet Outlet

0

206.42 160.00

0

C C

C 52.62 125.24

0.60 182076.62

m2 as calculated above kcal/hr m2 C

kcal/kg 0C kcal

Heat to be supplied by Hot oil to raise temperature from 160 C to 180 C = Calculation for Heat required to maintain temperature at 180 C Diameter of TR4101 = 2500 mm Height of TR4101 = 4200 mm Surface area of reactor TR4101 thru which heat loss will occur = considering the surface area of the top and bottom dish end Total surface area of reactor

2.5 4.2

182076.62 Kcal

m m

(cylindrical portion) 32.99 m2 (cylindrical portion) 19.63 m2 dish end top and bottom 52.62 m2

3

As per literautre, heat transfer coefficient for heat loss thru an insulated vessel= 2.15 kcal/hr m2 C source : http://www.spiraxsarco.com/Resources/Pages/Steam-Engineering-Tutorials/steam-engineering-principles-and-heattransfer/energy-consumption-of-tanks-and-vats.aspx Temperature inside the reactor = 180 0C Ambient temperature = 35 0C Heat to be supplied to maintain 160 C = 16404.81 kcal As the flow rate of hot oil to the limpet is constrained by the flow rate of the pump PC4104 which is 30 m3/hr total heat to be supplied by Hot Oil= 198481.43 kcal/hr Specific Heat of Hot oil = 0.64 kcal/kg 0C 0 Inlet temperature of hot oil = 230.00 C Flow rate of hot oil = 25.00 m3/hr 25 m3/h going to Limpet and 5 m3/h going to FFE Flow rate of hot oil = 21050.00 kg/hr 0 Outlet temperature of hot oil = 215.15 C Calculating Log mean temperature difference 0 Hot oil inlet 230.00 C 0 process inlet 160.00 C LMTD = 50.59 Surface area of reactor TR4101 = Heat transfer coefficient = Heating the reaction mass to 203 C Specific Heat of Reaction Mass = Heat to be supplied by Hot Oil =

0

Outlet Outlet

215.15 180.00

0 0

C C

C 52.62 74.56

0.60 209388.12

m2 as calculated above kcal/hr m2 C

kcal/kg 0C kcal

Heat to be supplied by Hot oil to raise temperature from 180 C to 203 C =

209388.12 Kcal

Calculation for Heat required to maintain temperature at 203 C in reactor Diameter of TR4101 = 2500 mm 2.5 m Height of TR4101 = 4200 mm 4.2 m (cylindrical portion) Surface area of reactor TR4101 thru which heat loss will occur = 32.99 m2 (cylindrical portion) considering the surface area of the top and bottom dish end 19.63 m2 dish end top and bottom Total surface area of reactor 52.62 m2 As per literautre, heat transfer coefficient for heat loss thru an insulated vessel= 2.15 kcal/hr m2 C source : http://www.spiraxsarco.com/Resources/Pages/Steam-Engineering-Tutorials/steam-engineering-principles-and-heattransfer/energy-consumption-of-tanks-and-vats.aspx Temperature inside the reactor = 203 0C Ambient temperature = 35 0C Heat to be supplied to maintain 160 C = 19006.95 kcal

4

As the flow rate of hot oil to the limpet is constrained by the flow rate of the pump PC4104 which is 30 m3/hr total heat to be supplied by Hot Oil= 266261.01 kcal time 2.50 hrs total heat to be supplied by Hot Oil= 106504.40 kcal/hr Specific Heat of Hot oil = 0.64 kcal/kg 0C 0 Inlet temperature of hot oil = 230.00 C Flow rate of hot oil = 15.00 m3/hr 25 m3/h going to Limpet and 5 m3/h going to FFE Flow rate of hot oil = 12630.00 kg/hr 0 Outlet temperature of hot oil = 216.72 C Calculating Log mean temperature difference 0 Hot oil inlet 230.00 C 0 process inlet 180.00 C LMTD = 28.06 Surface area of reactor TR4101 = Heat transfer coefficient =

0

Outlet Outlet

216.72 203.00

0 0

C C

C 52.62 72.14

m2 as calculated above kcal/hr m2 C

for FFE As the flow rate of hot oil to the limpet is constrained by the flow rate of the pump PC4104 which is 30 m3/hr total heat to be supplied by Hot Oil= 347561.96 kcal time 2.50 hrs total heat to be supplied by Hot Oil= 139024.78 kcal/hr Specific Heat of Hot oil = 0.64 kcal/kg 0C 0 Inlet temperature of hot oil = 230.00 C Flow rate of hot oil = 15.00 m3/hr 25 m3/h going to Limpet and 5 m3/h going to FFE Flow rate of hot oil = 12630.00 kg/hr 0 Outlet temperature of hot oil = 212.67 C Calculating Log mean temperature difference 0 Hot oil inlet 230.00 C 0 process inlet 180.00 C LMTD = 24.54 Surface area of reactor TR4101 = Heat transfer coefficient =

0

Outlet Outlet

212.67 203.00

0 0

C C

C 52.62 107.65

m2 as calculated above kcal/hr m2 C

5

Crude MeOH

Kg 13838 1334.24

Kmol 16.51 41.64

T 0C Crude 160

Kg 13838

Kmol 16.51

180

Vacuum Stripping MEOH (stripped off)

At 400 mbar pressure, boiling point of Methanol =

42.86

0

C

At 20mbar pressure, boiling point of Methanol =

-10.50

0

C

T 0C

1334.14

41.64

Specific heat of Methanol Liquid= 0.60 kcal/kg 0C Specific heat of Methanol Vapour= 0.33 kcal/kg 0C 210.00 kcal/kg Latent Heat of Methanol @ 160C= 280.00 kcal/kg Latent Heat of Methanol @ 400 mbar= 293.00 kcal/kg Latent Heat of Methanol @ 20 mbar= Since the Latent heat value at 160 C and 400 mbar is not available, higher latent heat value is assumed

Vacuum Stripping of MeOH in EC-4111

Mass of Methanol evolved @ upto 400 mbar =

523.42

kg/hr

Time required for methanol evaluation = Assuming non-condensables =

1.70 10.00

hrs kg/hr

Mass of Methanol evolved @ upto 400 mbar =

533.42

kg/hr

172366.67

kcal/hr

Mass of Methanol evolved @ upto 20 mbar =

197.13

kg/hr

Time required for methanol evaluation = Assuming non-condensables =

1.70 10.00

hrs kg/hr

Mass of Methanol evolved @ upto 20 mbar =

207.13

kg/hr

Heat to be provided by Refrigerant Liquid @ 400 mbar =

Peak load As per GSI

Peak load As per GSI

Heat to be provided by Refrigerant Liquid @ 20 72273.44 kcal/hr mbar = Considering the peak heat load condition, maximum heat load will be considered Heat to be provided by Refrigerant Liquid for MeOH condensation

172366.67

kcal/hr

6

0.85

kcal/kg 0C

Temperature difference =

-20.00

to

Flow of Refrigrant Liquid = Flow of Refrigrant Liquid =

40556.86 36.21

kg/hr m3/hr

Specific Heat of Refrigarant Liquid =

Methanol removal at 2 mbar, condensed at the discharge of Vacuum pump, at atmospheric conditions At atmospheric pressure, boiling point of Methanol 0 64.60 C = Specific heat of Methanol Liquid= 0.60 kcal/kg 0C Specific heat of Methanol Vapour = 0.33 kcal/kg 0C Latent Heat of Methanol @ 160C and atm Atmospheric Stripping of 262.50 kcal/kg pressure= MeOH in EC-4110 Mass of Methanol evolved @ 2 mbar = 35.00 kg/hr Refrigrant Liquid load to condense second cut of 10904.29 kcal/hr Specific Heat of Refrigarant Liquid = 0.85 kcal/kg 0C

Crude

Temperature difference =

-7.00

to

Flow of Refrigrant Liquid = Flow of Refrigrant Liquid =

1425.40 1.27

kg/hr m3/hr

Kg 13838

Kmol 16.51

T 0C 160

-15

0

C

Density =

Considering a dedicated chilling plant for this Heat exchanger 1120 kg/m3

Peak load As per GSI

2

0

C

Density =

PP base Heating and recovery TR-4101

Crude

PP Base

temperature range as mentioned by GSI, as per utility details mentioned, Inlet RL temperature is -10 C 1120 kg/m3 Kg 12372

Kmol 16.51

T 0C

3520.00

12.04

203

203

With the flow rate of the pump only 30 m3/h, assuming 50% going to limpet and 50% to FFE. Specific Heat of Reaction Mass = Heat to be supplied by Hot Oil =

0.60 410003.92

kcal/kg 0C kcal

Heat to be supplied by Hot oil to raise temperature from 160 C to 203 C =

410003.92 Kcal

7

Reactor heating

Heat to be supplied by Limpet= Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Time Flow of Hot oil = Flow of Hot oil =

347561.96 0.64 230.00 54734.17 2.50 21893.67 26.00

Kcal kcal/kg 0C 0 C kg hr kg/hr m3/hr

220 0C as given by GSI Density =

842 kg/m3

As the flow rate of hot oil to the limpet is constrained by the flow rate of the pump PC4104 which is 30 m3/hr total heat to be supplied by Hot Oil= 347561.96 kcal time 2.50 hrs total heat to be supplied by Hot Oil= 139024.78 kcal/hr Specific Heat of Hot oil = 0.64 kcal/kg 0C 0 Inlet temperature of hot oil = 230.00 C Flow rate of hot oil = 15.00 m3/hr 25 m3/h going to Limpet and 5 m3/h going to FFE Flow rate of hot oil = 12630.00 kg/hr 0 Outlet temperature of hot oil = 212.67 C Calculating Log mean temperature difference 0 Hot oil inlet 230.00 C 0 process inlet 180.00 C LMTD = 24.54 Surface area of reactor TR4101 = Heat transfer coefficient = Heat to be supplied by recirculation HE= Mass of PP base= Specific Heat of PP Base Assuming Latent heat of PP base = PP Base evaporation in Total heat to be supplied to FFE = FFE Time to strip PP base = Total heat to be supplied to FFE = Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

0

Outlet Outlet

212.67 203.00

0 0

C C

C 52.62 107.65

m2 as calculated above kcal/hr m2 C

410003.92

Kcal

3520.00 0.51 81.00 347561.96 2.50 139024.78 0.64 230.00 21893.67 26.00

kg kcal/kg 0C kcal/kg kcal hr kcal/hr kcal/kg 0C 0 C kg/hr m3/hr

Falling Film Evaporator

as given by GSI as given by GSI

220 0C Density =

842 kg/m3

8

As the flow rate of hot oil to the limpet is constrained by the flow rate of the pump PC4104 which is 30 m3/hr total heat to be supplied by Hot Oil= 347561.96 kcal time 2.50 hrs total heat to be supplied by Hot Oil= 139024.78 kcal/hr Specific Heat of Hot oil = 0.64 kcal/kg 0C 0 Inlet temperature of hot oil = 230.00 C Flow rate of hot oil = 15.00 m3/hr 25 m3/h going to Limpet and 5 m3/h going to FFE Flow rate of hot oil = 12630.00 kg/hr 0 Outlet temperature of hot oil = 212.67 C Calculating Log mean temperature difference 0 Hot oil inlet 230.00 C 0 process inlet 180.00 C LMTD = 24.54 Surface area of reactor TR4101 = Heat transfer coefficient =

0

Outlet Outlet

212.67 203.00

0 0

C C

C 52.62 107.65

m2 as calculated above kcal/hr m2 C

Assuming Recovered PP base to be kept in molten state above is boiling point Thus assuming PP base to be condensed till 90 C Mass of PP base= Specific Heat of PP Base Latent heat of PP base = Heat to be removed by tempered water = Assuming time = PP base condensation in Heat to be removed by tempered water = EC4112 Specific Heat of tempered Refrigrant Liquid =

3520.00 0.51 81.00 487977.60 2.50 195191.04

kg kcal/kg 0C kcal/kg kcal hrs kcal/hr

0.85

kcal/kg 0C

Temperature difference for Tempered Refrigrant Liquid Flow of Tempered Refrigrant Liquid= Flow of Tempered Refrigrant Liquid=

80.00

0

22963.65 20.50

kg/hr m3/hr

Genetration of Tempered water at start up Hold up of RL inside EC4112 Hold up of RL inside ET4112 Hold up of RL inside connecting pipe line and pump total hold up of RL inside system total hold up of RL inside system Specific Heat of tempered Refrigrant Liquid =

0.31 1.78 0.39 2.98 3342.34 0.85

m3 m3 m3 m3 kg kcal/kg 0C

80.00

0

3342.34 255688.83 255688.83 500.60 510.76

kg/hr kcal/hr kcal/hr kcal/kg kg/hr

Temperature difference for Tempered Refrigrant Liquid

Tempered Water Generation for Startup Flow of Tempered Refrigrant Liquid= Enthalpy in Tempered water ET-4112 Heat to be provided by Steam Latent heat of Steam Flow of steam required

as given by GSI as given by GSI

90 0C

C

C

Density =

1120 kg/m3

considering 20% margin of safety)

-10 0C to be heated in 1 hr

9

Kg Crude

13838.09

Kg Crude

13838.09

Kmol 16.51

Kmol

160

Transfer to TR-4102 maintain T=160 0C Heating with Recirculation

160

Filtration FC-4101 ( transferred in 3 batches)

T 0C

T 0C

16.51

Specific Heat of Reaction Mass =

TR4102 maintain

0.60

Kg Crude

13838.09

Kg Crude

13838.09

Kmol

T 0C

16.51

Kmol 16.51

160

T 0C 160

kcal/kg 0C

Calculation for Heat required to maintain temperature at 160 C Diameter of TR4102 = 2700 mm 2.7 m Height of TR4102 = 4500 mm 4.5 m (cylindrical portion) Surface area of reactor TR4101 thru which heat loss will occur = 38.17 m2 (cylindrical portion) considering the surface area of the top and bottom dish end 22.90 m2 dish end top and bottom Total surface area of reactor 61.07 m2 As per literautre, heat transfer coefficient for heat loss thru an insulated vessel= 2.15 kcal/hr m2 C source : http://www.spiraxsarco.com/Resources/Pages/Steam-Engineering-Tutorials/steam-engineering-principles-and-heattransfer/energy-consumption-of-tanks-and-vats.aspx Temperature inside the reactor = 203 0C Ambient temperature = 35 0C Heat to be supplied to maintain 160 C = 22059.41 kcal Heat to be supplied by hot oil in Reactor Limpet=

22059.41

kcal/hr

Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

0.635 230 3473.923 4.126

kcal/kg 0C 0 C kg/hr m3/hr

Crude

Kg 13838.09

Kmol 16.51

MeOH + Water (7%) MeOH Water

20800.37 19304.13 1453.00

683.22 602.50 80.72

220 0C Density =

842 kg/m3

T 0C 160

Crystallization TR-4201

Crude MeOH + Water (7%)

Kg 13838.09 20800.37

Kmol 16.51 683.22

T 0C 5 15-20

10

10

Considering the reaction mass is divided in to

Vacuum Chilling

2.00

batches

total Mass of MeOH to be chilled = Mass of MeOH to be chilled per batch

20800.37 10400.18

kg kg/batch

Inlet temperature of MeoH MeOH to be chilled to Specific heat of MeOH Heat required to Chill MeOH Time for chilling Heat required to Chill MeOH

35.00 10.00 0.60 156002.76 1.50 104001.84

0

C C kcal/kg 0C kcal hr kcal/hr

Applying vacuum to chill MeOH Boiling point of MeOH at 74 mm Hg Latent Heat of MeOH at 74 mm Hg Mass of MeOH evoporated

74.00 15.00 291.00 357.39

mmHg 0 C kcal/kg kg/hr

Mass of MeOH to be condensed in ET4210

357.39

kg/hr

0.60 291.00 15.00 10.00 105074.02

kcal/kg 0C kcal/kg 0 C 0 C kcal/kg

105074.02 0.85

kcal/hr kcal/kg 0C

Temperature difference =

-7.00

to

Flow of Refrigrant Liquid = Flow of Refrigrant Liquid =

13735.17 12.26

kg/hr m3/hr

Mass of reaction crude added to crystallizer Number of batches of crystallization

13838.09 2.00

kg

Mass of reaction crude added to crystallizer

6919.04

kg/batch

Time taken to charge crude = Mass of reaction crude added to crystallizer Specific heat of reaction crude Enthalpy of Crude

2.50 2767.62 0.60 207571.30

hr kg/hr kcal/kg 0C kcal/hr

Specific heat of MeOH (liquid) Latent Heat of MeOH at 74 mm Hg Inlet Temperature Outlet Temperature ET4210 load for MeOH Heat to be removed chilling Refrigrant Liquid load to condense MeOH = Specific Heat of Refrigarant Liquid =

0

2

0

C

temperature range as mentioned by GSI, as per utility details mentioned, Inlet RL temperature is -10 C

Density =

1120 kg/m3

as per timecycle given by GSI

11

ET4210 load during Crude addition

Chilling of Crude for crystallization

Crude MeOH + Water (7%)

Mass of Methanol water added to crystallizer Number of batches of crystallization Mass of MeOH Water added to crystallizer Specific heat of MeOH water Enthalpy of MeOH Time of addition of Crude Enthalpy of Methanol

20800.37 2.00 10400.18 0.60 -156002.76 2.50 -62401.10

kg/batch kcal/kg 0C kcal/batch hrs kcal/hr

Heat load to be taken by the condenser = Specific Heat of Refrigarant Liquid = Temperature difference = Flow rate of Refrigerant liquid required to Remove Flow rate of Refrigerant liquid required to Remove

145170.19 0.85 -7.00 18976.50 16.94

kcal/hr kcal/kg 0C to kg/hr m3/hr

Considering Heat balance per batch Mass of Crude in TR4201 Specific Heat of Reaction Mass = Enthalpy of Reaction mass =

6919.04 0.60 518928.24

kg/batch kcal/kg 0C kcal/batch

Mass of MeOH in TR4201 Specific Heat of Methanol solution= Enthalpy of Methanol solution =

10400.18 0.60 -156002.76

kg/batch kcal/kg 0C kcal/batch

Enthalpy of Mixture = Time for chilling = Enthalpy of Mixture = Amount of MeOH evaporated

362925.48 2.50 145170.19 498.87

kcal/batch

Heat load to be taken by the condenser = Specific Heat of Refrigarant Liquid = Temperature difference = Flow rate of Refrigerant liquid required to Remove Flow rate of Refrigerant liquid required to Remove

145170.19 0.85 -7.00 18976.50 16.94

kcal/hr kcal/kg 0C to kg/hr m3/hr

Kg 13838.09 20800.37

Kmol 16.51 683.22

kg

kcal/hr kg/hr

2 0C Density =

1120 kg/m3

maintain vacuum of 74 mm Hg

2 0C Density =

1120 kg/m3

T 0C 20.00

Hold up in TR-4202

Crude MeOH + Water (7%)

Kg 13838.09 20800.37

Kmol 16.51 683.22

T 0C 15

12

Chilling in TR4202

Slurry Product MeOH Water MeOH Wash MeOH Water

Capacity check for ET4301

Wet Cake MeOH Water

Mass of Crude in TR4202 Mass of MeOH in TR4202 Specific Heat of solution= heat to be provided by RL to chill = Time for chilling = heat to be provided by RL to chill = Specific Heat of Refrigarant Liquid = Temperature difference = Flow rate of Refrigerant liquid required to Remove Flow rate of Refrigerant liquid required to Remove Kg 34638.96 13862.38 19323.58 1453.00

Kmol

6919.04 10400.18 0.60 51957.68 0.5 103915.363 0.85 -7.00 13583.71 12.13

kg/batch kg/batch kcal/kg 0C kcal hr kcal/hr kcal/kg 0C to kg/hr m3/hr

2 0C Density =

T 0C

15

Centrifuging Feed capacity 602kg/cycle Cycle time 30min

6813.77 6677.50 136.28 Mass of MeOH Water mix to be chilled Specific Heat of solution=

3000.00 0.61

kg/h kcal/kg 0C

heat to be provided by RL =

45600.00

kcal/hr

heat to be provided by chilled water= Specific Heat of Chilled Water= Temperature difference = Flow rate of Chilled water Flow rate of Chilled water

45600.00 1.00 -7.00 5066.67 5.07

kcal/hr kcal/kg 0C to kg/hr m3/hr

Kg 13093.16 1826.52 137.48

Kmol

1120 kg/m3

Wet Cake Product MeOH Water

Kg 13093.16 11129.16 1826.52 137.48

Mother Liquor

28359.57

15

T 0C 15

15

MeOH from solvent recovery to be chilled to 20 C as mentioned by GSI

2 0C Density =

1000 kg/m3

T 0C Drying

Kmol

Product

Kg 11129.16

Solvent MeOH water

1964.00 1826.52 137.48

Kmol

T 0C 64.5

64.5

13

Capacity check for EC4401

Mass of MeOH Water evaporated in DA4401 Specific Heat of solution= Latent heat of MeOH water at 250 mmbar heat to be provided by RL = Capacity of Dryer = Total drying time per batch of Anox 20 = heat to be provided by Chilled water Specific Heat of Chilled Water= Temperature difference = Flow rate of Chilled Water Flow rate of Chilled Water

1964.00 0.63 280.00 586305.064 585 19 30818.9 1.00 10.00 3852.36 3.85

kg/batch kcal/kg 0C kcal/kg 0C kcal kg/hr hr kcal/hr kcal/kg 0C to kg/hr m3/hr

18 0C Density =

1000 kg/m3

Methanol Recovery

Mother Liquor Tars MeOH Water

Kg 31657.81 2733.34 27335.32 1589.27

Kmol

T 0C

Tars (total) Tars Water MeOH

Tar Separation MeOH distillation TP4601 TP4604

10

MeOH water MeOH Water

Kg 3037.05 2733.34 151.85 151.85 28620.76 27183.5 1437.42

Kmol

T 0C 100

100

Assuming the Mixture is heated to Temperature of 80 C which is above the boiling point of Water+MeOH 0.6 276.44

kcal/kg 0C kcal/kg

9621389.08

kcal

Heat to be provided by Hot Oil Heat to be provided by Hot Oil Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

9621389.08 506388.90 0.64 230.00 79746.28 94.71

kcal kcal/hr kcal/kg 0C 0 C kg/hr m3/hr

Heat to be provided by Steam Heat to be provided by Steam Latent heat of Steam Flow of steam required

9621389.08 506388.90 500.60 1011.56

kcal kcal/hr kcal/kg kg/hr

90.00 170.00

0

Specific Heat of Mixture = Latent Heat of MeOH water Mixture Heat to be supplied by Steam to heat from 10 C to 90 C =

Vessel Reboiler Load

Vessel Reboiler Load

Steam generation using Hot oil Inlet temperature of condensate Steam generation temperature

0

C C

220 0C Density =

842 kg/m3

as per utility details provided by GSI

14

Latent heat of steam at 7 bar (g) Heat to be provided by Hot oil Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

MeOH water MeOH Water

Kg 28620.76 27183.46 1437.42

Kmol

488.80 575377.56 0.64 230.00 90610.64 107.61

Reboiler load

220 0C Density =

T C 90

842 kg/m3

MeOH + Water (2%) MeOH Water

0

Feed rate to column = Cycle time for distillaition Reflux ratio

Condenser load

kcal/kg kcal/hr kcal/kg 0C 0 C kg/hr m3/hr

Methanol - Water Distillation

MeOH + Water (96%) MeOH Water 28620.76 1506.36 19.00 3.00

Total MeOH water mixture to be condensed Specific heat of mixture Latent heat of MeOH Water mixture = Heat to be supplied by Chilled water = Heat to be supplied by Chilled water = Specific Heat of Chilled water = Temperature difference = Flow rate of Chilled Water required to Remove heat Flow rate of Chilled Water required to Remove heat

32484.300 0.608 268.05 13881520.74 730606.3546 1.00 10.00

Total MeOH water mixture to the reboiler Specific heat of mixture Latent heat of MeOH Water mixture = Heat to be supplied by hot oil= Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

442.040 0.608 268.05 216895.0272 0.64 230.00 34156.70 40.57

Kg 27700.67 27146.66 554.01 920.10 36.81 883.41

Kmol

T 0C 35

35

kg kg/hr hr

kg kcal/kg K kcal/kg kcal kcal/hr

taken from PRO II simulation

0

kcal/kg C to

91325.8

kg/hr

91.3

m3/hr kg/hr kcal/kg K kcal/kg kcal kcal/kg 0C 0 C kg/hr m3/hr

18 0C

Density =

1000 kg/m3

taken from PRO II simulation 220 0C Density =

842 kg/m3

15

Feed to column F= Mole Fraction in MeOH= H2O = Distillate Bottom Feed

Tars MeOH Water

D W F

Distillate D= MeOH = Water =

1457.9 kg/h 1428.8 kg/h 29.2 kg/h

Bottoms B= MeOH = Water =

48.4 kg/h 1.9 46.5 kg/h

1506.36 kg/h 0.95 1430.7 kg/h 75.6 kg/h xd= xw = xf =

Kg 12148.18 607.41 607.41

0.98 0.04 0.95

Kmol -

T 0C 35

Tars washing MeOH stripping (vacuum 100 Tor)

Kg 10933.36

Tars

MeOH Water 0.60

kcal/kg 0C

433.35

kcal/kg

Heat to be supplied by Hot Oil = Time taken Heat to be supplied by Hot Oil = Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

1291779.56 3.50 184539.94 0.64 230.00 29061.41 34.51

kcal hrs kcal/hrs kcal/kg 0C 0 C kg m3

Specific Heat of Tars Heat to be supplied by Hot Oil = Time taken Recirculation Heating Heat to be supplied by Hot Oil = ER4151 (50% by limpet Specific Heat of Hot oil = and 50% by HE) Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

0.60 1291779.56 3.50 184539.94 0.64 230.00 29061.41 34.51

kcal/kg 0C kcal hrs kcal/hrs kcal/kg 0C 0 C kg m3

Specific Heat of Tars Latent heat of MeOH Water mixture at 100 torr Limpet Heating and vapourization (50% by limpet and 50% by HE)

98% wt 2% wt

607.41 607.41

Kmol -

T 0C 140

-

140

220 0C Density =

842 kg/m3

220 0C Density =

842 kg/m3

16

MeOH condensation EC4102A

Specific heat of Methanol Water Mixture @ 140 C = Latent Heat of Methanol Water Mixture at 100 torr= Mass of Methanol Water Mixture evolved = Time required for methanol evaluation = Mass of Methanol Water Mixture evolved = Chilled water load to condense MeOH Water Mixture = Specific Heat of Chilled Water = Temperature difference = Flow of Chilled Water = Flow of Chilled Water =

Specific Heat of Remaining Tars = Mass to be cooled Time to be cooled in Mass to be cooled Temperature range to be cooled Reaction Mass cooling Chilled water load = Specific Heat of Chilled Water = Temperature difference = Flow of Chilled water = Flow of Chilled water = Specific Heat of Tars Mass to be heated = Temperature range to be Heated Latent Heat of Cyclohexane Limpet Heating Heat to be supplied by Hot Oil = Cyclo-Hexane stripping Time taken (50% by limpet and 50% Heat to be supplied by Hot Oil = by HE) Specific Heat of Hot oil = Temperature difference for Hot Oil Flow of Hot oil = Flow of Hot oil =

140.00

0.60 22339.97 60.00 95.00 2060318.77 5.50 187301.71 0.64 230.00 29496.33 35.03

0.729 433.35 1214.82 4.5 270.0 137651.6 1 10 17206.46 17.21

kcal/kg 0C kcal/kg kg hrs kg/hr kcal/hr kcal/kg 0C to kg/hr m3/hr

0.6 10933.36 1.50 7288.91 0 C 284267.4 1.00 10.00 35533.43 35.53

kcal/kg 0C kg hrs kg/hr

kcal/kg 0C kg 0 C kcal/kg kcal hrs kcal/hrs kcal/kg 0C 0 C kg m3

(As per GSI) (As per GSI)

18 0C Density =

1000 kg/m3

75 0C kcal/hr kcal/kg 0C to kg/hr m3/hr

18 0C Density =

1000 kg/m3

140 0C

220 0C Density =

842 kg/m3

17

Heat to be supplied by Hot Oil = Recirculation Heating Time taken Heat to be supplied by Hot Oil = ER4151 Cyclo-Hexane stripping Specific Heat of Hot oil = (50% by limpet and 50% Temperature difference for Hot Oil by HE) Flow of Hot oil = Flow of Hot oil =

Cyclohexane condensation EC4102A

Specific heat of Cyclohexane @ 140 C = Latent Heat of Cyclohexane @ 140 C and 100 Torr= Mass of Methanol Water Mixture evolved = Time required for methanol evaluation = Mass of Methanol evolved @ 20 mbar = Chilled Water load to condense Cyclohexane = Specific Heat of Chilled Water = Temperature difference = Flow of Chilled Water = Flow of Chilled Water =

2060318.77 5.50 187301.71 0.64 230.00 29496.33 35.03

kcal hrs kcal/hrs kcal/kg 0C 0 C kg m3

Density =

0.45 95 10400.00 5.5 1890.9 268981.8 1 10 33622.73 33.62

kcal/kg 0C kcal/kg kg hrs kg/hr kcal/hr kcal/kg 0C to kg/hr m3/hr

220 0C 842 kg/m3

(As per GSI) (As per GSI)

18 0C Density =

1000 kg/m3

18

LIBRA TECHCON LTD. MUMBAI

SR NO 1 2 3 4 5 6 7

Refrigerant Liquid Point of Use  0 0 Vacuum Stripping of MeOH in EC4111(‐20 Cto ‐15 C ) Atmospheric Stripping of MeOH in EC4110 Vacuum Chilling of MeOH for crystallization in ET4210 Load on ET4210 during crude addition Load on ET4210 during crude addition Chilling of crude in Crystallizer TR4201 Maintaining Temp in crude hold up vessel TR4202 MeOH chilling in ET4301

12 13 14 15

Chilled Water Solvent condensation in EC4401 Solvent condensation in EC4401 Top product condensation in Distillation EC4610A/B Hot oil chilling in ET4102 Hot oil chilling in ET4111 Total exclding tars washing MeOH stripping during tars washing  in EC4102A Reaction Mass cooling during tars washing in ET4152 C Cyclohexane Condensation in EC4102A  l h C d i i EC4102A Hot oil chilling in ET4151 Total load required for tars washing

PLANT:

Anti-oxidants p plant

CLIENT :

Gulf Stabilizers Industries

Heat Load 172366.67 kcal/hr 10904.29 kcal/hr 105074.02 kcal/hr 145170 19 145170.19 kcal/hr 145170.19 kcal/hr 103915.36 kcal/hr 45600.00 kcal/hr

Heat Load 57.00 3.61 34.75 48 01 48.01 48.01 34.36 15.08

TR TR TR TR TR TR TR

Mass flow rate of RL 40556.86 kg/hr 1425.40 kg/hr 13735.17 kg/hr 18976 50 18976.50 kg/hr 18976.50 kg/hr 13583.71 kg/hr 5066.67 kg/hr

477956.52

kcal/hr

158.05

TR

79609.13

kg/hr

71.62

m3/hr

Drying Solvent Recovery Reaction Reaction

30818 89 30818.89 730606.35 92480.00 92480.00 853905.24

kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr

10 19 10.19 241.60 30.58 30.58 282.38

TR TR TR TR TR

3852 36 3852.36 91325.79 11560.00 11560.00 106738.16

kg/hr kg/hr kg/hr kg/hr kg/hr

3 85 3.85 91.33 11.56 11.56 106.74

m3/hr m3/hr m3/hr m3/hr m3/hr

Tars washing Tars washing TTars washing hi Tars washing

137651.65 284267.43 268981.82 268981 82 92480.00 645729.25

kcal/hr kcal/hr kkcal/hr l/h kcal/hr kcal/hr

45.52 94.00 88.95 88 95 30.58 213.53

TR TR TR TR TR

17206.46 35533.43 33622.73 33622 73 11560.00 80716.16

kg/hr kg/hr kkg/hr /h kg/hr kg/hr

17.21 35.53 33 33.62 62 11.56 80.72

m3/hr m3/hr m3/hr 3/h m3/hr m3/hr

Section Reaction Reaction Crystallization Crystallization Crystallization Crystallization Centrifuging

Total load required for Refrigerant liquid (peak load)

8 9 10 11

SHEET:

Anox20 RL and Chilled Water Capacity

Volumetric flowrate of RL 36.21 m3/hr 1.27 m3/hr 12.26 m3/hr 16 94 16.94 m3/hr 16.94 m3/hr 12.13 m3/hr 5.07 m3/hr

Peak peak peak peak peak

peak peak peak peak

peak peakk peak

Hot oil point of use

Section

Heat Load

Mass flow rate of hot oil

Mass flow rate of hot oil Volumetric flowrate of hot oil

16 17 18 19 20 21 22 23

heating of PP base in ET4101 reaction mass heating in TR4101 maintain temperature & endothermicity in TR4101 reactor heating ‐ PP base stripping in TR4101 FFE ‐ PP base stripping in ET4110 heating maintain in TR4102 TP 4604 vessel reboiler ER4610 Distillation column reboiler ER4611 Total excluding tars washing g g

reaction reaction reaction reaction reaction reaction fractionation fractionation

436050.00 89928.90 378295.32 139024.78 139024.78 22059.41 506388.90 216895.0272 1159333.93

kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr

68669.29 14162.03 25260.00 21893.67 21893.67 3473.92 79746.28 34156.70 182572.27

kg/hr kg/hr kg/hr kg/hr kg/hr kg/hr kg/hr kg/hr kg/hr g

68.67 14.16 25.26 21.89 21.89 3.47 79.75 34.16 182.57

Ton/hr Ton/hr Ton/hr Ton/hr Ton/hr Ton/hr Ton/hr Ton/hr Ton/hr

81.55 16.82 30.00 26.00 26.00 4.13 94.71 40.57 216.83

3 m /hr m3/hr m3/hr m3/hr m3/hr m3/hr m3/hr m3/hr m3/hr

24 25 26 27

limpet heating ‐ for tars washing in TR4151 Tars Heating in ER4151 limpet heating(cyclohexane) in TR4151 Tars Heating (cyclohexane) in ER4151 total load required for tars washing

tar washing tar washing tar washing tar washing

184539.94 184539.94 187301.71 187301.71 374603.41

kcal/hr kcal/hr kcal/hr kcal/hr kcal/hr

29061.41 29061.41 29496.33 29496.33 58992.66

kg/hr kg/hr kg/hr kg/hr kg/hr

29.06 29.06 29.50 29.50 58.99

Ton/hr Ton/hr Ton/hr Ton/hr Ton/hr

34.51 34.51 35.03 35.03 70.06

m3/hr m3/hr m3/hr m3/hr m3/hr

Steam point of use 28

heat to be supplied by steam in ET4112

29 30 31

Steam for generating hot water in EP4401 Steam for generating hot water in EP4402 Steam for generating hot water in EP4403

section tempered water  generation Drying Drying Drying

heat load

Mass flow rate of steam

255688.83

kcal/hr

510.76

kg/hr

30000 30000 30000

kcal/hr kcal/hr kcal/hr

60 60 60

kg/hr kg/hr kg/hr

peak

peak peak

peak peak peak

peak peak

LIBRA TECHCON LTD. MUMBAI

Anox20 Utility Capacity summary

Steam

Current Entire plant Entire plant - current Anox 20 process Current Anox 20 process usage New Anox 20 process requirement Total requirement (Entire plant current Anox 20 process + New Anox 20 Process) Current utility capacity Capacity usage of the plant Spare capacity available

Mkcal/hr 2.25 1.05 1.20 0.09 1.14 2.044 55.91% 0.90

Hot Oil

Current Entire plant Entire plant - current Anox 20 process Current Anox 20 process usage New Anox 20 process requirement Total requirement (Entire plant current Anox 20 process + New Anox 20 Process) Current utility capacity Capacity usage of the plant Additional capacity required

Mkcal/hr 4.21 2.70 1.51 1.16 3.86 3.18 121.50% 0.68

need to be checked

SHEET: PLANT: CLIENT :

Anti-oxidants plant Gulf Stabilizers Industries

Chilled water requirement Mkcal/hr 3.09

TR 1020.93

1.06

351.44

Current Anox 20 process usage

2.02

669.49

New Anox 20 process requirement

0.85

282.38

1.92

633.81

2.4 79.86% 0.48

793.65

Mkcal/hr 1.51

TR 498.60

1.26

415.67

0.25

82.93

0.48

158.05

1.73

573.73

1.46 118.83% 0.27

482.80

Current Entire plant Entire plant - current Anox 20 process

Total requirement (Entire plant current Anox 20 process + New Anox 20 Process) Current utility capacity Capacity usage of the plant Spare capacity available

Refrigerant Liquid

Current Entire plant Entire plant - current Anox 20 process Current Anox 20 process usage New Anox 20 process requirement Total requirement (Entire plant current Anox 20 process + New Anox 20 Process) Current utility capacity Capacity usage of the plant Additional capacity required

But the refrigerant liquid required for the new plant will require a temperature range of -20 to -15 deg C Thus a new plant will have to be procured.

Current Entire plant Entire plant - current Anox 20 process Current Anox 20 process usage New Anox 20 process requirement Total requirement (Entire plant current Anox 20 process + New Anox 20 Process) Current utility capacity Capacity usage of the plant Spare capacity available

Mkcal/hr 1.51

TR 498.60

1.26

415.67

0.25

82.93

0.00

0.00

1.26

415.67

1.46 86.10% 0.20

482.80

Thus a new RL plant with temperature range from (-20 to -15 deg C) will free up capacity in the existing plant

DOC NO CAD NO PLANT REV Client: GSI

Project:  Anox20 modification and process revamp

EL‐001 EL‐001 GSI, Saudi Arabia R0

CONTACT NO

EQUIPMENT LIST

R5

4‐Dec‐17

ISSUED FOR APPROVAL

VG

MSB

MSB

R4

9‐Oct‐17

ISSUED FOR APPROVAL

VG

MSB

MSB

ISSUED FOR APPROVAL

VG

MSB

MSB

ISSUED FOR APPROVAL

VG

MSB

MSB MSB

R3 R2

1‐Sep‐17

R1

23‐Aug‐17

ISSUED FOR APPROVAL

VG/SD

MSB

R0

21‐Aug‐17

ISSUED FOR APPROVAL

VG/SD

MSB

MSB

REV

DATE

DESCRIPTION

PREPARED BY

CHECKED BY

APPROVED BY

DOC No. : CAD No. : REV No. : PLANT : CONTRACT No. :

EQUIPMENT LIST - Reaction Client:

M/s Gulf Stabilizer Industries Ltd.

GSI

QTY SR. NO.

EQPT. TAG NO.

Locat ion

MOC

CAPACITY

SIZE

CONDITIONS

DIA x HT. (m)

OPERATING PRESSURE (bar)

DESCRIPTION

1 2 3 4

PK4101 BF4101 BH4101 TS4101

Pentaerythritol bag cutting Unit BH4101 Blower Pentaerythritol hopper baghouse Pentaerythritol hopper

1 1 1 1

SF SF SF FF

SS304L SS304L SS304L

2.5 m3

φ1000/1500 x 1900

5

ET4101

PPBase preheater

1

SF

SS304L

21 m2

φ350 x 3660

6

TP4114

Catalyst loading vessel

1

SS316

1 m3

φ1020 x 1250

7

TR4101

Synthesis reactor

8

MA4101

TR4101 Agitator

9

ET4102

TR4101 circulation oil cooler

10

PC4104

11

1

FF

SS304L

24 m3

1

GF

CS

7.4 m2

TR4101 Jacket Hot Oil Circulation

1

GF

CS

30m3/hr, 18.6m

ET4110

Reaction Mass Recirculation FFE

1

FF

SS316

36.7m2

φ500 x 2500

12

PC4110

Reaction Mass Recirculation Pump

1

GF

SS316

30 m3/hr, 18.6 m

-

13

EC4112

PP Base Vapour Condenser

1

SF

SS316

19.55 m2

Ø450 x 2500

14

TP4113

Cold Trap

1

TF

SS316

15

EC4111

TR4101 Vapor condenser - Vacuum

1

SF

SS316

22.94 m2

φ450 x 2500

16

EC4110

TR4101 Vapor condenser - Atmospheric

1

SF

SS316

2.51 m2

φ200 x 1500

17 18 19 20 21 22 23

TP4110 TP4111 TP4112 PC4105 PC4106 PK4102 TR4102

methanol collector - Atmospheric Methanol Collector - Vacuum PP Base Collector CP4601 Feed / Methanol to distillation CP4601 Feed / Methanol to distillation Vacuum Pump Crude product Dilution tank

1 1 1 1 1 1 1

FF FF FF GF GF FF FF

SS316 SS316 SS316 SS304L SS304L SS304L SS304L

3 m3 2 m3 2 m3 3m3/hr, 26.4 3m3/hr, 20.3 5000 N3/hr 30.8 m3

φ1530 x 1875 φ1300 x 1600 φ1300 x 1600

TR4102 Agitator

1

25

TS4110

Dryer Product Loading Hopper

1

26

PC4111

TR4102 Jacket Hot Oil Circulation

1

27

ET4111

TR4102 circulation oil cooler

28

PC4113

29 30 31

FC4101 PC4112 ET4112

FF

FV to atm

φ2500 x 4200

SS304L

MA4102

DESIGN PRESSURE (bar)

OPERATING TEMP. (ºC)

DESIGN TEMP. (ºC)

250 Nm3/hr

FF

24

EMPTY WEIGHT

0.3/-0.03 shell - 6 Tube - 10 FV to 3.5

35

210

6

shell - 10 Tube - 6

φ200 x 2440 shell - 4 Tube - FV shell - 4 Tube - FV

shell - 10 Tube - 6 shell - 6 Tube - FV to 6

150 shell - 220 Tube - 260 60

shell - 200 Tube - 150 shell - 240 Tube - 160 shell - 70 Tube - 160

shell - 260 Tube - 200 shell - 90 Tube - 260

Installed

φ2700 x 4500

shell - 6 Tube - FV to 6 shell - 6 Tube - FV to 6 FV to 6 FV to 6 FV to 6

shell - -20/-15 Tube - 160 shell - -20/-15 Tube - 160 35 35 90

shell - -20/60 Tube - 260 shell - -20/60 Tube - 260 60 60 100

210

6

SS304L SS304L

2.5 m3

φ1000/1500 x 1900

GF

CS

30m3/hr, 18.6m

-

-

E E E E

Pentaerythritol Nitrogen blanketing

-

E

TEMA Class - BEU

-

-

1

GF

CS

7.4 m2

φ250 x 2440

TR4151 Transfer Pump

1

GF

SS304L

15 m3/hr, 29 m

-

Raw product filter Tempered water pump Tempered water heat excahnger

1 1 1

GF GF FF

SS304L CS CS

4 m2 30m3/hr, 18.6m 11.38 m2

0.48 x 1.58 x 1.5

-

E

Flanges of reactor to be converted to SORF so that Vacuum tightness can be achieved

30

N

To be modified for Up-Pumping flow with double mechanical seal suitable for vacuum

-

E

3.7

E

-

N

-

3.7

-

N

-

-

N

-

4.5/3.5

6 6/6

-

TEMA Class - BEM Magnetic Drive Centrifugal

Double Mechanical Seal

N -

N

-

N

3.7 2.2 15 -

N N N E E N E

TEMA Class - BEM TEMA Class - BEM Jacketed Jacketed Magnetic Drive Centrifugal Single Mechanical Seal, Centrifuga

To be modified for Up-Pumping flow with double mechanical seal suitable for vacuum

N

150

-

N

-

3.7

N

Magnetic Drive Centrifugal

shell - 200 Tube - 150

-

N

TEMA Class - BEM

-

-

3.7

N

Magnetic drive centrifugal

-10/70

210 170

3.7 -

E N N

CRT Type, For Anox20 Magnetic Drive

-

shell - 10 Tube - 6 -

N

25 0.3/-0.03 -

REMARKS

Kg

shell - 4 Tube - FV shell - 4 Tube - atm. atm. FV to atm FV to atm

Exisiting / New

EL-001 EL-001

-

d same as exsiting PC4104 and ET-

DOC No. : CAD No. : REV No. : PLANT : CONTRACT No. :

EQUIPMENT LIST - Crystallization Client:

GSI

M/s Gulf Stabilizer Industries Ltd. QTY

EQPT. TAG SR. NO. NO.

Locat ion

MOC

CAPACITY

SIZE

CONDITIONS

DIA x HT. (m)

OPERATING PRESSURE (bar)

EMPTY WEIGHT

Exisiting / New

EL-001 EL-001

REMARKS

DESCRIPTION

1 2 3 4 5 6

TR4201 MA4201 PC4202 PC4201 TR4202 MA4202

Crystallizer TR4201 Agitator Crystallizer discharge Crystallizer refrigerant circulation Crystallized product surge drum TR4202 Agitator

1 1 1 1 1 1

FF FF GF GF SF SF

SS304L SS304L SS304L CS SS304L SS304L

7

ET4210

MeOH Chiller

1

SF

SS304L

8 9

PK4201 TS4201

Liquid Ring Vacuum Pump

1 1

TF

SS304L SS304L

Acetic Acid Shot tank

26.6 m3

φ 2500 x 4600

25m3/hr, 40m 45 m3/hr, 16m 34.7 m3

φ 2800 x 4700

19.95 m2 0.4 m3

φ 450 x 2500 φ 615 x 1000

DESIGN PRESSURE (bar)

OPERATING TEMP. (ºC)

-10 / 150

6 -

Shell 4 Tube FV to atm.

3 Shell 6 Tube FV to 6 FV to 3

DESIGN TEMP. (ºC)

-

Shell (-10) to 2 Tube 70

-10 / 150 Shell 90 Tube 90 150

Installed

Kg

15 15 5.5 9

-

-

-

N

-

N E

15 -

E E E E E E

4, 45 deg Pitched blades Double mechanical Seal, centrifug

6, 45 deg Pitched blades

DOC No. : CAD No. : REV No. : PLANT : CONTRACT No. :

EQUIPMENT LIST - Centrifuging, Drying and solid handling Client:

M/s Gulf Stabilizer Industries Ltd.

GSI

QTY SR. NO.

EQPT. TAG NO.

Locat ion

MOC

CAPACITY

SIZE

CONDITIONS

DIA x HT. (m)

OPERATING PRESSURE (bar)

EMPTY WEIGHT

Exisiting / New

EL-001 EL-001

REMARKS

DESCRIPTION

1 2

CF4301 ET4301

Crystallised product centrifuge CF4301 Washing solvent cooler

1 1

SF TF

3

ET4302

CF4301 Washing solvent heater

1

TF

4 5 6 7 8

TP4401 TP4402 SC4401 BH4401 DA4401

DA4401 Charge 1 st lock vessel DA4401 Charge 2nd lock vessel DA4401 Twin screw feeder DA4401 Jet pulse filter Anox 20 dryer

1 1 1 1 1

9

EC4401

DA4401 vapor condenser

10 11 12 13 14 15

EP4401 PC4401 EP4402 PC4402 EP4403 PC4403

16

SS304L SS304L Shell - CS Tube - SS304L

602 kg/cycle 6.9 m2

3.14 m2 φ200 x 3660

2.2 m2

φ200 x 1830

FF FF FF FF FF

SS304L SS304L SS304L SS304L SS304L

2 m3 2 m3

1

TF

SS304L

Dryer jacket 1 st zone water heater DA4401 Jacket 1 st zone water circulation Dryer jacket 2 nd zone water heater DA4401 Jacket 2 nd zone water circultion Dryer jacket 3 rd zone water heater DA4401 Jacket 3 rd zone water circulation

1 1 1 1 1 1

FF FF FF FF FF FF

SS304L CS SS304L CS SS304L CS

PK4401

TP4401 and TP4403 Vacuum system

1

TF

SS304L

17

PK4402

TP4402 and DA4401 Vacuum system

1

TF

18 19

TP4403 TP4404

DA4401 Discharge lock vessel Dryer jacket warm water expansion drum

1 1

20 21 22 23 24 25 26 27 28 29 30 31 32

TS4501 RV4501 SS4501 GH4501 TS4502 SP4502 PK4502 TS4503 RV4503 PK4501 BH4502 BH4503 BF4502

Dried product hopper TS4501 Discharge Rotary valve Dryed product screen SS4501 Oversize mill Pneum. conveying feed hopper Pneumatic conveying transporter ANOX 20 pneumatic conveying package Anox 20 storage silo TS4503 Feeding Rotary valve Anox 20 Packaging Unit De-dusting baghouse TS4503 Dust filter BH4502 Blower

1 1 1 1 1 1 1 1 1 1 1 1 1

DESIGN PRESSURE (bar)

6 Shell - 6 bar & FV Tube - 6 bar

OPERATING TEMP. (ºC)

DESIGN TEMP. (ºC) 150 Shell - 200 Tube - 150

Installed

Kg

-

E E

TEMA Class - BEM

-

E

TEMA Class - BEU

11 kw 11 kw

150

75

E E E E E

150

-

N

200/150

2.2 2.2 2.2

E E E E E E

264 m3/hr, 230 mmhg

15

E

SS304L

59 m3/hr, 225 mm hg

5.5

E

GF TF

SS304L CS

0.4 m3 1.2 m3

4 kw -

E E

GF GF GF GF GF GF GF SF SF GF TF TF TF

SS304L SS304L SS304L SS304L SS304L SS304L SS304L SS304L SS304L SS304L

0.4 m3 520 kg/hr 520 kg/hr 100 kg/hr 0.2 m3

-

E E E E E E E E E E E E E

SS304L

2.5 m2 9.7m2

φ300 x 2440

3/FV Shell - 3 bar & FV Tube - 6 bar 6 6

200/150

20 m3/hr, 17m 20 m3/hr, 17m 6

200/150

20 m3/hr, 17m

520 kg/hr 28 m3 3000 kg/hr 4-6 big bags /hr

3000 Nm3/hr

φ935 x 1500

3

150

φ900 x 1075

3/-0.02 0.07

150 40

1 m2 sieve area

φ2400 x 7700

0.14 / -0.02

40/70 150

TEMA Class - BEM Magnetic drive centrifugal Magnetic drive centrifugal Magnetic drive centrifugal Liquid Ring Type Double Mechanical Seal. Flush Seal Liquid Ring Type Double Mechanical Seal. Flush Seal

Hammer mill with screen wire mes

Anox 20 Anox 20

OC No. : D No. : V No. : LANT : CONTRACT No. :

EQUIPMENT LIST - Solvent Recovery Client:

GSI

M/s Gulf Stabilizer Industries Ltd. QTY

SR. NO.

EQPT. TAG NO.

LOCA TION

MOC

CAPACITY

SIZE

CONDITIONS

DIA x HT. (m)

OPERATING PRESSURE (bar)

1 1 1 1

GF GF FF GF

SS304L SS304L SS304L SS304L

33.5 m3 3m3/hr, 26.3m 9.7 m3 10 m3/hr, 18.6m

φ2800 x 4500

ER4610

TP4604 Reboiler

1

FF

SS304L

23.88 m2

φ600 x 2500

CP4610

Water / Methanol distillation column

1 GF,FF,SF

PC4610A/B

5 6

TP4601 PC4601 TP4604

Exisiting / New

REMARKS

DESCRIPTION

Mother Liquor collector Mother liquor to distillation Mother Liquor distillation unit TP4604 Bottom circulation

1 2 3 4

EMPTY WEIGHT

φ1850 x 3000 -

DESIGN PRESSURE (bar)

OPERATING TEMP. (ºC)

3

DESIGN TEMP. Installed (ºC) 150

Kg

2.2 2.2

-

E E E N

-

-

N

Magnetic drive centrifugal

Shell - 4 Tube - atm.

3 Shell - 10 Tube - 3.5

Shell - 240 Tube - 120

150 Shell - 260 Tube - 160

Tube - 6 Shell - FV to 3.5

Tube 10 to 18 Shell - 65

Tube 0 to 60 Shell - 260

-

-

N

TEMA Class - BEM

-

φ680 x 8750

N

Magnetic drive centrifugal TEMA Class - BEM Pall ring 1'' packing

7

EC4610A

CP4610 Overhead Primary condenser

1

SF

316SS

63.84m2

φ700 x 2500

Tube - 4 Shell - atm.

8

EC4610B

CP4610 Overhead Secondary condenser

1

SF

316SS

63.84m2

φ700 x 2500

Tube - 4 Shell - atm.

Tube - 6 Shell - FV to 3.5

Tube 10 to 18 Shell - 65

Tube 0 to 60 Shell - 260

-

-

N

TEMA Class - BEM

9

ER4611

CP4610 Reboiler

1

GF

316SS

9.58 m2

φ300 x 2500

Shell - 4 Tube - atm.

Shell - 240 Tube - 120

-

N

TEMA Class - BEM

TP4603

1 1 1 1 1 1

FF GF GF GF GF GF

SS304L SS304L SS304L SS304L SS304L SS304L

1.5 m3 15 m3/hr, 29 m 33.5 m3 14.7 m3 15 m3/hr, 29 m 25 m3/hr, 55 m

φ1000 x 1500

Shell - 260 Tube - 160 150

-

10 11 12 13 14 15

Shell - 10 Tube - 3.5 3

PC4611

TP4602 TP4105 PC4612

PC4603A

EL-001 EL-001

CP4601 Reflux accumulator CP4601 Reflux pump DISTILLED SOLVENT COLLECTOR CP4601 Bottom accumulator CP4601 Bottom pump Solvent recycle pump

3 6

φ2800 x 4500 φ2000 x 4000 -

-

-

150 150 -

-

3.7 3.7 7.5

E N E E N E

Magnetic Drive, centrifugal

Magnetic Drive, centrifugal Magnetic drive

LIBRA TECHCON LIMITED DOCUMENT CLIENT PROJECT PROJECT No.

: : : :

Line List M/S Gulf Stabilizers Industries Basic Engineering Package LTL/876

DOC NO. DEPARTMENT REVISION DATE

Size in 10 3/4" 2 4 4 3 2 3 2 3 2 2 2 0.75 0.75 8 1 2 2 2 2 2 0.75 0.75 8 3 3 2 2 1 1 2 3 2 0.75 0.75 2 3 2 0.75 0.75 2 1.5 1.5 2 1.5 8 2 2 0.75 1 1

Service

Line Number

MOC

Insulation

SHEET NO.

P UA P P P P P P BD BD BD BD BD CD CD P P P P P P BD CD CD P P P P P P P BD BD BD CD CD BD BD BD CD CD P P P P P P P P CD P P

P3153 S1242 P3153 P3153 P3153 P3153 P3153 P3153 P1261  P1261  P1261  P1261  P1261  P1261  P1261  P3153 P3153 P3153 P3153 P3153 P3153 P1261  P1261  P1261  P3153 P3153 P3153 P3153 P3153 P3153 P3153 P1261  P1261  P1261  P1261  P1261  P1261  P1261  P1261  P1261  P1261  P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P1261  P3153 P3153

H/J N N H/J H/J H/J N N P P P P P P P I/H S S S S S P P P I/P S S N N N N P P P P P P P P P P N N N N N I/P N N P N N

PD‐40‐001 PD‐40‐01 PD‐40‐006 PD‐40‐002 PD‐40‐002 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐003 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐001 PD‐40‐001

0.75 8 2 0.75

CD P BD CD

410001 770001 410002 410003 410005 410004 410006 410007 410008 410009 410010 410011 410012 410013 410014 410015 410016 410017 410042 410043 410044 410018 410019 410020 410045 410046 410047 410048 410049 410050 410051 410021 410022 410023 410024 410025 410026 410027 410028 410029 410030 410031 410032 410062 410033 410052 410053 410054 410055 410034 410035 410036 410037 410038 410039 410040 410041

P1261  P3153 P1261  P1261 

P I/C P P

PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014

: : : :

LTL/876‐ LL ‐001 PROCESS R0 17/10/2017

Tentative Length m 10

Inch Dia

10 5 20 5 10 10 10 10 10 10 10 10 10 10 8 10 5 5 5 10 10 10 8 15 2 10 15 7 5 10 10 10 10 10 10 10 10 10 10 8 8 8 8 8 5 8 10 10 10 8

20 20 80 15 20 30 20 30 20 20 20 7.5 7.5 80 8 20 10 10 10 20 7.5 7.5 64 45 6 20 30 7 5 20 30 20 7.5 7.5 20 30 20 7.5 7.5 16 12 12 16 12 40 16 20 7.5 10 8

10 10 10 10

7.5 80 20 7.5

100

Deleted

Deleted Deleted

Deleted

Deleted Deleted

Deleted Deleted Deleted

2 2 3 3 3 1 1/2 1" 3/4" 1" 1" 1.5" 1" 1.5" 8" 1.5" 1" 1" 1" 3'' 3 3 1 12 2 3 1 8 1 1 0.75 2 2 2 1 1 3/4'' 3/4'' 1" 1" 2" 2 3 2 2 1 0.75 6 6 1 6 1 3 1 1 1 2 4 2.5 2.5 2 2 2 1 2 2 4 1

P P P P P P BD1 SW P UN P BD1 P P P BD1 BD1 BD1 BD P P P P P P P P P P CD BD P BD P BD1 P UA P P BD BD P P P P CD P P P P P P P P BD BD P P P P P P P P P P P

410056 410057 410058 410059 410060 410061 410063 410064 410065 410066 410067 410068 410069 410070 410071 410072 410073 410074 410075 420001 420002 420003 420004 420005 420006 420007 420008 420009 420010 420011 420012 420013 420014 420015 420016 420017 770001 420018 420019 420020 460001 460002 460003 460004 460005 460006 460007 460008 460009 460010 460011 460012 460013 460014 460015 460016 460017 460018 460019 460020 460021 460022 460023 460024 460025 460026 460027

P3153 P3153 P3153 P3153 P3153 P3153 P1261 P1261 P3153 S1242 P3153 P1261  P3153 P3153 P3153 P1261 P1261 P1261 P1261 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P1261  P1261  P3153 P1261  P3153 P1261 P3153 S1242 P3153 P3153 P1261 P1261  P3153 P3153 P3153 P3153 P1261  P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P1261  P1261  P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153 P3153

N N N N N N P P S N N P I/P S N P P P P N N N N I/C N I/C N I/C N P P I/C P N P N N S S P P I/H I/H I/H S P I/H I/H I/H I/P I/P I/P I/P I/P P P N N N N N N N I/H I/H I/H N

PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐001 PD‐40‐01 PD‐40‐01 PD‐40‐01 PD‐40‐03 PD‐40‐03 PD‐40‐03 PD‐40‐03 PD‐40‐03 PD‐40‐05 PD‐40‐05 PD‐40‐05 PD‐40‐05 PD‐40‐01 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐06 PD‐40‐06 PD‐40‐06 PD‐40‐06 PD‐40‐06 PD‐40‐06 PD‐40‐06 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012

10 10 10 10 15

20 20 30 30 45 0

10 10 10 12 5 5 7 12 10 10 10 10 7 10

30 30 10 144 10 15 7 96 10 10 7.5 20 14 20

10 15 5 3 15 10 10 15 15 10 10 10 6 8 10 10 15 8 20 25 10 25 25 7 5 5 8

20 45 10 6 15 7.5 60 90 15 60 10 30 6 8 10 20 60 20 50 50 20 50 25 14 10 20 8

Deleted Deleted

Deleted Deleted Deleted Deleted

Deleted

Deleted

1 1 0.75 2 0.75 6 3 4 3 3 1 1 1 1 1 1 1 1 1 1 1 1 3/4" 3/4" 3 3 2 2 2 2 3 3 4 4 4 1 4 4 4 4 1 1 1 1 3 3 3 3 1.5 1.5 3 3 2 2 2 2 2 2 2 2 3 3 2 2 2 2 4

P P CD P CD P P P BD BD WW UN UN UN UN UN UN UN UN UN UN UN UN UN CHR CHS CHR CHS CHR CHS CHS CHR RL RL RL RL RL RL RL RL RL RL RL RL RLS RLR RL RL RLR RLS RL RL RLS RLR RL RL RLR RLS RL RL RLS RLR RL RL RLR RLS RLR

460028 460029 460030 460031 460032 460033 460034 460035 460036 460037 460038 780001 780004 780002 780003 780005 780006 780007 780008 780009 780010 780011 780012 780013 730001 730002 730003 730004 730005 730006 730007 730008 730009 730010 730011 730012 730013 730014 730015 730016 730047 730048 730049 730050 730017 730018 730019 730020 730021 730022 730023 730024 730025 730026 730027 730028 730029 730030 730031 730032 730033 730034 730035 730036 730037 730038 730039

P3153 P3153 S1261 P3153 P3153 P3153 P3153 P3153 P1261 P1261 P1353 S1242 P3153 S1242 P3153 P3153 S1242 P3153 S1242 P3153 S1242 S1242 P3153 P3153 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140 S1140

N N P I/H P I/P I/P I/C P P N N N N N N N N N N N N N N I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C I/C

PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐012 PD‐40‐001 PD‐40‐001 PD‐40‐006 PD‐40‐006 PD‐40‐0012 PD‐40‐001 PD‐40‐0012 PD‐40‐001 PD‐40‐0012 PD‐40‐001 PD‐40‐01 PD‐40‐06 PD‐40‐06 PD‐40‐003 PD‐40‐003 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐014 PD‐40‐014 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐005 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006 PD‐40‐006

5 25 10 3 10

5 25 7.5 6 7.5

Deleted

Deleted Deleted

Deleted Deleted

Deleted Deleted

Deleted Deleted

Deleted Deleted Deleted Deleted Deleted Deleted

Deleted Deleted Deleted Deleted

4 5 5 3 3 5 5 4 4 3 2 2 4 4 4 4 2 4 3/4'' 4 3/4'' 2 2 4 4 3 3 2 4 4 2 4 4 4 4 2 3/4'' 4 1 4 1 4 1 2 1 R1 R0 Rev

RLR CHR CHS CHR CHS CHR CHS HOS HOR HOR HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO HO LS LC LS LC LS LC LS LC

730040 730041 730042 730043 730044 730045 730046 760001 760002 760024 760003 760004 760005 760006 760007 760008 760009 760010 760011 760012 760025 760026 760027 760013 760014 760015 760016 760017 760018 760019 760020 760021 760022 760023 760028 760029 760030 750001 750002 750003 750004 750005 750006 750007 750008 Issued for approval Issued for approval Description

S1140 S1140 S1140 S1140 S1140 S1140 S1140 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1261  P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 P1223 SA10 SA10 SA10 SA10 SA10 SA10 SA10 SA10

I/C I/C I/C I/C I/C I/C I/C I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/H I/P I/H I/P I/H I/P I/H I/H

PD‐40‐006 PD‐40‐012 PD‐40‐012 PD‐40‐014 PD‐40‐014 PD‐40‐012 PD‐40‐012 PD‐40‐002 PD‐40‐002 PD‐40‐002 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐003 PD‐40‐011 PD‐40‐011 PD‐40‐012 PD‐40‐012 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐014 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐004 PD‐40‐005 PD‐40‐005 PD‐40‐06 PD‐40‐06

4/12/2017 17/10/2017 Date

VG VG Prepared

Deleted Deleted

VG VG Chkd

MSB MSB Apvd

INSTRUMENT INDEX NOTES 1, 2, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13,

HOLDS 1, 2, 3, 4, 5,

REFERENCE DOCUMENTS 1, P&ID

CONSULTANT: 805/806. Hallmark Business Plaza, Guru Nanak, Hospital Road, Bandra (East), Mumbai - 400 051, India

LIBRA TECHCON LIMITED CLIENT: GULF ANTIOXIDANTS PLANT

P0

FOR REVIEW & APPROVAL

SR/MB

VG

MSB

REV

DESCRIPTION

PREPARED BY

CHECKED BY

APPROVED BY

3rd PARTY APPROVED

EM OR DM APPROVED

PROJECT:

ANOX20

05.12.2017

LOCATION:

AL-JUBAIL, KINGDOM OF SAUDHI ARABIA

SHEET:

1 OF 2

DATE

DOCUMENT NO.:

LTL/857-II-03-001

REV:

P0

SR. NO.

TAG NO.

EQUIPMENT

SERVICE

1

TI410026

TEMPERATURE AT 10"‐P‐410001‐P3153‐H/J

2

PCV410001

3

PSV410015

4

PCV410002

PRESSURE CONTROL VALVE AT 1"‐UN‐780004‐P3153‐N

5

HV410003

ON-OFF VALVE AT THE INLET OF TP4114

6 7 8 9

PT410001 LI410001 PI410001 TI410001

PROCESS MEDIUM

METHANOL

PRESSURE CONTROL VALVE AT 1"‐BD1‐41XXX‐P1261‐P TP4114

PRESSURE SAFETY VALVE AT TP4114

TP4114 TP4114 TP4114

PRESSURE AT 10"-P-410001-P3153-H/J LEVEL AT TANK TP4114 PRESSURE AT TANK TP4114 TEMPERATURE AT TANK TP4114

TP4114

WEIGH SCALE FOR TP4114

LiOMe METHANOL & PP base vapours LiOMe LiOMe LiOMe

10

HV410004

11

WT410002

12

HV410043

ON-OFF VALVE AT THE OUTLET OF TS4101

13

HV410041

ON-OFF VALVE AT THE INLET OF TR4101

METHANOL

ON-OFF VALVE AT THE OUTLET OF TP4114

LiOMe LiOMe PENTAERYTHRITOL

14

HV410045

ON-OFF VALVE AT 4"-HO-41004-P1223-I/H

HOT OIL

15

HV410044

ON-OFF VALVE AT 4"-HO-41003-P1223-I/H

HOT OIL

16

FT410006

FLOW AT HOT OIL SUPPLY

HOT OIL

17

HV410006

ON-OFF VALVE AT THE INLET OF TR4102

CRUDE

18 19 20

PSH410001 PSE410001 TSV410001 PI410002

TR4101 TR4101

HIGH PRESSURE AT TR4101 RUPTURE DISC AT TR4101 TEMPERATURE SAFETY VALVE PRESSURE AT 4"‐P‐410005‐P3153‐H/J

HOT OIL CRUDE

PCV410003

PRESSURE CONTROL VALVE AT 1 1/2"‐P‐410067‐P3153‐N

NITROGEN

PT410002

PRESSURE AT 1"‐BD1‐410068‐P1261‐P

NITROGEN

PCV410004

PRESSURE CONTROL VALVE AT 1 1/2"‐P‐410067‐P3153‐N

NITROGEN

PCV410005

PRESSURE CONTROL VALVE AT 1"‐UN‐780007‐P3153‐N

NITROGEN

HV410038 WT410001

ON-OFF VALVE AT THE INLET OF TS4110 TS4110

WEIGH SCALE FOR TS4110

NITROGEN DRY ANOX20

HV410039

ON-OFF VALVE AT THE OUTLET OF TS4110

DRY ANOX20

HV410011

ON-OFF VALVE AT THE INLET OF TR4102

DRY ANOX20

PSE410002 TSV410002 TSV410003 TI410005

RUPTURE DISC AT TR4102 TEMPERATURE SAFETY VALVE TEMPERATURE SAFETY VALVE TEMPERATURE AT 3"‐CH‐730001‐S1140‐I/C

HOT OIL CHILLED BRINE CHILLED BRINE

HV410046

ON-OFF VALVE AT 4"-HO-760007-P1223-I/H

HOT OIL

HV410047

ON-OFF VALVE AT 4"-HO-760008-P1223-I/H

HOT OIL

TV410007

TEMPERATURE CONTROL VALVE AT 2"-HO-760004-P1223-I/H

PI410003

PRESSURE AT DISCHARGE OF PC4111

HOT OIL

HV410048

HOT OIL

INSTRUMENT TYPE

TEMPERATURE INDICATOR DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE SAFETY VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE TRANSMITTER LEVEL INDICATOR PRESSURE INDICATOR TEMPERATURE INDICATOR PNEUMATICALLY OPERATED ON/OFF VALVE WEIGHT TRANSMITTER PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE FLOW TRANSMITTER PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE SWITCH RUPTURE DISC TEMPERATURE SAFETY VALVE PRESSURE INDICATOR DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE TRANSMITTER DIAPHRAGM ACTUATOR CONTROL VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PNEUMATICALLY OPERATED ON/OFF VALVE WEIGHT TRANSMITTER PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE RUPTURE DISC TEMPERATURE SAFETY VALVE TEMPERATURE SAFETY VALVE TEMPERATURE INDICATOR PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE INDICATOR PNEUMATICALLY OPERATED ON/OFF VALVE

ON-OFF VALVE AT THE OUTLET OF TR4102

CRUDE

TEMPERATURE AT TR4102

CRUDE

TEMPERATURE TRANSMITTER

TE410007/TT410007

TEMPERATURE AT DISCHARGE OF PC4111

HOT OIL

TEMPERATURE TRANSMITTER

HV410008

ON-OFF VALVE AT 3"-P-410004-P3153-H/J

CRUDE

HV410009

ON-OFF VALVE AT 3"-P-41014-P3153-S

CRUDE

TE410006/TT410006

TR4102

HV410010

ON-OFF VALVE AT 3"-P-410007-P3153-N

CRUDE

TSV410019

TEMPERATURE SAFETY VALVE

HOT OIL

HV410012

ON-OFF VALVE AT 2"-P-410006-P3153-N

HV410049

ON-OFF VALVE AT 3"-P-41044-P3153-N

FT410007 PI410004 PI410005 PI410006 TI410008

FLOW AT 3"-P-41044-P3153-N PRESSURE AT DISCHARGE OF PC4113 PRESSURE AT THE INLET OF PC4113 PRESSURE AT 4"‐RL‐730014‐S1140‐I/C TEMPERATURE AT EC4112

EC4112

HV410015

ON-OFF VALVE AT 2"-P-410042-P3153-S

HV410051

ON-OFF VALVE AT 1"-UN-780009-P3153-N

PSV410006 LT410002 TI410009 PI410007

TP4112 TP4112 TP4112

PRESSURE SAFETY VALVE AT TP4112 LEVEL AT TP4112 TEMPERATURE AT TP4112 PRESSURE AT 1"‐RL‐730047‐S1140‐I/C

METHANOL CRUDE CRUDE CRUDE CRUDE TEMPERED WATER TEMPERED WATER PP BASE NITROGEN PP BASE PP BASE TEMPERED WATER

PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE TEMPERATURE SAFETY VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE FLOW TRANSMITTER PRESSURE INDICATOR PRESSURE INDICATOR PRESSURE INDICATOR TEMPERATURE INDICATOR PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE SAFETY VALVE LEVEL TRANSMITTER TEMPERATURE INDICATOR PRESSURE INDICATOR

SHORT FORM

INPUT TYPE

TI

NA

TEMPERATURE INDICATION CONTROL VALVE

FUNCTION

ACCESSORIES

P & ID NO.

LINE NO.

PD-40-001

10"-P-410001-P3153-H/J

POSITIONER

PD-40-001

1"-BD1-41063-P1261-P

POSITIONER

PD-40-001

1"-UN-780004-P3153-N

PCV 

AO

PSV

NA

SAFETY VALVE

PCV 

AO

CONTROL VALVE

XV

DO

ON-OFF VALVE

PD-40-001

1"-UN-780004-P3153-N

PT LI PI TI

AI NA NA NA

PRESSURE MEASUREMENT LEVEL INDICATION PRESSURE INDICATION TEMPERATURE INDICATION

PD-40-001 PD-40-001 PD-40-001 PD-40-001

10"-P-410001-P3153-H/J

XV

DO

ON-OFF VALVE

PD-40-001

1"-P-410035-P3153-N

PD-40-001

WT

AI

WEIGHT MEASUREMENT

PD-40-001

XV

DO

ON-OFF VALVE

PD-40-001

10"-P-41005-P3153-I/H

XV

DO

ON-OFF VALVE

PD-40-001

1 1/2"-P-410061-P3153-N

XV

DO

ON-OFF VALVE

PD-40-001

4"-HO-41004-P1223-I/H

XV

DO

ON-OFF VALVE

PD-40-001

4"-HO-41003-P1223-I/H

FT

AI

FLOW MEASUREMENT

PD-40-001

4"-HOS-760001-P1223-I/H

XV

DO

ON-OFF VALVE

PD-40-001

4"-P-41037-P3153-H/J

PSH PSE TSV PI

DI DI NA NA

PRESSURE SWITCH SAFETY SAFETY VALVE PRESSURE INDICATION

PD-40-001 PD-40-001 PD-40-002 PD-40-002

3"-HOR-760002-P1223-I/H 4"-P-410005-P3153-H/J

PCV 

AO

CONTROL VALVE

PT

AI

PRESSURE MEASUREMENT

POSITIONER

PD-40-003

1 1/2"-P-410067-P3153-N

PD-40-003

1"-BD1-410068-P1261-P

PCV 

AO

CONTROL VALVE

POSITIONER

PD-40-003

1 1/2"-P-410067-P3153-N

PCV 

AO

CONTROL VALVE

POSITIONER

PD-40-003

1"-UN-780007-P3153-N

XV

DO

ON-OFF VALVE

PD-40-003

1"-UN-780007-P3153-N

WT

AI

WEIGHT MEASUREMENT

PD-40-003

XV

DO

ON-OFF VALVE

PD-40-003

XV

DO

ON-OFF VALVE

PD-40-003

PSE TSV TSV TI

DI NA NA NA

SAFETY SAFETY VALVE SAFETY VALVE TEMPERATURE INDICATION

PD-40-003 PD-40-003 PD-40-003 PD-40-003

2"-BD-47008-P1261-P 2"-HO-760003-P1223-I/H 3"-CH-730001-S1140-I/C 3"-CH-730001-S1140-I/C

XV

DO

ON-OFF VALVE

PD-40-003

4"-HO-760007-P1223-I/H

XV

DO

ON-OFF VALVE

PD-40-003

4"-HO-760008-P1223-I/H

TV

AO

CONTROL VALVE

PI

NA

PRESSURE INDICATION

XV

DO

TT

AI

POSITIONER

PD-40-003

2"-HO-760004-P1223-I/H

PD-40-003

4"-HO-760012-P1223-I/H

ON-OFF VALVE

PD-40-003

8"-P-410070-P3153-S

TEMPERATURE MEASUREMENT

PD-40-003

TT

AI

TEMPERATURE MEASUREMENT

PD-40-003

XV

DO

ON-OFF VALVE

PD-40-003

4"-HO-760012-P1223-I/H 3"-P-410004-P3153-H/J

XV

DO

ON-OFF VALVE

PD-40-003

3"-P-41014-P3153-S 3"-P-410007-P3153-N

XV

DO

ON-OFF VALVE

PD-40-003

TSV

NA

SAFETY VALVE

PD-40-003

2"-BD-410012-P1261-P

XV

DO

ON-OFF VALVE

PD-40-003

2"-P-410006-P3153-N

XV

DO

ON-OFF VALVE

PD-40-003

3"-P-41044-P3153-S

FT PI PI PI TI

AI NA NA NA NA

FLOW MEASUREMENT PRESSURE INDICATION PRESSURE INDICATION PRESSURE INDICATION TEMPERATURE INDICATION

PD-40-003 PD-40-003 PD-40-003 PD-40-004 PD-40-004

3"-P-41044-P3153-S 3"-P-41044-P3153-S 3"-P-41044-P3153-S 4"-RL-730014-S1140-I/C

XV

DO

ON-OFF VALVE

PD-40-004

2"-P-410042-P3153-S

XV

DO

ON-OFF VALVE

PD-40-004

1"-UN-780009-P3153-N

PSV LT TI PI

NA AI NA NA

SAFETY VALVE LEVEL MEASUREMENT TEMPERATURE INDICATION PRESSURE INDICATION

PD-40-004 PD-40-004 PD-40-004 PD-40-004

1"-RL-730047-S1140-I/C

COMMENT

TSV410005

TEMPERATURE SAFETY VALVE

HV410016

ON-OFF VALVE AT 3"-P-410017-P3153-S

TEMPERED WATER PP BASE

HV410017

ON-OFF VALVE AT 2"-P-410044-P3153-S

TE410010/TT410010

TEMPERATURE AT 4"‐RL‐730014‐S1140‐I/C

PP BASE

TSV410008

TEMPERATURE SAFETY VALVE

LOW PRESSURE STEAM

FV410004

FLOW CONTROL VALVE AT 2"‐LS‐750003‐SA10‐I/H

LOW PRESSURE STEAM

PI410008 TSV410007

PRESSURE AT 2"‐LS‐750003‐SA10‐I/H TEMPERATURE SAFETY VALVE

LOW PRESSURE STEAM REFRIGERENT LIQUID

TEMPERED WATER

TV410011

TEMPERATURE CONTROL VALVE AT 1"-RL-730009-S1140-I/C

PI410009 PI410010

PRESSURE AT DISCHARGE OF PC4112 PRESSURE AT INLET OF PC4112

HV410023

ON-OFF VALVE AT 3''-P-410047-P3153-S

METHANOL

HV410024

ON-OFF VALVE AT 2''-P-410049-P3153-N

METHANOL

TI410014 PI410011 TSV410010

TEMPERATURE AT 3''-RL-730017-S1140-I/C PRESSURE AT EC4111 TEMPERATURE SAFETY VALVE

EC4111

HV410042

ON-OFF VALVE AT 1''-UN-780007-P3153-N

PCV410006

PRESSURE CONTROL VALVE AT

HV410035

REFRIGERENT LIQUID TEMPERED WATER TEMPERED WATER

REFRIGERENT LIQUID REFRIGERENT LIQUID REFRIGERENT LIQUID NITROGEN METHANOL VAPOUR

ON-OFF VALVE AT 8''-P-410053-P3153-I/P

METHANOL VAPOUR

PT410003

PRESSURE AT 8''-P-410053-P3153-I/P

METHANOL VAPOUR

HV410053

ON-OFF VALVE AT 2''P-410048-P3153-N

METHANOL

PSV410011 PT410004

PRESSURE SAFETY VALVE PRESSURE AT 1''-BD1-410072-P1261-P

METHANOL VAPOUR METHANOL VAPOUR

PCV410007

PRESSURE CONTROL VALVE AT 1 1/2''-P-410071-P3153-N

TI410020 TSV410013 PT410023

TEMPERATURE AT 2''-RL-730025-S1140-I/C TEMPERATURE SAFETY VALVE PRESSURE AT 1''-BD-410074-P1261-P

PCV410008

PRESSURE CONTROL VALVE 1''-BD1-410074-P1261 -P

PT410022

PRESSURE AT 1''-BD1-410073-P1261 -P

PCV410009 PSV410014 LT410004 PI410012 LSXHH410002 TI410022 LSXHH410001 LT410003 TSV410012

TP4110 TP4110 TP4110 TP4111 TP4111

HV410052

NITROGEN REFRIGERENT LIQUID REFRIGERENT LIQUID REFRIGERENT LIQUID

PRESSURE CONTROL VALVE 1''-BD1-410073-P1261 -P

NITROGEN

PRESSURE SAFETY VALVE AT 3''-BD-410027-P-1261-P LEVEL AT TP4110 PRESSURE AT 2"-RL-730025-S1140-I/C HIGH LEVEL AT TP4110 TEMPERATURE AT TP4110 HIGH LEVEL AT TP4111 LEVEL AT TP4111 TEMPERATURE SAFETY VALVE

METHANOL VAPOUR METHANOL METHANOL METHANOL METHANOL METHANOL METHANOL REFRIGERENT LIQUID

ON-OFF VALVE AT 2''P-410031-P3153-N

METHANOL

PI410013 PI410014

PRESSURE AT THE DISCHARGE OF PC4105 PRESSURE AT THE DISCHARGE OF PC4106

METHANOL METHANOL

PCV420001

PRESSURE CONTROL VALVE AT 3/4''-P-420017-P3153-N

PCV420002

PRESSURE CONTROL VALVE AT 3/4''-UN-780013-S1242-N

FI420002

FLOW AT 3/4''-UN-780013-S1242-N

HV420001

ON-OFF VALVE AT 3''-P-420002P-3153-N

FT420001 PT420002 WT420005 WV420004

FLOW AT 3''-P-420002P-3153-N PRESSURE AT 3''-P-420002P-3153-N WEIGH SCALE FOR TS4201 WEIGHT CONTROL VALVE AT THE BOTTOM OF TS4201

TS4201 TS4201

HV420003

ON-OFF VALVE AT 2''-P-410002-S3153-N

HV420002

ON-OFF VALVE AT 1''-UN-780003-P3153-N

PT420001 PCV420003 TI420002 TSV420003

PRESSURE AT 1''-UN-780003-P3153-N PRESSURE CONTROL VALVE AT 1''-UN-780002-S1242-N TEMPERATURE AT 3''-RL-730034-S1140-I/C TEMPERATURE SAFETY VALVE

PCV420004 TI420001 LT420001 TSV420004 TV420003

PRESSURE CONTROL VALVE AT 8''-P-420008-P3153-N TR4201

NITROGEN METHANOL METHANOL METHANOL ACETIC ACID ACETIC ACID WATER NITROGEN NITROGEN NITROGEN REFRIGERENT LIQUID REFRIGERENT LIQUID METHANOL VAPOUR

TEMPERATURE AT 12''-P-420004-P3153-N LEVEL AT TR4201 TEMPERATURE SAFETY VALVE

METHANOL VAPOUR METHANOL / CRUDE REFRIGERENT LIQUID

TEMPERATURE CONTROL VALVE AT 4''-RL-730040-S1140-I/C

REFRIGERENT LIQUID

TV420006

TEMPERATURE CONTROL VALVE AT 2''-LS-75XXX-SA10-I/H

LOW PRESSURE STEAM

PSV420002

PRESSURE SAFETY VALVE

LOW PRESSURE STEAM

TEMPERATURE SAFETY VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE

TSV

NA

SAFETY VALVE

PD-40-004

1"-RL-730047-S1140-I/C

XV

DO

ON-OFF VALVE

PD-40-004

3"-P-410017-P3153-S

XV

DO

ON-OFF VALVE

PD-40-004

2"-P-410044-P3153-S

TEMPERATURE TRANSMITTER

TT

AI

TEMPERATURE MEASUREMENT

PD-40-004

4"-RL-730014-S1140-I/C

TSV

NA

SAFETY VALVE

PD-40-004

FV

AO

CONTROL VALVE

PI TSV

NA NA

PRESSURE INDICATION SAFETY VALVE

TV

AO

CONTROL VALVE

PD-40-004

1"-RL-730009-S1140-I/C

PI PI

NA NA

PRESSURE INDICATION PRESSURE INDICATION

PD-40-004 PD-40-004

4"-RL-730013-S1140-I/C 1"-RL-730012-S1140-I/C

XV

DO

ON-OFF VALVE

PD-40-005

3''-P-410047-P3153-S

XV

DO

ON-OFF VALVE

PD-40-005

3''-P-410047-P3153-N

TI PI TSV

NA NA NA

TEMPERATURE INDICATION PRESSURE INDICATION TEMPERATURE SAFETY VALVE

PD-40-005 PD-40-005 PD-40-005

3''-RL-730017-S1140-I/C 3"-RL-730017-S1140-I/C 1''-UN-780007-P3153-N

TEMPERATURE SAFETY VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE INDICATOR TEMPERATURE SAFETY VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE INDICATOR PRESSURE INDICATOR PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE TEMPERATURE INDICATOR PRESSURE INDICATOR TEMPERATURE SAFETY VALVE PNEUMATICALLY OPERATED ON/OFF VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE TRANSMITTER PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE SAFETY VALVE PRESSURE TRANSMITTER DIAPHRAGM ACTUATOR CONTROL VALVE TEMPERATURE INDICATOR TEMPERATURE SAFETY VALVE PRESSURE TRANSMITTER DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE TRANSMITTER DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE SAFETY VALVE LEVEL TRANSMITTER PRESSURE INDICATOR LEVEL SWITCH TEMPERATURE INDICATOR LEVEL SWITCH LEVEL TRANSMITTER TEMPERATURE SAFETY VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE INDICATION PRESSURE INDICATION DIAPHRAGM ACTUATOR CONTROL VALVE DIAPHRAGM ACTUATOR CONTROL VALVE ROTAMETER PNEUMATICALLY OPERATED ON/OFF VALVE FLOW TRANSMITTER PRESSURE TRANSMITTER WEIGHT TRANSMITTER WEIGHT CONTROL VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE TRANSMITTER PRESSURE CONTROL VALVE TEMPERATURE INDICATOR TEMPERATURE SAFETY VALVE DIAPHRAGM ACTUATOR CONTROL VALVE TEMPERATURE INDICATOR LEVEL TRANSMITTER TEMPERATURE SAFETY VALVE DIAPHRAGM ACTUATOR CONTROL VALVE DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE SAFETY VALVE

POSITIONER

POSITIONER

2"-LS-750003-SA10-I/H

PD-40-004

2"-LS-750003-SA10-I/H

PD-40-004 PD-40-004

2"-LS-750003-SA10-I/H 1"-RL-730009-S1140-I/C

XV

DO

ON-OFF VALVE

PD-40-005

PCV

AO

CONTROL VALVE

PD-40-005

XV

DO

ON-OFF VALVE

PD-40-005

8''-P-410053-P3153-I/P

PT

AI

PRESSURE MEASUREMENT

PD-40-005

8''-P-410053-P3153-I/P

XV

DO

ON-OFF VALVE

PD-40-005

2''P-410048-P3153-N

PSV PT

NA AI

PRESSURE SAFETY VALVE PRESSURE MEASUREMENT

PD-40-005 PD-40-005

3''-BD-410022-P-1261-P 1''-BD1-410072-P1261-P

PCV

AO

CONTROL VALVE

PD-40-005

1 1/2''-P-410071-P3153-N

TI TSV PT

NA NA AI

TEMPERATURE INDICATION TEMPERATURE SAFETY VALVE PRESSURE MEASUREMENT

PD-40-005 PD-40-005 PD-40-005

2''-RL-730025-S1140-I/C 2''-RL-730026-S1140-I/C 1''-BD-410074-P1261-P

PCV

AO

CONTROL VALVE

PT

AI

PRESSURE MEASUREMENT

PCV

AO

CONTROL VALVE

PSV LT PI LS TI LS LT TSV

NA AI NA DI NA DI AI NA

PRESSURE SAFETY VALVE LEVEL MEASUREMENT PRESSURE INDICATOR INDICATION TEMPERATURE INDICATION INDICATION LEVEL MEASUREMENT TEMPERATURE SAFETY VALVE

PD-40-005 PD-40-005 PD-40-005 PD-40-005 PD-40-005 PD-40-005 PD-40-005 PD-40-005

XV

DO

ON-OFF VALVE

PD-40-005

2''P-410031-P3153-N

POSITIONER

POSITIONER

POSITIONER

PD-40-005

1''-BD1-410074-P1261 -P

PD-40-005

1''-BD1-410073-P1261 -P

PD-40-005

1''-BD1-410073-P1261 -P 3''-BD-410027-P-1261-P 2"-RL-730025-S1140-I/C

2''-BD-410023-P1261-P

PI PI

NA NA

PRESSURE INDICATION PRESSURE INDICATION

PD-40-005 PD-40-005

1.5''-P-410032-P3153-N 1.5''-P-410052-P3153-N

PCV

AO

CONTROL VALVE

POSITIONER

PD-40-006

3/4''-P-420017-P3153-N

PCV

AO

CONTROL VALVE

POSITIONER

PD-40-006

3/4''-UN-780013-S1242-N

FI

NA

ROTAMETER

PD-40-006

3/4''-UN-780013-S1242-N

XV

DO

ON-OFF VALVE

PD-40-006

3''-P-420002P-3153-N

FT PT WT WV

AI AI AI AO

FLOW MEASUREMENT PRESSURE MEASUREMENT WEIGHT INDICATION CONTROL VALVE

PD-40-006 PD-40-006 PD-40-006 PD-40-006

3''-P-420002P-3153-N 3''-P-420002P-3153-N

XV

DO

ON-OFF VALVE

PD-40-006

2''-P-410002-S3153-N

XV

DO

ON-OFF VALVE

PD-40-006

1''-UN-780003-P3153-N

PT PCV TI TSV

AI AO NA NA

PRESSURE MEASUREMENT PRESSURE CONTROL VALVE TEMPERATURE INDICATION TEMPERATURE SAFETY VALVE

PD-40-006 PD-40-006 PD-40-006 PD-40-006

1''-UN-780003-P3153-N 1''-UN-780002-S1242-N 3''-RL-730034-S1140-I/C 3''-RL-730034-S1140-I/C

PCV

AO

CONTROL VALVE

PD-40-006

8''-P-420008-P3153-N

TI LT TSV

NA AI NA

TEMPERATURE INDICATION LEVEL TRANSMITTER TEMPERATURE SAFETY VALVE

PD-40-006 PD-40-006 PD-40-006

12''-P-420004-P3153-N

TV

AO

CONTROL VALVE

PD-40-006

4''-RL-730040-S1140-I/C

TV

AO

CONTROL VALVE

PD-40-006

2''-LS-750007-SA10-I/H

PSV

NA

PRESSURE SAFETY VALVE

PD-40-006

2''-LS-750007-SA10-I/H

4''-RL-730039-S1140-I/C

TW420004/TT420 004 TW420003/TT420 003 TI460001 TSV460001 PI460001

REFRIGERENT LIQUID

TEMPERATURE TRANSMITTER

TT

AI

TEMPERATURE MEASUREMENT

PD-40-006

TR4201

TEMPERATURE AT TR4201

TEMPERATURE AT 4''-RL-42002-S1140-I/C

METHANOL / CRUDE

TEMPERATURE TRANSMITTER

TT

AI

TEMPERATURE MEASUREMENT

PD-40-006

TP 4604

TEMPERATURE AT TP 4604 TEMPERATURE SAFETY VALVE PRESSURE AT 4"-HOR-760013-P1223-I/H

METHANOL / WATER HOT OIL HOT OIL

TI TSV PI

NA NA NA

TEMPERATURE INDICATION TEMPERATURE SAFETY VALVE PRESSURE INDICATION

PD-40-011 PD-40-011 PD-40-011

TV

AO

CONTROL VALVE

PI FT

NA AI

PRESSURE INDICATION FLOW MEASUREMENT DIFFERENTIAL PRESSURE MEASUREMENT PRESSURE SAFETY VALVE TEMPERATURE INDICATION PRESSURE MEASUREMENT TEMPERATURE SAFETY VALVE TEMPERATURE INDICATOR TEMPERATURE INDICATOR TEMPERATURE INDICATOR TEMPERATURE INDICATOR TEMPERATURE INDICATOR LEVEL INDICATOR LEVEL TRANSMITTER TEMPERATURE INDICATOR PRESSURE INDICATION TEMPERATURE SAFETY VALVE

DPT460001

CP4610

DIFFERENTIAL PRESSURE AT CP4610

WATER / METHANOL

PSV460004 TI460002 PT460001 TSV460002 TI460004 TI460005 TI460006 TI460007 TI460008 LG460001 LT460001 TI460009 PI460003 TSV460004

CP4610

PRESSURE SAFETY VALVE TEMPERATURE AT 6''-P-460010-P3153-I/P PRESSURE AT CP4610 TEMPERATURE SAFETY VALVE TEMPETATURE AT CP4610 TEMPETATURE AT CP4610 TEMPETATURE AT CP4610 TEMPETATURE AT CP4610 TEMPETATURE AT CP4610 LEVEL AT CP4610 LEVEL AT CP4610 TEMPERATURE AT 4''-P-460026-P3153-I/H PRESSURE AT 1 1/2"-P-46020-P3153-S TEMPERATURE SAFETY VALVE

WATER / METHANOL WATER / METHANOL WATER / METHANOL CHILLED WATER WATER / METHANOL WATER / METHANOL WATER / METHANOL WATER / METHANOL WATER / METHANOL WATER / METHANOL WATER / METHANOL WATER / METHANOL HOT OIL HOT OIL

HV460004

ON-OFF VALVE AT 1''-P-460009-P3153-I/H

WATER / METHANOL

PI460005

PRESSURE AT THE DISCHARGE OF PC4612

WATER / METHANOL

TEMPERATURE INDICATOR TEMPERATURE SAFETY VALVE PRESSURE INDICATOR DIAPHRAGM ACTUATOR CONTROL VALVE PRESSURE INDICATOR FLOW TRANSMITTER DIFFERENTIAL PRESSURE TRANSMITTER PRESSURE SAFETY VALVE TEMPERATURE INDICATOR PRESSURE TRANSMITTER TEMPERATURE SAFETY VALVE TEMPERATURE INDICATOR TEMPERATURE INDICATOR TEMPERATURE INDICATOR TEMPERATURE INDICATOR TEMPERATURE INDICATOR LEVEL INDICATOR LEVEL TRANSMITTER TEMPERATURE INDICATOR PRESSURE INDICATOR TEMPERATURE SAFETY VALVE PNEUMATICALLY OPERATED ON/OFF VALVE PRESSURE INDICATOR

TT460012

TEMPERATURE AT THE OUTLET OF EC4610B

WATER / METHANOL

TEMPERATURE TRANSMITTER

PCV460001

PRESSURE CONTROL VALVE AT 1"‐UN‐780005‐P3153‐N

NITROGEN

PCV460002

PRESSURE CONTROL VALVE AT 1"‐P‐460011‐P3153‐I/P

WATER / METHANOL

TEMPERATURE SAFETY VALVE PRESSURE SAFETY VALVE AT TP4603 TEMPERATURE AT 2.5"‐P‐460019‐P3153‐N

CHILLED BRINE WATER / METHANOL WATER / METHANOL

TV460001

TEMPERATURE CONTROL VALVE AT 4"-HOR-760013-P1223-I/H

PI460002 FT460002

PRESSURE AT THE DISCHARGE OF PC4610A/B FLOW AT 6''-P-460006-P3153-I/H

TARS METHANOL / WATER

TSV460005 PSV460003 TI460003

CP4610 CP4610 CP4610 CP4610 CP4610 CP4610 CP4610 CP4610

TP4603

HOT OIL

FV460004

FLOW CONTROL VALVE AT 2.5"‐P‐460019‐P3153‐N

WATER / METHANOL

FT460004 PI460004

FLOW AT 2.5"‐P‐460019‐P3153‐N PRESSURE AT 2.5"‐P‐460018‐P3153‐N

WATER / METHANOL WATER / METHANOL

DIAPHRAGM ACTUATOR CONTROL VALVE DIAPHRAGM ACTUATOR CONTROL VALVE TEMPERATURE SAFETY VALVE PRESSURE SAFETY VALVE TEMPERATURE INDICATOR DIAPHRAGM ACTUATOR CONTROL VALVE FLOW TRANSMITTER  PRESSURE INDICATOR

POSITIONER

4''-RL-42002-S1140-I/C

2''-BD-460001-P1261-P 4"-HOR-760013-P1223-I/H

PD-40-011

4''-HOR-760013-P1223-I/H

PD-40-011 PD-40-012

2''-P-460004-P3153-I/H 6''-P-460006-P3153-I/H

DPT

AI

PSV TI PT TSV TI TI TI TI TI LI LT TI PI TSV

NA NA AI NA NA NA NA NA NA NA AI NA NA NA

PD-40-012

XV

DO

ON-OFF VALVE

PD-40-012

1''-P-460009-P3153-I/H

PI

NA

PRESSURE INDICATION

PD-40-012

1''-P-460029-P3153-N

PD-40-0012

1"‐P‐460011‐P3153‐I/P

`

PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012 PD-40-012

6''-P-460010-P3153-I/P 8''-CHR-730041-S1140-I/C

4''-P-460026-P3153-I/H 1 1/2"-P-46020-P3153-S 3''-HOR-760015-P1223I/H

TI

NA

TEMPERATURE MEASUREMENT

PCV 

AO

CONTROL VALVE

POSITIONER

PD-40-012

1"-UN-780005-P3153-N

PCV 

AO

CONTROL VALVE

POSITIONER

PD-40-012

1"-P-460011-P3153-I/P

TSV PSV TI

NA NA NA

SAFETY VALVE SAFETY VALVE TEMPERATURE INDICATION

PD-40-012 PD-40-012 PD-40-012

2.5"‐P‐460019‐P3153‐N

FV

AO

CONTROL VALVE

PD-40-012

2.5"‐P‐460019‐P3153‐N

FT PI

AI NA

FLOW MEASUREMENT PRESSURE INDICATION

PD-40-012 PD-40-012

2.5"‐P‐460019‐P3153‐N 2.5"-P-460018-P3153-N

POSITIONER

3"-CHR-730045-S1140-I/C

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR ET4111

DOC NO.

:

LTL/876- PDS - E1

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 8/9/2017

Service of Unit

TR4102 circulation oil cooler

Size

ET4111

Tag No

Ø250 mm x 2440 mm Type

Shell & tube

Horizantal

Orientation:

7.4 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

SHELL SIDE

TUBE SIDE

:

HOT OIL (THERMINOL 55)

Chilled Water

:

25350

11560 -

vapor

Kg/hr

:

-

liquid

Kg/hr

:

25350

11560

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

25350

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

845

1000

:

6-7

1.08-1.31

0.1065

0.5163

cP

Viscosity

:

Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

:

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

1.5

1.5

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.50

1

64

56.5 3.55

4

92480

LMTD (corrected) Shell

CONSTRUCTION

18

10

46.25

°C Tube

Design pressure

Kg/cm2 g

:

10

6

Design temperature

°C

:

260

150

:

SA 106 Gr B

SA 179

MOC

1

:

No. of passes Nos

52

Shell

ID

250

Type of Support

Saddle Support

Insulation

Protective Insulation

Pitch

Square

Tubes

OD

Baffles:

19.05 mm

2 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service N1

Tube side inlet

Length : 2440 mm Pitch

SIZE, NB

Rating

80

150#

N2

Tube side outlet

80

150#

N3

Tube Side Drain

20

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

100

150#

25.4 mm

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

100

150#

Code requirements:

ASME Sec. VIII DIV. 1 - TEMA C Remarks

* - please check as per code NOTES: (1) THE HEAT EXCHANGER HAS TO PROVIDE THE COOLING OF TR4102 FROM 203 TO APPROX. 160°C, (HOT OIL INITIAL TEMP.220 °C)

R0 Rev

Issued for approval Description

8/9/2017 Date

VG Prepared

VG Chkd

MSB Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR EC4110

DOC NO.

:

LTL/876- PDS - E3

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 9/19/2017

Service of Unit

TR4101 Methanol Vapor condenser - Atmospheric Ø200 mm x 1500 mm Type

Size

EC4110

Tag No

Shell & tube

Horizantal

Orientation:

2.51 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

TUBE SIDE

SHELL SIDE

:

Methanol Vapours + air

Refrigrant liquid

:

40

2911.17 -

vapor

Kg/hr

:

40

liquid

Kg/hr

:

-

2911.17

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

5

-

Fluid vaporized or condensed Kg/hr

:

35

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

-

1120

:

0.5

0.89

:

32

-

:

0.5

0.5163

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

15

1.5

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.60

0.85

160

35 atm.

4

12372.47

LMTD (corrected) Tube

CONSTRUCTION

-15

-20

103.68

°C Shell

Design pressure

Kg/cm2 g

:

6

6

Design temperature

°C

:

260

(-20) to 60

:

SS316

SS316

MOC

1

:

No. of passes Nos

21

Shell

ID

200

Type of Support

Saddle Support

Insulation

Protective Insulation

Pitch

Square

Tubes

OD

Baffles:

25.4

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service N1

Tube side inlet

Length : 1500 mm Pitch

SIZE, NB

Rating

50

150#

N2

Tube side outlet

50

150#

N3

Tube Side Drain

25

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

50

150#

31.75 mm

25

N6

Shell Vent

25

150#

N7

Shell liquid Outlet

50

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R2

Issued for approval

4/12/2017

VG

VG

MSB

R1

Issued for approval

13/10/2017

VG

VG

MSB

R0

Issued for approval

8/9/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR EC4111

DOC NO.

:

LTL/876- PDS - E4

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 9/19/2017

Service of Unit

TR-4101Vaccum methanol condensation Ø450 mm x 2500 mm Type

Size

EC4111

Tag No Shell & tube

Vertical

Orientation:

22.94 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

TUBE SIDE

SHELL SIDE

:

Methanol +Air

Refrigrant liquid

:

528.42

43720.56 -

vapor

Kg/hr

:

528.42

liquid

Kg/hr

:

-

43720.56

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

5

-

Fluid vaporized or condensed Kg/hr

:

523.42

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

792

-

:

0.5

0.89

:

32

-

:

0.5

0.5163

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2

:

Velocity

M/s

:

15

1.5

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.60

0.85

160

35 FV

4 (gauge)

LMTD (corrected)

185812.4 Tube

CONSTRUCTION

-15

-20

103.68

°C Shell

Design pressure

Kg/cm2 g

:

FV to 6

6

Design temperature

°C

:

260

(-30) to 60

:

SS316

SS316

MOC

1

:

No. of passes Nos

115

Shell

ID

450

Type of Support

Saddle Support

Insulation

Protective Insulation

Pitch

Triangular

Tubes

OD

Baffles:

25.4

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service N1

Tube side inlet

Length : 2500 mm Pitch

SIZE, NB

Rating

200

150#

N2

Tube side outlet

50

150#

N3

Tube Side Vapour Outlet

200

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

80

150#

31.75 mm

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

80

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R2

Issued for approval

3/12/2017

VG

VG

MSB

R1

Issued for approval

13/10/2017

VG

VG

MSB

R0

Issued for approval

8/9/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR EC4112

DOC NO.

:

LTL/876- PDS - E5

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 9/19/2017

Service of Unit

PP base Vapor condenser - Vacuum

Size

EC4112

Tag No

Ø450 mm x 2500 mm Type

Shell & tube

Vertical

Orientation:

19.55 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

TUBE SIDE

SHELL SIDE

:

PP base Vapours

Tempered Water

:

1408

46772.1 -

vapor

Kg/hr

:

1408

liquid

Kg/hr

:

-

46772.1

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

1408

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

-

1120

:

-

1.08-1.31

:

-

-

:

0.5

0.5163

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2

:

Velocity

M/s

:

15

1.5

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.30

0.85

203

90 FV

4 (gauge)

198781.425

LMTD (corrected) Tube

CONSTRUCTION

85

80

43.76

°C Shell

Design pressure

Kg/cm2 g

:

FV to 6

6

Design temperature

°C

:

260

105

:

SS316

SS316

MOC

1

:

No. of passes Nos

98

Shell

ID

450

Type of Support

Saddle Support

Insulation

Protective Insulation

Pitch

Square

Tubes

OD

Baffles:

25.4

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service N1

Tube side inlet

Length : 2500 mm Pitch

SIZE, NB

Rating

250

150#

N2

Tube side outlet

80

150#

N3

Tube Side vapour Outlet

200

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

100

150#

31.75 mm

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

100

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R2

Issued for approval

3/12/2017

VG

VG

MSB

R1

Issued for approval

13/10/2017

VG

VG

MSB

R0

Issued for approval

8/9/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR ET4112

DOC NO.

:

LTL/876- PDS - E6

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 8/9/2017

Service of Unit

Tempered Water heater

Size

ET4112

Tag No

1.5m x 0.48m x 1.58m Type

plate

13.65 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

HOT SIDE

COLD SIDE

:

Steam

Refrigrant liquid

:

510.76

3342.30 -

vapor

Kg/hr

:

510.76

liquid

Kg/hr

:

-

3342.30

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

-

-

Steam condensed

Kg/hr

:

510.76

-

Density

Kg/m3

:

2.92

1120

:

0.214

0.89

:

18

-

:

0.6

0.6

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

20

1.5

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.000307

Heat exchanged

Kcal/hr

:

0.56

0.85

155

155

80

-10

4.5

4

255685.95

LMTD (corrected)

120.61

°C

HOT SIDE

CONSTRUCTION

COLD SIDE

Design pressure

Kg/cm2 g

:

6*

6*

Design temperature

°C

:

170

170

:

CS

CS

MOC

Plates

18

Nos

Shell

length

Type of Support

Saddle Support

Insulation

-

Pitch

-

1

1

:

No. of passes

0.48m

width

BWG

-

height : 1.58m

Pitch

% Cut

-

1.5m Baffles:

-

Nozzle and Manways Service

SIZE, NB

Rating

N1

Cold side inlet

100

150#

N2

Cold side outlet

100

150#

N3

Cold Side Drain

25

150#

N4

Cold Side Vent

25

150#

N5

Hot Side Inlet

50

150#

-

N6

Hot Side Vent

25

150#

N7

Hot Side Outlet

25

150#

TEMA Class B

Code requirements: Remarks * - please check as per code

R2

Issued for approval

3/12/2017

VG

VG

MSB

R1

Issued for approval

13/10/17

VG

VG

MSB

R0

Issued for approval

8/9/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR ET4210

DOC NO.

:

LTL/876- PDS - E7

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 13/10/2017

Service of Unit

TR4201 methanol chiller

Size

ET4210

Tag No

Ø450 mm x 2500 mm Type

Shell & tube

Horizantal

Orientation

19.95 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

TUBE SIDE

SHELL SIDE

:

Methanol

Refrigerant Liquid

:

362.400

24681.25 -

vapor

Kg/hr

:

362.400

liquid

Kg/hr

:

-

24681.25

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

5

-

Fluid vaporized or condensed Kg/hr

:

357.400

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

792

1120

:

0.5

0.89

:

32

-

:

0.5163

0.5

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

15

1

Fouling resistance

m2-hr-°C/Kcal

:

0.0002

0.000205

Heat exchanged

Kcal/hr

:

0.46

0.85

15

10 FV to atm

104895.3125

4

LMTD (corrected) Tube

CONSTRUCTION

-15

-20

32.40

°C Shell

Design pressure

Kg/cm2 g

:

FV to 6

6

Design temperature

°C

:

100

-20

:

SS304L

SS304L

MOC

1

:

No. of passes Nos

100

Shell

ID

450

Type of Support

Saddle Support

Insulation

Cold Insulation

Pitch

Square

Tubes

OD

Baffles:

25.4

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service N1

Tube side inlet

Length : 2500 mm Pitch

SIZE, NB

Rating

300

150#

N2

Tube side outlet

50

150#

N3

Tube Side Drain

25

150#

N4

Tube Side Vent

200

150#

N5

Shell Inlet

80

150#

31.75mm

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

80

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R1

Issued for approval

3/12/2017

VG

VG

MSB

R0

Issued for approval

13/10/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR ER4610

DOC NO.

:

LTL/876- PDS - E8

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 13/10/2017

Service of Unit

TP4604 Vessel reboiler

Size

ER4610

Tag No

Ø600 mm x 2500 mm Type

Shell & tube

Vertical

Orientation

23.88 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

SHELL SIDE

TUBE SIDE

:

Hot Oil

Tars

:

79746.28

1666.20 -

vapor

Kg/hr

:

-

liquid

Kg/hr

:

79746.28

1666.20

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

-

1506.5

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

842

-

:

0.5-5

-

:

-

-

:

0.5163

0.1065

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

1

1

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.64

0.6

240

220 4

atm.

506388.90

LMTD (corrected) Shell

CONSTRUCTION

100

10

124.90

°C Tube

Design pressure

Kg/cm2 g

:

10

3.5

Design temperature

°C

:

260

160

:

SS304L

SS304L

MOC

1

:

No. of passes Nos

78

Shell

ID

600

Type of Support

Saddle Support

Insulation

Hot Insulation

Pitch

Square

Tubes

OD

Baffles:

40mm

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service

Length : 2500 mm Pitch

SIZE, NB

Rating

N1

Tube side inlet

50

150#

N2

Tube side outlet

150

150#

N3

Tube Side Drain

25

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

100

150#

47.625 mm

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

100

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R1

Issued for approval

3/12/2017

VG

VG

MSB

R0

Issued for approval

13/10/17

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR ER4611

DOC NO.

:

LTL/876- PDS - E9

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 13/10/2017

Service of Unit

column reboiler

Size

ER4611

Tag No

Ø300 mm x 2500 mm Type

Shell & tube

Vertical

Orientation

9.58 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

TUBE SIDE

SHELL SIDE

:

process fluid

hot oil

:

677

34156.75 -

vapor

Kg/hr

:

-

liquid

Kg/hr

:

677

34156.75

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

579.1

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

-

842

:

-

-

:

-

-

:

0.5163

0.1065

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

1

1

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.60

0.635

35

87.5 Atm.

4

216895.3625

LMTD (corrected)

TUBE SIDE

CONSTRUCTION

220

240

162.66

°C

SHELL SIDE

Design pressure

Kg/cm2 g

:

FV to 3.5

10

Design temperature

°C

:

150

260

:

SS316

SS316

MOC

1

:

No. of passes Nos

48

Shell

ID

300

Type of Support

Saddle Support

Insulation

Protective Insulation

Pitch

Triangular

Tubes

OD

Baffles:

25.4mm

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service

Length : 2500 mm Pitch

SIZE, NB

Rating

N1

Tube side inlet

50

150#

N2

Tube side outlet

100

150#

N3

Tube Side Drain

25

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

80

150#

31.75mm

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

80

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R1

Issued for approval

3/12/2017

VG

VG

MSB

R0

Issued for approval

13/10/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR EC4610A/B

DOC NO.

:

LTL/876- PDS - E10

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 13/10/2017

Service of Unit

Distillation Column Primary and secondary condenser Ø700 mm x 2500 mm Type

Size

EC4610A/B

Tag No

Shell & tube

Horizantal

Orientation

63.84 m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

TUBE SIDE

SHELL SIDE

:

Chilled liquid

methanol+water

:

45662.90

2735.5 2735.5

vapor

Kg/hr

:

-

liquid

Kg/hr

:

45662.90

-

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

-

2735.5

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

1000

796.16

:

0.89

0.5 - 5

:

-

-

:

0.5163

0.5

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

1.5

20

Fouling resistance

m2-hr-°C/Kcal

:

0.0002

0.000205

Heat exchanged

Kcal/hr

:

1.00

0.608

10

18 4

atm

365303.2

LMTD (corrected)

CONSTRUCTION

35

65

34.48

°C

Tube

Shell

Design pressure

Kg/cm2 g

:

6

FV to 3.5

Design temperature

°C

:

0 to 60

260

:

SS316

SS316

MOC

1

:

No. of passes Nos

320

Shell

ID

700 mm

Type of Support

Saddle Support

Insulation

Protective Insulation

Pitch

Triangular

Tubes

OD

Baffles:

25.4 mm

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service

Length : 2500 mm Pitch

SIZE, NB

Rating

N1

Tube side inlet

125

150#

N2

Tube side outlet

125

150#

N3

Tube Side Drain

25

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

150

150#

31.75mm

25

N6

Shell Vapour Vent

150

150#

N7

Shell liquid Outlet

80

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R0

Issued for approval

3/12/2017

VG

VG

MSB

R0

Issued for approval

13/10/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR ET4110

DOC NO.

:

LTL/876- PDS - E11

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

PROJECT PROJECT No.

: :

Basic Engineering Package LTL/876

REVISION DATE

: :

R0 13/10/2017

Service of Unit

TR4101 falling film evaporator Ø500mm x 2500 mm

Size

ET4110

Tag No Shell & tube

Type

Vertical

Orientation

36.7m2

Surf/Unit

PERFORMANCE OF ONE UNIT General

Fluid circulated Total fluid entering

Kg/hr

SHELL SIDE

TUBE SIDE

:

hot oil

reaction mass

:

22822.9

1408 -

vapor

Kg/hr

:

-

liquid

Kg/hr

:

22822.9

1408

steam

Kg/hr

:

-

-

non condensables

Kg/hr

:

-

-

Fluid vaporized or condensed Kg/hr

:

-

-

Steam condensed

Kg/hr

:

-

-

Density

Kg/m3

:

842

-

:

6-7

-

:

-

-

:

0.1065

0.5163

cP

Viscosity Molecular weight vapors Thermal conductivity

Kcal/hr-m-°C

Specific heat

Kcal/ Kg-°C

:

Temperature In/Out

°C

:

Operating Pressure

Kg/cm2 (g)

:

Velocity

M/s

:

1

1

Fouling resistance

m2-hr-°C/Kcal

:

0.000205

0.0002

Heat exchanged

Kcal/hr

:

0.64

0.6

240

220 4

FV

144925.415

LMTD (corrected)

CONSTRUCTION

203

90

21.60

°C

Shell

Tube

Design pressure

Kg/cm2 g

:

10

FV to 6

Design temperature

°C

:

260

260

:

SS316

SS316

MOC

1

:

No. of passes Nos

92

Shell

ID

500

Type of Support

Saddle Support

Insulation

Hot Insulation

Pitch

Square

Tubes

OD

Baffles:

50.4mm

1 BWG

12

Single Segmental

% Cut

Nozzle and Manways Service

Length : 2500 mm Pitch 63 mm

SIZE, NB

Rating

N1

Tube side inlet

100

150#

N2

Tube side outlet

250

150#

N3

Tube Side Drain

25

150#

N4

Tube Side Vent

25

150#

N5

Shell Inlet

100

150#

25

N6

Shell Vapour Vent

25

150#

N7

Shell liquid Outlet

100

150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

Code requirements: * - please check as per code

R1

Issued for approval

3/12/2017

VG

VG

MSB

R0

Issued for approval

13/10/2017

VG

VG

MSB

Rev

Description

Date

Prepared

Chkd

Apvd

LIBRA TECHCON LIMITED

DOCUMENT

:

PDS FOR EC4401 - new

DOC NO.

:

LTL/876- PDS - E12

CLIENT

:

M/S Gulf Stabilizers Industries

DEPARTMENT

:

PROCESS

REVISION DATE Tag No Orientation

: :

R0 4/12/2017

PROJECT PROJECT No. Service of Unit Size Surf/Unit

Basic Engineering Package : LTL/876 : DR4401 overhead condenser Ø400mm x 2500 mmType Shell & tube 17.16m2

EC4110 Horizantal

PERFORMANCE OF ONE UNIT General SHELL SIDE Fluid circulated

TUBE SIDE

:

MeOH vapours

Chilled water

Total fluid entering

Kg/hr

:

103.37

3648.73

vapor liquid

Kg/hr Kg/hr

: :

103.37 -

3648.73

steam

Kg/hr K /h

:

-

-

non condensables Fluid vaporized or condensed Steam condensed Density Viscosity Molecular weight vapors Thermal conductivity Specific heat Temperature In/Out Operating Pressure Velocity Fouling resistance Heat exchanged

Kg/hr Kg/hr Kg/hr Kg/m3 cP

: : : : : : : : : : : : :

103.37 1.5 0.1065 0.30

0.5163 1

CONSTRUCTION Design pressure Design temperature MOC No of passes No. Tubes Shell Type of Support Insulation Pitch

N1 N2 N3 N4 N5 N6 N7

Kcal/hr-m-°C Kcal/ Kg-°C °C Kg/cm2 (g) M/s m2-hr-°C/Kca Kcal/hr Kg/cm2 g °C

: : : : 86 OD Nos 400 ID Saddle Support Baffles: Hot Insulation Triangular Nozzle and Manways Service Tube side inlet Tube side outlet Tube Side Drain Tube Side Vent Shell Inlet Shell Vapour Vent Shell liquid Outlet

Code requirements:

33 8 33.8

30

18

10

FV 20 0.000205

4 1 0.0002

29189.84

LMTD (corrected) Shell FV to 6 260 SS304L 1

25.4mm

BWG

12

Single Segmental

SIZE, NB 50 50 25 25 150 25 25

°C

17.82

Tube FV to 6 260 SS304L 1 Length : 2500 mmPitch 31.75 % Cut

25

Rating 150# 150# 150# 150# 150# 150# 150#

ASME Sec. VIII DIV. 1 - TEMA C Remarks

p * - please check as p per code R0 Rev

Issued for approval Description

4/12/2017 Date

VG Prepared

VG Chkd

MSB Apvd

LIBRA TECHCON LTD.

MAGNETIC TYPE CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA TEMPERED WATER CIRCULATION

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PC4112

PAGE

HYDROCARBON

YES

NO

PUMPING TEMP.

NUMBER OF REQ'D

TOXIC

DATE

SPECIFIC GRAVITY AT P.T.

PERFORMANCE AT RATED 1.12

1.12

mm

CORROSIVE (IF ANY)

.

NEGLIGIBLE

NONE

SUC. PRESS.

COMPOUND

NOR.4.0

1.35 18.6 >7

DIFF. PRESS.

SOLIDS (IF ANY) ; NAME

DIFF. HEAD

CONTENT

%wt NPSH AVAILABLE

CORR. ALLOW.

1.6

mm

FLOW CONTROL

m

NO. OF STAGE

m3/h

5.35

CP DISCH. PRESS.

PROPOSAL CURVE NO. NPSH REQ'D

bara

RATED 30

CAPACITY

OPER.0.63 / MAX. 10

Kg/l

PARTICLE DIA. ℃ VAPOR PRESS. AT P.T.

VISCOSITY AT P.T.

ROTATING SPEED

rpm

bara

DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

SIZE

* *

SUCTION DISCHARGE

; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

ROTATION FROM CPLG. END □ CW

AUTO.

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

*

YES

NO

- STUFFING BOX ;

YES

IMPELLER DIA.

; RATED

TYPE ; BEARING TYPE ;

℃

- SEAL GLAND : mm

VENT YES

DRAIN

SHAFT INNER MAGNET

Kg/cm2G

GAUGE

MAIN BUSH

*

MAX./MIN.

FLOOD

RING OIL

FLINGER

MAGNETIC

mm REAR CASING OVERHUNG

□ GEAR

CONST. LEVEL OILER

SHOP TESTS

□ DRIVER MFR. BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

* MAGNETIC COUPLING TYPE ;

SEPARATLY COUPLED

CLOSE COUPLED

TEMP. DESIGN / OPER. / MIN. ;

/

/

PRESSURE DESIGN / OPER. ; MAGNETS TORQUE DESIGN / NOR. AT OPER. TEMP.

℃

□ DISMANTLE & INSP. AFTER TEST

kg/cm2G

□ OTHER

316 S.S

INNER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

OUTER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

BRACKET ;

CARBON

UTILITY DATA kg-m

/

CONTAINMENT SHELL ;

CARBON

□ WT. NPSH

SHOP INSPECTION

kg/cm2G

REAR CASING BURST PRESSURE ;

MAIN BUSHING ;

C.S

JACKET

*

MFR'S TYPE NO.

□ V-BELT

CASING GASKET BASE PLATE

PURE OIL MIST.

PUMP MFR.

OUTTER MAGNET THRUST RING

NO

MOUNT. ; □ BETWEEN BRGS

DRIVER HALF MTD. BY ; DIR

*

* * * * * * * *

IMPELLER

□ IN-LINE

HYDRO. TEST

C.S

CASING

THRUST

GREASE

;

API CLASS

END TOP

□ NEAR CENTERLINE

CONNECT ; NO

POSITION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

250

* *

; TYPE

DRIVER

R.F R.F

RADIAL

LUBE ; COUPLING

FACING

bar

□ CCW

MATERIALS

RATING

FOOT

m m3/h

m MIN. CONTINUOUS

MANUAL

ANSI 150 # ANSI 150 #

RADIAL □ BARREL

%

m MAX. HEAD RATED IMP.

CONSTRUCTION NOZZLES

1

ONE / 0 September 8, 2017

(MAIN / SPARE)

VG

BY

TRUE DENSITY

80

OF

REQ. NO.

OPERATION CONDITIONS EACH PUMP Refrigration Liquid

LIQUID NAME

1

SPEC./CODE NO.

HEATING FLUID TYPE :

ZIRCONIA

PRESS.(NOR./DES) :

barg ℃

TEMP.(NOR./DES) : COOLING FLUID :

SIC.

ℓ/hr

QT'Y PRESS. (OPER./DES) :

SHAFT ;

316 S.S

HASTELLOY C-276

O-RING ;

VITON

TEFLON

barg ℃

TEMP. (OPER./DES) :

KALREZ

NITROGEN : PRESS. (OPER./DES) :

barg ℃

TEMP. (OPER./DES) :

MOTOR DRIVER

*

RATED HP

SERVICE FACTOR

Kw

1.15 FRAME

*

MFR. TYPE

SPEED BEARINGS

SQIRREL-CAGE INDUCTION

INSUL.

EExe ⅡT4 / IP55 TEMP. RISE

ENC.

* *

rpm

PAINTING CL.Ⅰ,DIV.2,Gr.D

HAZARDOUS RATING

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

LUBE

F B

*

PRIMER : FINAL : □ INDOOR

LOCATION

FULL LOAD AMPS

*

LOCKED ROTOR AMPS

A APPROX. WT. PUMP & BASE

*

A MOTOR

*

Kg

OUTDOOR

* TOTAL

Kg

*

Kg

REMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2.

* PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE.

1 0 REVISION NO.

FOR APPROVAL FOR APPROVAL NOTES

VG

VG

MSB

21/9/2017

VG

VG

MSB

8/9/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LTD.

MAGNETIC TYPE CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA TR4102 JACKET HOT OIL CIRCULATION

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PC4111

PAGE

HYDROCARBON

YES

NO

PUMPING TEMP.

NUMBER OF REQ'D

TOXIC

DATE

SPECIFIC GRAVITY AT P.T.

PERFORMANCE AT RATED Kg/l

PARTICLE DIA.

mm

℃ VAPOR PRESS. AT P.T.

0.74

OPER.0.63 / MAX. 10

CORROSIVE (IF ANY)

.

NEGLIGIBLE

NONE

SUC. PRESS.

COMPOUND

NOR.4.0

1.35 18.6 >7

DIFF. PRESS.

SOLIDS (IF ANY) ; NAME

DIFF. HEAD

CONTENT

%wt NPSH AVAILABLE

CORR. ALLOW.

1.6

mm

FLOW CONTROL

m

NO. OF STAGE

m3/h

5.35

CP DISCH. PRESS.

PROPOSAL CURVE NO. NPSH REQ'D

bara

RATED 30

CAPACITY

VISCOSITY AT P.T.

ROTATING SPEED

rpm

bara

DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

SIZE

* *

SUCTION DISCHARGE

; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

ROTATION FROM CPLG. END □ CW

AUTO.

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

*

YES

NO

- STUFFING BOX ;

YES

IMPELLER DIA.

; RATED

TYPE ; BEARING TYPE ;

℃

- SEAL GLAND : mm

VENT YES

DRAIN

SHAFT INNER MAGNET

Kg/cm2G

GAUGE

MAIN BUSH

*

MAX./MIN.

FLOOD

RING OIL

FLINGER

MAGNETIC

mm REAR CASING OVERHUNG

□ GEAR

CONST. LEVEL OILER

SHOP TESTS

□ DRIVER MFR. BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

* MAGNETIC COUPLING TYPE ;

SEPARATLY COUPLED

CLOSE COUPLED

TEMP. DESIGN / OPER. / MIN. ;

/

/

PRESSURE DESIGN / OPER. ; MAGNETS TORQUE DESIGN / NOR. AT OPER. TEMP.

℃

□ DISMANTLE & INSP. AFTER TEST

kg/cm2G

□ OTHER

316 S.S

INNER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

OUTER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

BRACKET ;

CARBON

UTILITY DATA kg-m

/

CONTAINMENT SHELL ;

CARBON

□ WT. NPSH

SHOP INSPECTION

kg/cm2G

REAR CASING BURST PRESSURE ;

MAIN BUSHING ;

C.S

JACKET

*

MFR'S TYPE NO.

□ V-BELT

CASING GASKET BASE PLATE

PURE OIL MIST.

PUMP MFR.

OUTTER MAGNET THRUST RING

NO

MOUNT. ; □ BETWEEN BRGS

DRIVER HALF MTD. BY ; DIR

*

* * * * * * * *

IMPELLER

□ IN-LINE

HYDRO. TEST

C.S

CASING

THRUST

GREASE

;

API CLASS

END TOP

□ NEAR CENTERLINE

CONNECT ; NO

POSITION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

250

* *

; TYPE

DRIVER

R.F R.F

RADIAL

LUBE ; COUPLING

FACING

bar

□ CCW

MATERIALS

RATING

FOOT

m m3/h

m MIN. CONTINUOUS

MANUAL

ANSI 150 # ANSI 150 #

RADIAL □ BARREL

%

m MAX. HEAD RATED IMP.

CONSTRUCTION NOZZLES

1

ONE / 0 September 8, 2017

(MAIN / SPARE)

VG

BY

TRUE DENSITY

210

OF

REQ. NO.

OPERATION CONDITIONS EACH PUMP THRMINOL 55

LIQUID NAME

1

SPEC./CODE NO.

HEATING FLUID TYPE :

ZIRCONIA

PRESS.(NOR./DES) :

barg ℃

TEMP.(NOR./DES) : COOLING FLUID :

SIC.

ℓ/hr

QT'Y PRESS. (OPER./DES) :

SHAFT ;

316 S.S

HASTELLOY C-276

O-RING ;

VITON

TEFLON

barg ℃

TEMP. (OPER./DES) :

KALREZ

NITROGEN : PRESS. (OPER./DES) :

barg ℃

TEMP. (OPER./DES) :

MOTOR DRIVER

*

RATED HP

SERVICE FACTOR

Kw

1.15 FRAME

*

MFR. TYPE

SPEED BEARINGS

SQIRREL-CAGE INDUCTION

INSUL.

EExe ⅡT4 / IP55 TEMP. RISE

ENC.

* *

rpm

PAINTING CL.Ⅰ,DIV.2,Gr.D

HAZARDOUS RATING

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

LUBE

F B

*

PRIMER : FINAL : □ INDOOR

LOCATION

FULL LOAD AMPS

*

LOCKED ROTOR AMPS

A APPROX. WT. PUMP & BASE

*

A MOTOR

*

Kg

OUTDOOR

* TOTAL

Kg

*

Kg

REMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2.

* PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE.

0 REVISION NO.

FOR APPROVAL NOTES

VG

VG

MSB

8/9/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LTD.

CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA TR4101 Reaction Mass Recirculation Pump

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PAGE

PC4110

CRUDE ANOX 20(SLURRY)

HYDROCARBON

YES

PUMPING TEMP.

NO

TOXIC

NUMBER OF REQ'D

DATE

SPECIFIC GRAVITY AT P.T.

PERFORMANCE AT RATED

TRUE DENSITY

Kg/l

PARTICLE DIA. CAPACITY

OPER.0.63 / MAX. 10

CP DISCH. PRESS.

CORROSIVE (IF ANY)

.

NONE

COMPOUND

1.35 18.6

DIFF. HEAD

CONTENT CORR. ALLOW.

1.6

mm

FLOW CONTROL

ROTATING SPEED DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

MANUAL

rpm

bara

>7

%wt NPSH AVAILABLE

m

NO. OF STAGE

3 m /h

NOR.4.0

DIFF. PRESS.

NPSH REQ'D

bara

5.35

SUC. PRESS.

SOLIDS (IF ANY) ; NAME

PROPOSAL CURVE NO.

mm NEGLIGIBLE

RATED 30

0.74

VISCOSITY AT P.T.

%

m

MAX. HEAD RATED IMP.

m

MIN. CONTINUOUS

NOM. SIZE

* *

SUCTION DISCHARGE ; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

ROTATION FROM CPLG. END □ CW

AUTO.

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

YES

℃

mm

DRAIN

IMPELLER SHAFT

YES

CASEWEARING Kg/cm 2G

GAUGE

PACKING GLAND

*

MAX./MIN.

mm OVERHUNG

RING OIL

FLINGER

FLEXIBLE

JACKET

CONST. LEVEL OILER

*

SHOP TESTS

□ DRIVER MFR.

□ V-BELT

BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

SHAFT SEAL ASSEMBLY AT SHIPPING ; □ GP

NORMAL OPERATING ; □ GP

MS

GLAND PACKING SIZE

MATERIAL

MS

TYPE ; MATERIALS ;

□ BALANCED

□ UNBALANCED

API CODE

XSPFN

□ DISMANTLE & INSP. AFTER TEST

NO. OF RING

□ CARTRIDGE

□ OTHER

□ BELLOWS

UTILITY DATA

JOHN CRANE STATIONARY RING SIC.OR EQ. MFR.

CARBON

ROTATING RING

VITON

SHAFT PACKING

HEATING FLUID TYPE : PRESS.(NOR./DES) :

VITON

STATOR PACKING

□ SS

□ TUBING 3 m /h

TOTAL COOLING WATER REQ'D

7311

SEAL FLUSHPIPING PLAN

COOLING FLUID : □ PIPE

□ CS

SS

Kg/cm 2G

TUBING

□ CS

AUX. SEAL QUENCH FLUID

□ PIPE

3 m /h

QT'Y

AUXILIARY SEAL PLAN

PRESS. (OPER./DES.) :

3 m /h

EXTERNAL SEAL FLUSH FLUID

SS

TUBING

RESERVOIR BY

ℓ/hr

QT'Y

SIGHT F.l. REQ'D

PACKING COOLING INJECTION REQ'D TOTAL

*

SERVICE FACTOR

*

MFR.

Kw

SPEED

1.15 FRAME BEARINGS

SQUIRREL-CAGE INDUCTION INSUL.

TYPE

EExeⅡ T 4 / IP55 TEMP. RISE

ENC.

* *

rpm

NITROGEN : barg

PRESS. (OPRT./DES.) :

□ PIPE

PAINTING CL.I,DIV.2,Gr.D

F B

PRIMER : SEE ATTACHED PAINTING SPEC.

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

barg ℃

TEMP. (OPER./DES.) :

MFR.

HAZARDOUS RATING LUBE

barg ℃

TEMP. (OPER./DES.) :

MOTOR DRIVER RATED HP

barg ℃

TEMP.(NOR./DES) :

AUXILIARY PIPING □ CU

CW PIPE PLAN

□ WT. NPSH

SHOP INSPECTION

DOUBLE □ SINGLE □ DRY GAS □ PUMPING RING □ THROTTLE BUSHING

MECH. SEAL

TEFLON C.S

BASE PLATE

MFR'S TYPE NO.

PUMP MFR.

□ GEAR

DIR

PURE OIL MIST.

SEAL PLATE CASING GASKET

THRUST FLOOD

IMP. WEARING SHAFT SLEEVE

NO

MOUNT. ; □ BETWEEN BRGS

DRIVER HALF MTD. BY ; ;

*

C.S 316SS 316SS

CASING

□ IN-LINE

HYDRO. TEST VENT

- SEAL GLAND :

RADIAL GREASE

API CLASS

END TOP

□ NEAR CENTERLINE

250

NO

LOCATION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

CONNECT ;

; TYPE

DRIVER

R.F R.F

bar

* *

; RATED

LUBE ; COUPLING

*

YES

TYPE ; BEARING TYPE ;

FACING

NO

- STUFFING BOX ; IMPELLER DIA.

RATING

FOOT

□ CCW

MATERIALS

ANSI 150 # ANSI 150 # □ BARREL

RADIAL

m m3/h

CONSTRUCTION NOZZLES

1

ONE / 0 September 21, 2017

(MAIN / SPARE)

VG

BY

℃ VAPOR PRESS. AT P.T.

160 to 203

OF

REQ. NO.

OPERATION CONDITIONS EACH PUMP LIQUID NAME

1

SPEC./CODE NO.

FINAL : SEE ATTACHED PAINTING SPEC.

*

FULL LOAD AMPS LOCKED ROTOR AMPS

□ INDOOR

LOCATION

* *

A

APPROX. WT. PUMP & BASE

A

MOTOR

*

Kg

OUTDOOR

* TOTAL

Kg

*

Kg

EMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2. 3.

* PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE. * PUMP MANUFACTURE TO ADVISE THESE POINT AT QUOTATION STAGE.

4.

PUMP IMPELLER COUPLING TO BE DESIGNED TO AVOID BACKWARD ROTATION FROM HEAD OF LIQUID AT PUMP SHUT DOWN. THERE NO NON-RETURN VALVE FITTED TO THE PUMPS DISC. PIPEWORK.

1 0 REVISION NO.

FOR APPROVAL FOR APPROVAL NOTES

VG

MSB

MSB

21/11/2017

VG

MSB

MSB

21/09/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LTD.

MAGNETIC TYPE CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA TP4604 Bottom circulation

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PC4610A/B

PAGE

Tars YES

HYDROCARBON

NUMBER OF REQ'D

NO

TOXIC

DATE

PERFORMANCE AT RATED Kg/l

PARTICLE DIA.

OPER.0.63 / MAX. 10

CORROSIVE (IF ANY)

.

NEGLIGIBLE

NONE

NOR.4.0

SUC. PRESS.

COMPOUND

1.35 18.6 >7

DIFF. PRESS.

SOLIDS (IF ANY) ; NAME

DIFF. HEAD

CONTENT

%wt NPSH AVAILABLE 1.6

CORR. ALLOW.

FLOW CONTROL

mm

ROTATING SPEED

rpm

bara

DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

MANUAL

m

NO. OF STAGE

3 m /h

5.35

CP DISCH. PRESS.

NPSH REQ'D

bara

RATED 10

CAPACITY

VISCOSITY AT P.T.

PROPOSAL CURVE NO.

mm

℃ VAPOR PRESS. AT P.T.

0.74

SPECIFIC GRAVITY AT P.T.

%

m

MAX. HEAD RATED IMP.

m

MIN. CONTINUOUS

m m3/h

ROTATION FROM CPLG. END □ CW

AUTO.

CONSTRUCTION NOZZLES

SIZE

* *

SUCTION DISCHARGE

; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

YES

- STUFFING BOX ; IMPELLER DIA.

R.F R.F

℃

250 CONNECT ; - SEAL GLAND :

* *

GREASE

mm

*

HYDRO. TEST VENT

DRAIN

YES

IMPELLER SHAFT

Kg/cm 2G

GAUGE

RING OIL

FLINGER

MAIN BUSH

*

MAGNETIC

DRIVER HALF MTD. BY ; DIR

□ GEAR

PURE OIL MIST.

mm OVERHUNG

CASING GASKET

*

SHOP TESTS

BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

* MAGNETIC COUPLING SEPARATLY COUPLED

TYPE ;

C.S

JACKET

CONST. LEVEL OILER

□ DRIVER MFR.

□ V-BELT

REAR CASING BASE PLATE

MFR'S TYPE NO.

PUMP MFR.

OUTTER MAGNET THRUST RING

THRUST FLOOD

* * * * * *

INNER MAGNET

NO

MAX./MIN.

C.S SS316 SS316

CASING

□ IN-LINE

MOUNT. ; □ BETWEEN BRGS

; TYPE ;

API CLASS

END TOP

□ NEAR CENTERLINE

bar

NO

POSITION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

RADIAL

LUBE ;

DRIVER

FACING

NO

TYPE ;

COUPLING

*

YES

; RATED

BEARING TYPE ;

RATING

□ BARREL

CLOSE COUPLED

□ WT. NPSH

SHOP INSPECTION

℃

□ DISMANTLE & INSP. AFTER TEST

PRESSURE DESIGN / OPER. ;

2 kg/cm G

□ OTHER

REAR CASING BURST PRESSURE ;

kg/cm 2G

TEMP. DESIGN / OPER. / MIN. ;

/

/

MAGNETS TORQUE DESIGN / NOR. AT OPER. TEMP. 316 S.S

INNER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

OUTER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

CARBON

BRACKET ;

CARBON

UTILITY DATA kg-m

/

CONTAINMENT SHELL ;

MAIN BUSHING ;

□ CCW

MATERIALS

ANSI 150 # ANSI 150 # FOOT

RADIAL

1

ONE / ONE September 21, 2017

(MAIN / SPARE)

VG

BY

TRUE DENSITY

120

PUMPING TEMP.

OF

REQ. NO.

OPERATION CONDITIONS EACH PUMP LIQUID NAME

1

SPEC./CODE NO.

HEATING FLUID TYPE :

ZIRCONIA

PRESS.(NOR./DES) :

barg ℃

TEMP.(NOR./DES) : COOLING FLUID :

SIC.

ℓ/hr

QT'Y PRESS. (OPER./DES) :

SHAFT ;

316 S.S

HASTELLOY C-276

O-RING ;

VITON

TEFLON

barg ℃

TEMP. (OPER./DES) : KALREZ

NITROGEN : PRESS. (OPER./DES) :

barg ℃

TEMP. (OPER./DES) :

MOTOR DRIVER

*

RATED HP SERVICE FACTOR

Kw

1.15 FRAME

*

MFR. TYPE

SPEED BEARINGS

SQIRREL-CAGE INDUCTION

INSUL.

EExe ⅡT 4 / IP55 TEMP. RISE

ENC.

* *

rpm

PAINTING CL.Ⅰ,DIV.2,Gr.D

HAZARDOUS RATING

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

LUBE

F B

PRIMER : FINAL :

*

□ INDOOR

LOCATION

*

FULL LOAD AMPS LOCKED ROTOR AMPS

*

A

APPROX. WT. PUMP & BASE

A

MOTOR

*

Kg

OUTDOOR

* TOTAL

Kg

*

Kg

REMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2.

* PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE.

0 REVISION NO.

FOR APPROVAL NOTES

VG

VG

MSB

21/9/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LTD.

MAGNETIC TYPE CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA CP4601 REFLUX PUMP

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PC4611

PAGE

HYDROCARBON

YES

NO

PUMPING TEMP.

NUMBER OF REQ'D

TOXIC

DATE

PARTICLE DIA.

SPECIFIC GRAVITY AT P.T.

0.997

CAPACITY

0.92

CP DISCH. PRESS.

NONE

.

PERFORMANCE AT RATED Kg/l mm

℃ VAPOR PRESS. AT P.T.

VISCOSITY AT P.T. CORROSIVE (IF ANY) COMPOUND

0.03

NOR.1.34 / MAX. 1.59

3.09 31.4 >7

DIFF. PRESS. DIFF. HEAD

CONTENT

%wt NPSH AVAILABLE

CORR. ALLOW.

mm

FLOW CONTROL

m

NO. OF STAGE

m3/h

RATED 15

PROPOSAL CURVE NO. NPSH REQ'D

bara

4.43

SUC. PRESS.

SOLIDS (IF ANY) ; NAME

ROTATING SPEED

SIZE

* *

SUCTION DISCHARGE ; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

*

YES

NO

- STUFFING BOX ;

YES

IMPELLER DIA. TYPE ;

BEARING TYPE ;

ROTATION FROM CPLG. END □ CW

AUTO.

GREASE

FLOOD

RING OIL

YES

DRAIN

SHAFT INNER MAGNET

Kg/cm2G

GAUGE

MAIN BUSH

*

mm REAR CASING OVERHUNG

□ GEAR

CONST. LEVEL OILER

SHOP TESTS

□ DRIVER MFR. BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

* MAGNETIC COUPLING TYPE ;

SEPARATLY COUPLED

CLOSE COUPLED

TEMP. DESIGN / OPER. / MIN. ;

/

/

PRESSURE DESIGN / OPER. ;

℃

□ DISMANTLE & INSP. AFTER TEST

kg/cm2G

□ OTHER

316 S.S

INNER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

OUTER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

CARBON

BRACKET ;

CARBON

UTILITY DATA kg-m

/

CONTAINMENT SHELL ;

MAIN BUSHING ;

□ WT. NPSH

SHOP INSPECTION

kg/cm2G

REAR CASING BURST PRESSURE ; MAGNETS TORQUE DESIGN / NOR. AT OPER. TEMP.

C.S

JACKET

*

MFR'S TYPE NO.

□ V-BELT

CASING GASKET BASE PLATE

PURE OIL MIST.

PUMP MFR.

OUTTER MAGNET THRUST RING

NO

MAX./MIN.

FLINGER

MAGNETIC

DIR

VENT

SS316 SS316 * * * * * *

IMPELLER

THRUST

DRIVER HALF MTD. BY ; ;

*

HYDRO. TEST

CS

CASING

□ IN-LINE

MOUNT. ; □ BETWEEN BRGS

; TYPE

DRIVER

℃

- SEAL GLAND : mm

□ CCW

API CLASS

END TOP

□ NEAR CENTERLINE

CONNECT ; NO

POSITION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

RADIAL

LUBE ; COUPLING

R.F R.F

150

* *

; RATED

FACING

bar

m m3/h

m MIN. CONTINUOUS

MATERIALS

RATING

□ BARREL

%

m MAX. HEAD RATED IMP.

MANUAL

ANSI 150 # ANSI 150 # FOOT

RADIAL

rpm

bara

CONSTRUCTION NOZZLES

1

ONE / 0 21/09/2017

(MAIN / SPARE)

VG

BY

TRUE DENSITY

25

OF

REQ. NO.

OPERATION CONDITIONS EACH PUMP WATER & METHANOL

LIQUID NAME

1

SPEC./CODE NO.

HEATING FLUID TYPE :

ZIRCONIA

PRESS.(NOR./DES) :

barg ℃

TEMP.(NOR./DES) : COOLING FLUID :

SIC.

ℓ/hr

QT'Y PRESS. (OPER./DES) :

SHAFT ;

316 S.S

HASTELLOY C-276

O-RING ;

VITON

TEFLON

barg ℃

TEMP. (OPER./DES) : KALREZ

NITROGEN : PRESS. (OPER./DES) :

barg ℃

TEMP. (OPER./DES) :

MOTOR DRIVER

*

RATED HP

SERVICE FACTOR

Kw

SPEED

1.15 FRAME

MFR.

*

BEARINGS

TYPE

SQIRREL-CAGE INDUCTION

INSUL.

EExe ⅡT4 / IP55 TEMP. RISE

ENC.

* *

rpm

PAINTING CL.Ⅰ,DIV.2,Gr.D

HAZARDOUS RATING

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

LUBE

F B

*

FULL LOAD AMPS

PRIMER : SEE ATTACHED PAINTING SPEC. FINAL : SEE ATTACHED PAINTING SPEC. □ INDOOR

LOCATION

*

LOCKED ROTOR AMPS

A APPROX. WT. PUMP & BASE

*

A MOTOR

*

Kg

OUTDOOR

* TOTAL

Kg

*

Kg

REMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2.

** MINIMUM FLOW ASSURED BY SPILL BACK RO. VERIFY THE PURCHASED PUMP MIN.FLOW * PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE.

3.

0 REVISION NO.

FOR APPROVAL NOTES

VG

VG

MSB

21/09/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LTD.

MAGNETIC TYPE CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA CP4601 BOTTOM PUMP

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PC4612

HYDROCARBON

YES

NO

PUMPING TEMP.

NUMBER OF REQ'D

TOXIC

PARTICLE DIA.

SPECIFIC GRAVITY AT P.T.

0.997

CAPACITY

0.92

CP DISCH. PRESS.

NONE

.

mm

COMPOUND

0.03

DATE

NOR.1.34 / MAX. 1.59

3.09 31.4 >7

DIFF. PRESS. DIFF. HEAD

CONTENT

%wt NPSH AVAILABLE

CORR. ALLOW.

mm

FLOW CONTROL

m

NO. OF STAGE

m3/h

RATED 15

PROPOSAL CURVE NO. NPSH REQ'D

bara

4.43

SUC. PRESS.

SOLIDS (IF ANY) ; NAME

ROTATING SPEED

SIZE

* *

SUCTION DISCHARGE

; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

*

YES

NO

- STUFFING BOX ;

YES

IMPELLER DIA.

; RATED

TYPE ; BEARING TYPE ;

ROTATION FROM CPLG. END □ CW

AUTO.

℃

- SEAL GLAND : mm

FLOOD

RING OIL

DRAIN

YES

SHAFT INNER MAGNET

Kg/cm2G

GAUGE

MAIN BUSH

*

mm REAR CASING OVERHUNG

□ GEAR

CONST. LEVEL OILER

SHOP TESTS

□ DRIVER MFR. BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

* MAGNETIC COUPLING TYPE ;

SEPARATLY COUPLED

CLOSE COUPLED

TEMP. DESIGN / OPER. / MIN. ;

/

/

PRESSURE DESIGN / OPER. ;

℃

□ DISMANTLE & INSP. AFTER TEST

kg/cm2G

□ OTHER

316 S.S

INNER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

OUTER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

CARBON

BRACKET ;

CARBON

UTILITY DATA kg-m

/

CONTAINMENT SHELL ;

MAIN BUSHING ;

□ WT. NPSH

SHOP INSPECTION

kg/cm2G

REAR CASING BURST PRESSURE ; MAGNETS TORQUE DESIGN / NOR. AT OPER. TEMP.

C.S

JACKET

*

MFR'S TYPE NO.

□ V-BELT

CASING GASKET BASE PLATE

PURE OIL MIST.

PUMP MFR.

OUTTER MAGNET THRUST RING

NO

MAX./MIN.

FLINGER

MAGNETIC

DIR

VENT

MOUNT. ; □ BETWEEN BRGS

DRIVER HALF MTD. BY ; ;

*

SS316 SS316 * * * * * *

IMPELLER

□ IN-LINE

HYDRO. TEST

CS

CASING

THRUST

GREASE

□ CCW

API CLASS

END TOP

□ NEAR CENTERLINE

CONNECT ; NO

POSITION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

150

* *

; TYPE

DRIVER

R.F R.F

RADIAL

LUBE ; COUPLING

FACING

bar

m m3/h

m MIN. CONTINUOUS

MATERIALS

RATING

FOOT

%

m MAX. HEAD RATED IMP.

MANUAL

ANSI 150 # ANSI 150 #

RADIAL □ BARREL

rpm

bara

CONSTRUCTION NOZZLES

1

PERFORMANCE AT RATED Kg/l

℃ VAPOR PRESS. AT P.T.

VISCOSITY AT P.T. CORROSIVE (IF ANY)

OF

ONE / 0 21/09/2017

(MAIN / SPARE)

VG

BY

TRUE DENSITY

25

1

REQ. NO.

OPERATION CONDITIONS EACH PUMP WATER & METHANOL

LIQUID NAME

PAGE

SPEC./CODE NO.

HEATING FLUID TYPE :

ZIRCONIA

PRESS.(NOR./DES) :

barg ℃

TEMP.(NOR./DES) : COOLING FLUID :

SIC.

ℓ/hr

QT'Y PRESS. (OPER./DES) :

SHAFT ;

316 S.S

HASTELLOY C-276

O-RING ;

VITON

TEFLON

barg ℃

TEMP. (OPER./DES) :

KALREZ

NITROGEN : PRESS. (OPER./DES) :

barg ℃

TEMP. (OPER./DES) :

MOTOR DRIVER

*

RATED HP

SERVICE FACTOR

Kw

1.15 FRAME

*

MFR. TYPE

SPEED BEARINGS

SQIRREL-CAGE INDUCTION

INSUL.

EExe ⅡT4 / IP55 TEMP. RISE

ENC.

* *

rpm

PAINTING CL.Ⅰ,DIV.2,Gr.D

HAZARDOUS RATING

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

LUBE

F B

*

FULL LOAD AMPS

PRIMER : SEE ATTACHED PAINTING SPEC. FINAL : SEE ATTACHED PAINTING SPEC. □ INDOOR

LOCATION

*

LOCKED ROTOR AMPS

A APPROX. WT. PUMP & BASE

*

A MOTOR

*

Kg

OUTDOOR

* TOTAL

Kg

*

Kg

REMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2.

** MINIMUM FLOW ASSURED BY SPILL BACK RO. VERIFY THE PURCHASED PUMP MIN.FLOW * PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE.

3.

0 REVISION NO.

FOR APPROVAL NOTES

VG

VG

MSB

21/09/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LTD.

MAGNETIC TYPE CENTRIFUGAL PUMP DATA SHEET ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA TR4101 Transfer Pump

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PC4152

PAGE

HYDROCARBON

YES

NO

PUMPING TEMP.

NUMBER OF REQ'D

TOXIC

DATE

SPECIFIC GRAVITY AT P.T.

PERFORMANCE AT RATED Kg/l

PARTICLE DIA.

mm

℃ VAPOR PRESS. AT P.T.

0.74

OPER.0.63 / MAX. 10

CORROSIVE (IF ANY)

.

NEGLIGIBLE

NONE

SUC. PRESS.

COMPOUND

NOR.4.0

1.35 30 >7

DIFF. PRESS.

SOLIDS (IF ANY) ; NAME

DIFF. HEAD

CONTENT

%wt NPSH AVAILABLE

CORR. ALLOW.

1.6

mm

FLOW CONTROL

m

NO. OF STAGE

m3/h

5.35

CP DISCH. PRESS.

PROPOSAL CURVE NO. NPSH REQ'D

bara

RATED 15

CAPACITY

VISCOSITY AT P.T.

ROTATING SPEED

rpm

bara

DESIGN EFFICIENCY

bara

BHP AT RATED

Kw

MAX. BHP RATED IMP.

Kw

bar

SIZE

* *

SUCTION DISCHARGE

; □ CENTERLINE

CASE-MOUNT -SPLIT

; □ AXIAL

ROTATION FROM CPLG. END □ CW

AUTO.

-PRESS.

; MAX. ALLOW

JACKET - CASING ;

*

YES

NO

- STUFFING BOX ;

YES

IMPELLER DIA.

; RATED

TYPE ; BEARING TYPE ;

℃

- SEAL GLAND : mm

*

VENT YES

SHAFT

DRAIN

Kg/cm2G

GAUGE

FLOOD

RING OIL

FLINGER

MAGNETIC

THRUST RING mm REAR CASING

OVERHUNG

□ GEAR

CONST. LEVEL OILER

SHOP TESTS

□ DRIVER MFR. BASE PLATE ;

COMMON

□ PURCHASER

□ NON-WIT. PERF.

WIT. PERF.

□ SEPARATE

□ NON-WIT. HYDRO.

WIT. HYDRO.

□ NPSH REQ'D

* MAGNETIC COUPLING TYPE ;

SEPARATLY COUPLED

CLOSE COUPLED

TEMP. DESIGN / OPER. / MIN. ;

/

/

PRESSURE DESIGN / OPER. ; MAGNETS TORQUE DESIGN / NOR. AT OPER. TEMP.

℃

□ DISMANTLE & INSP. AFTER TEST

kg/cm2G

□ OTHER

316 S.S

INNER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

OUTER MAGNET RING ;

ALNICO

NEODYMIUM

SAMARIUM COBALT

BRACKET ;

CARBON

UTILITY DATA kg-m

/

CONTAINMENT SHELL ;

CARBON

□ WT. NPSH

SHOP INSPECTION

kg/cm2G

REAR CASING BURST PRESSURE ;

MAIN BUSHING ;

C.S

JACKET

*

MFR'S TYPE NO.

□ V-BELT

CASING GASKET BASE PLATE

PURE OIL MIST.

PUMP MFR.

OUTTER MAGNET MAIN BUSH

*

MAX./MIN.

* * * * * *

INNER MAGNET

NO

MOUNT. ; □ BETWEEN BRGS

DRIVER HALF MTD. BY ; DIR

IMPELLER

□ IN-LINE

HYDRO. TEST

C.S SS316 SS316

CASING

THRUST

GREASE

;

API CLASS

END TOP

□ NEAR CENTERLINE

CONNECT ; NO

POSITION

TYPE VOLUTE ; □ SGL. □ MULTIPLE □ DIFFUSER

250

* *

; TYPE

DRIVER

R.F R.F

RADIAL

LUBE ; COUPLING

FACING

bar

□ CCW

MATERIALS

RATING

FOOT

m m3/h

m MIN. CONTINUOUS

MANUAL

ANSI 150 # ANSI 150 #

RADIAL □ BARREL

%

m MAX. HEAD RATED IMP.

CONSTRUCTION NOZZLES

1

ONE / 0 November 21, 2017

(MAIN / SPARE)

VG

BY

TRUE DENSITY

160

OF

REQ. NO.

OPERATION CONDITIONS EACH PUMP Crude Anox 20

LIQUID NAME

1

SPEC./CODE NO.

HEATING FLUID TYPE :

ZIRCONIA

PRESS.(NOR./DES) :

barg ℃

TEMP.(NOR./DES) : COOLING FLUID :

SIC.

ℓ/hr

QT'Y PRESS. (OPER./DES) :

SHAFT ;

316 S.S

HASTELLOY C-276

O-RING ;

VITON

TEFLON

barg ℃

TEMP. (OPER./DES) :

KALREZ

NITROGEN : PRESS. (OPER./DES) :

barg ℃

TEMP. (OPER./DES) :

MOTOR DRIVER

*

RATED HP

SERVICE FACTOR

Kw

1.15 FRAME

*

MFR. TYPE

SPEED BEARINGS

SQIRREL-CAGE INDUCTION

INSUL.

EExe ⅡT4 / IP55 TEMP. RISE

ENC.

* *

rpm

PAINTING CL.Ⅰ,DIV.2,Gr.D

HAZARDOUS RATING

480 / 3/ 60

VOLTS/PHASE/CYCLES

*

LUBE

F B

*

PRIMER : FINAL : □ INDOOR

LOCATION

FULL LOAD AMPS

*

LOCKED ROTOR AMPS

OUTDOOR

*

A APPROX. WT. PUMP & BASE

*

A MOTOR

*

Kg

TOTAL

Kg

*

Kg

REMARKS 1.

THE RECOMMENDED PACKING OR SEALING MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ.

2.

* PUMP MANUFACTURER TO ADVISE THESE POINTS AT QUOTATION STAGE.

0 REVISION NO.

FOR APPROVAL NOTES

VG

VG

MSB

21/11/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LIMITED VACUUM PUMP DATA SHEET (MECHANICAL TYPE) ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA REACTION VACUUM SYSTEM

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PK4102

PAGE

NAME

NUMBER OF REQ'D

VG

BY

PROPOSAL CURVE NO.

BY MFR. m 3/h CAPACITY ;

AT SUCTION COND.

AT ℃ 1ATA

PP base

Nm 3/h

Nm 3/h

1

DESIGN SUC. PRESS.

Kg/cm 2A MAX. VACUUM

7/FULL VAC.

DESIGN 1.0 DISCH. PRESS. 840 SUCTION TEMP. BY MANUFACTURER

MOLECULAR WEIGHT Kg/cm 3

SPECIFIC WEIGHT

DISCH. PRESS.

mmHg

EFF. AT RATING

%

BHP AT RATING

Kw

℃

CONTENT

mm

80

NOISE LEVEL @ 1m

db(A)

NOM. SIZE

RATING

FACING

LOCATION

2″

ANSI #150 ANSI #150

F.F F.F

TOP SIDE

DISCHARGE

TYPE ; ■ SCREW □ ROTARY □ LIQUID RING □ W/EJECTOR(GAS/STEAM) □ PISTON □ WET

SEALING LIQUID NAME ;

□

PRESS.(IN/OUT)

STRAINERS (¼″ MESH, S.S) ; ■ SUCTION

TEMP.(IN/OUT)

ANCHOR BOLT & NUTS ;

■ C.W INLET

□ GEAR ■ COMMON

■ YES

□ V-BELT

NORMAL OPERATING ;

□ GP

■ MS

□ SINGLE

GLAND PACKING SIZE - MAT'L EXTERNAL SEAL FLUSH ; □ SEALING LIQUID

N/A

□ Q'TY

Kg/cm 2G

DRY □ DOUBLE

■ MFR'S TYPE

CASING GASKET

■ MFR.

BASE PLATE

■ SEAL RING

□ F.I

API SEAL PLAN

□ P.I

AUX. SEAL PLAN

TESTS

CARBON T.C or EQ. KALREZ DRY

■ STATOR

□ CYCLONE SEPARATOR

SHOP TEST

EQUIP. NO. TYPE

EExdⅡB T4 / IP 55

ENC. FLAME

CL.Ⅰ, DIV.2, Gr.D VOLTS/PHASE/CYCLES 480 / 3 / 60 SERVICE FACTOR 1.15

SQUIRREL-CAGE INDUCTION

INSUL./TEMP.RISE BR'G

F/B

WITNESS

■ YES □ NO

■ YES □ NO

DISASSEMBLY

■ YES □ NO

□ YES □ NO

HYDROSTATIC T.

HAZARDOUS

RPM

REQ'D

RUNNING PERF.

PNEUMATIC T.

MOTOR DRIVER Kw

DUCTILE CAST IRON 304L S.S TEFLON CARBON STEEL

ROTOR/IMPELLER HEAT EXCHANGER

□ RESERVOIR

RATED H.P.

DUCTILE CAST IRON

HEAD

■ API CODE

■ PACKING

ACCESSORIES ;

MFR.

CAST IRON

CONES/PORTS

MATERIALS ; Liter/h

□ PRESS.

Kg/cm 2G

MATERIALS

SHAFT

MECH. SEAL TYPE ;

℃ kcal/m 2℃h

API CLASS

SHAFT SEAL ■ MS

barg

ℓ/h

□ NO BODY

□ GP

ℓ/h

4.0 / 10 / 16 0.0002

PRESS.(IN/OUT)

PAINTING COLOR ; □ MUNSEL NO. N-7.0

ASSEMBLY AT SHIPPING ;

cp Kg/cm 2A

STEAM ; Q'TY

■

□ SEPARATE

℃

AMB

TEMP.

FOULING FACTOR

PAINTING MAT'L ; □ 2 COAT OF VINYL ENAMEL

FLEXIBLE

■ DIR.

BASE PLATE ;

㎏/㎥ VISCO.

CHILLED WATER ; Q'TY

■ SUCTION & DISCHARGE NOZZLE

■ VERTICAL

ℓ/h

DENSITY VAPOR PRESS.

FLEXIBLE JOINT ; ■ CHILLED WATER LINE

CASING ; □ HORIZONTAL

Q'TY

VIB. ISOLATORS ; □ NEOPRENE PAD ■ SPRING

SEALING TYPE ; ■ OIL FREE □ OIL SEALED COUPLING TYPE ;

db(A)

UTILITY DATA

TORR.

SUCTION

□ CW □ CCW

NOISE LEVEL @ 1m

CONSTRUCTION NOZZLES

rpm

ROTATION FROM CPLG. END ;

CORR. ALLOW.

%wt

VAPOR PRESS. AT P.T.

DRIVE ;

Kw

ROTATING SPEED

COMPOUND

Methanol + PP Base + AIR

Torr

MAX.

NAME

VAPOR CONDENSATE (IF ANY) ;

Torr

mmHg

CORROSIVE (IF ANY) ;

RATIO OF Cp/Cv

Kg/cm 2A

mm Hg SUCTION VACUUM

MAX. VACUUM

■ DRY

m 3/h

API SUCTION CONDITION

PRESSURE ; SUCTION VACUUM

VAPOR NAME

2

PERFORMANCE

CAPACITY;

Reaction Mass Vapours Methanol

OF

PC4102X ONE (1) PK'G DATE 29/09/2017

PUMP ITEM NO.

OPERATION CONDITIONS EACH PUMP GAS COMPOSITION ;

1

SPEC./CODE NO.

VACUUM TEST

10.5

Kg/cm 2G

□ YES □ NO

Kg/cm 2G

■ YES □ NO

1.0

mmHg ■ YES □ NO □ YES □ NO

LOCATION ;

□ INDOOR

FULL LOAD AMPS

A APPROX. WT. PUMP & BASE

LOCKED ROTOR AMPS

A MOTOR

Kg

■ OUTDOOR Kg TOTAL

Kg

REMARKS 1. THE PACKING AND SEAL MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ. 2. TYPE OF VACUUM PUMP : NON - LUBRICATED, JACKETED CHILLED WATER COOLED TYPE AND CORROSION RESISTANT. 3. VENDOR SHALL PROVIDE 304L S.S FOR COOLER, VALVE, PIPING AND ALL ACCESSORIES. 4. SCOPE OF WORK : ATTACHED P & I.D NO. PD-30-1021-005-A1, REV.1 WITH FLEXIBLE TUBE, SIGHT GLASS, VALVES, JUNCTION BOX AND INSTRUMENTS. 0 REVISION NO.

5. NITROGEN : PRESSURE IN/OUT/DESIGN : 8.0 / - / 10.0 bar.

FOR APPROVAL NOTES

VG

VG

MSB

29/09/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LIMITED DRY TYPE VACUUM BOOSTER DATA SHEET (MECHANICAL TYPE) ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA DRY TYPE VACUUM BOOSTER FOR PK4102

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PK4102

PAGE

NAME

NUMBER OF REQ'D

VG

BY

PROPOSAL CURVE NO.

AT SUCTION (ACTUAL)

NOR.5000,

AT ℃ 1ATA

PP base

m 3/h CAPACITY ;

Nm 3/h

m 3/h

API SUCTION CONDITION

Nm 3/h

PRESSURE ;

1.0

SUCTION VACUUM DESIGN SUC. PRESS. DISCH. PRESS. MOLECULAR WEIGHT

SUCTION TEMP. Kg/cm 3

SPECIFIC WEIGHT

mmHg mmHg Kg/cm 2A ℃

CORROSIVE (IF ANY) ;

RATIO OF Cp/Cv

CONTENT

%

BHP AT RATING

Kw Kw rpm □ CW □ CCW

ROTATION FROM CPLG. END ;

CORR. ALLOW.

mm

NOISE LEVEL @ 1m

db(A)

UTILITY DATA

%wt

VAPOR PRESS. AT P.T.

Torr

EFF. AT RATING

ROTATING SPEED

COMPOUND

Methanol + PP Base + AIR

Torr

DISCH. PRESS.

MAX.

NAME

VAPOR CONDENSATE (IF ANY) ;

Kg/cm 2A

SUCTION VACUUM

Kg/cm 2A MAX. VACUUM

7/FULL VAC.

BY MFR. BY MFR. 80

MAX. VACUUM

VAPOR NAME

TORR.

80

NOISE LEVEL @ 1m

db(A)

SEALING LIQUID NAME ; Q'TY

ℓ/h

NOZZLES

NOM. SIZE

RATING

FACING

LOCATION

DENSITY

㎏/㎥ VISCO.

SUCTION

6″

ANSI #150 ANSI #150

F.F F.F

TOP BOTTOM

VAPOR PRESS.

CONSTRUCTION

DISCHARGE TYPE ; □ SCREW ■ ROTARY □ LIQUID RING □ W/EJECTOR(GAS/STEAM) □ PISTON ■ DRY

□ WET

□

PRESS.(IN/OUT)

STRAINERS (¼″ MESH, S.S) ; ■ SUCTION

TEMP.(IN/OUT)

■ C.W INLET

■ VERTICAL

ANCHOR BOLT & NUTS ;

□ DIR.

□ GEAR ■ COMMON

BASE PLATE ;

■ YES

■ V-BELT

NORMAL OPERATING ;

□ GP

■ MS

□ SINGLE

- MAT'L EXTERNAL SEAL FLUSH ; □ SEALING LIQUID

N/A

□ Q'TY

DRY

HEAD

□ DOUBLE

Kg/cm 2G

HEAT EXCHANGER

■ MFR'S TYPE

CASING GASKET

■ MFR.

BASE PLATE

■ SEAL RING

□ RESERVOIR

□ F.I

API SEAL PLAN

□ CYCLONE SEPARATOR

□ P.I

AUX. SEAL PLAN

SHOP TEST

EQUIP. NO. RPM TYPE

EExdⅡB T4 / IP 55

ENC. FLAME

CL.Ⅰ, DIV.2, Gr.D VOLTS/PHASE/CYCLES 480 / 3 / 60 SERVICE FACTOR 1.15

SQUIRREL-CAGE INDUCTION

INSUL./TEMP.RISE BR'G

F/B

WITNESS

■ YES □ NO

■ YES □ NO

DISASSEMBLY

■ YES □ NO

□ YES □ NO

HYDROSTATIC T.

HAZARDOUS

Kw

REQ'D

RUNNING PERF.

PNEUMATIC T.

MOTOR DRIVER RATED H.P.

TEFLON CARBON STEEL

TESTS

CARBON T.C or EQ. KALREZ DRY

■ STATOR ■ PACKING

ACCESSORIES ;

MFR.

DUCTILE CAST IRON

ROTOR/IMPELLER

■ API CODE

MATERIALS ; Liter/h

□ PRESS.

DUCTILE CAST IRON

SHAFT

MECH. SEAL TYPE ;

GLAND PACKING SIZE

CAST IRON

CONES/PORTS

SHAFT SEAL ■ MS

Kg/cm 2G

MATERIALS BODY

□ GP

℃ kcal/m 2℃h

API CLASS

PAINTING COLOR ; □ MUNSEL NO. N-7.0

ASSEMBLY AT SHIPPING ;

barg

ℓ/h

□ NO

■

□ SEPARATE

ℓ/h

4.0 / 10 / 16 0.0002

PRESS.(IN/OUT)

PAINTING MAT'L ; □ 2 COAT OF VINYL ENAMEL

COUPLING TYPE ;

cp

STEAM ; Q'TY

■ SUCTION & DISCHARGE NOZZLE

℃

AMB.

Kg/cm 2A

FOULING FACTOR

FLEXIBLE JOINT ; ■ CHILLED WATER LINE

CASING ; □ HORIZONTAL

TEMP.

CHILLED WATER ; Q'TY

VIB. ISOLATORS ; □ NEOPRENE PAD ■ SPRING

SEALING TYPE ; ■ OIL FREE □ OIL SEALED

DRIVE ;

2

PERFORMANCE

CAPACITY;

Reaction Mass Vapours Methanol

OF

BD4102X ONE (1) SET DATE 29/09/2017

PUMP ITEM NO.

OPERATION CONDITIONS EACH PUMP GAS COMPOSITION ;

2

SPEC./CODE NO.

10.5

Kg/cm 2G

□ YES □ NO

Kg/cm 2G

■ YES □ NO

mmHg ■ YES □ NO

VACUUM TEST

□ YES □ NO LOCATION ;

□ INDOOR

FULL LOAD AMPS

A APPROX. WT. PUMP & BASE

LOCKED ROTOR AMPS

A MOTOR

Kg

■ OUTDOOR Kg TOTAL

Kg

REMARKS 1. THE PACKING AND SEAL MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ. 2. TYPE OF VACUUM BOOSTER : NON-LUBRICATED, JACKETED CHILLED WATER COOLED TYPE AND CORROSION RESISTANT. 3. SCOPE OF SUPPLY : SEE ATTACHED P & I.D NO. PD-30-1021-005-A1, Rev.1 AND SECTIONS 1.0 & 2.0 OF THIS MATERIAL REQUISITION. 4. VENDOR SHALL DESIGN AND PROVIDE HASTELLOY "B" FOR TP3103 VAPOR/LIQUID SEPARATOR.

0 REVISION NO.

FOR APPROVAL NOTES

VG

VG

MSB

29/09/2017

PREP'D

CHK'D

APPR'D

DATE

LIBRA TECHCON LIMITED VACUUM PUMP DATA SHEET (MECHANICAL TYPE) ITEM NO. LTL-876 GULF STABILIZERS INDUSTRIES JUBAIL, KSA TR4201 VACUUM SYSTEM

CONTRACT NO. CLIENT LOCATION SERVICE OF UNIT

PK4201

PAGE

NUMBER OF REQ'D

VG

BY

1

4-Dec-17

DATE

PERFORMANCE

CAPACITY;

Solvent (methanol) Vapours

NAME

OF

PC4151X ONE (1) PK'G

PUMP ITEM NO.

OPERATION CONDITIONS EACH PUMP GAS COMPOSITION ;

1

SPEC./CODE NO.

PROPOSAL CURVE NO.

NOR.11.5, DESIGN 264

AT SUCT. COND. AT ℃ 1ATA

m 3/h CAPACITY ; 3 API SUCTION CONDITION Nm /h

3

m /h Nm 3/h

PRESSURE ; SEALING LIQUID ;

SUCTION VACUUM

Water

NAME

DISCH. PRESS.

32/86

SUCTION TEMP.

SPECIFIC WEIGHT

mmHg ℃

CORROSIVE (IF ANY) ;

RATIO OF Cp/Cv

mm

mmHg

85

NOISE LEVEL @ 1m

db(A)

NOM. SIZE

RATING

FACING

LOCATION

SUCTION

2″ 2″

ANSI #150 ANSI #150

F.F F.F

TOP TOP

TYPE ; □ SCREW □ ROTARY ■ LIQUID RING

VIB. ISOLATORS ; □ NEOPRENE PAD ■ SPRING

□ W/EJECTOR(GAS/STEAM) □ PISTON

STRAINERS (¼″ MESH, S.S) ; ■ SUCTION

□ WET

□ SEALING TYPE ; ■ OIL FREE □ OIL SEALED CASING ; □ HORIZONTAL

■ SUCTION & DISCHARGE NOZZLE

■ VERTICAL

□ GEAR ■ COMMON

■ YES

ANCHOR BOLT & NUTS ;

□ V-BELT

TEMP.(IN/OUT) PRESS.(IN/OUT)

MATERIALS API CLASS

304L S.S 304L S.S 304L S.S 304L S.S

SHAFT

NORMAL OPERATING ;

□ GP

■ MS

■ SINGLE

□ DOUBLE

ROTOR/IMPELLER

■ API CODE

* * JOHN CRANE or EQ.

HEAT EXCHANGER

■ SEALING LIQUID ■ Q'TY

SAME AS LIQUID RING FLUID

* *

■ PRESS.

Liter/h Kg/cm 2G

HEAD

■ SEAL RING

CARBON T.C or EQ. KALREZ SELF or EQ. N/A

■ STATOR

□ RESERVOIR

□ F.I

API SEAL PLAN

□ CYCLONE SEPARATOR

□ P.I

AUX. SEAL PLAN

MOTOR DRIVER EQUIP. NO.

HAZARDOUS

*

RATED H.P.

Kw

RPM *

*

TYPE

ENC.

EExeⅡT4 / IP55 *

INSUL./TEMP.RISE

FLAME

BASE PLATE

SQUIRREL-CAGE INDUCTION SERVICE

F/B

BR'G *

FACTOR

FULL LOAD AMPS

TESTS SHOP TEST

*

LOCKED ROTOR AMPS

REQ'D

WITNESS

RUNNING PERF.

■ YES □ NO

■ YES □ NO

DISASSEMBLY

■ YES □ NO

■ YES □ NO

PNEUMATIC T.

0.75

Kg/cm 2G

HYDROSTATIC T.

10.5

Kg/cm 2G

CL.Ⅰ, DIV.2, Gr.D VACUUM TEST 480 / 3 / 60 LOCATION ; 1.15

VOLTS/PHASE/CYCLES

MFR.

TEFLON or KALREZ C.S

CASING GASKET

MATERIALS ;

■ PACKING

ACCESSORIES ;

℃

FLUSHING

MECH. SEAL TYPE ;

■ MFR.

barg

TEMP.(IN/OUT)

CONES/PORTS

SHAFT SEAL

SEAL FLUSH ;

℃ ℓ/h

■ MS

■ MFR'S TYPE

barg

STEAM ; Q'TY

□ GP

- MAT'L

ℓ/h

* 5.3 / * 10 / 16

PRESS.(IN/OUT)

ASSEMBLY AT SHIPPING ; GLAND PACKING SIZE

℃

15

Kg/cm 2G

CHILLED WATER ; Q'TY

BODY

PAINTING COLOR ; □ MUNSEL NO. N-7.0

TEMP.

*

□ NO

■

□ SEPARATE

Water ℓ/h

*

PRESS.

PAINTING MAT'L ; □ 2 COAT OF VINYL ENAMEL

FLEXIBLE

■ DIR.

DRIVE ;

■ C.W INLET

FLEXIBLE JOINT ; ■ REF. ETHYLENE GLYCOL LINE

COUPLING TYPE ;

db(A)

SEALING LIQUID NAME ; Q'TY

NOZZLES DISCHARGE

□ CW □ CCW

NOISE LEVEL @ 1m

UTILITY DATA

CONSTRUCTION

BASE PLATE ;

Kw rpm

%wt

VAPOR PRESS. AT P.T.

□ DRY

Kw

ROTATION FROM CPLG. END ;

CORR. ALLOW.

CONTENT

%

BHP AT RATING ROTATING SPEED

COMPOUND

Methanol

VAPOR NAME

Torr

EFF. AT RATING MAX.

NAME

VAPOR CONDENSATE (IF ANY) ;

Kg/cm 2A Torr

SUCTION VACUUM

2 Kg/cm A MAX. VACUUM mmHg DISCH. PRESS.

7 / FULL VAC. 50 810 10

MAX. VACUUM MOLECULAR WEIGHT

mmHg

NOR.50, DESIGN 50

DESIGN SUC. PRESS.

FULL VAC.

■ YES □ NO ■ YES □ NO Torr. ■ YES □ NO □ YES □ NO

□ INDOOR

■ OUTDOOR

*

A APPROX. WT. PUMP & BASE

*

A MOTOR

*

Kg

Kg

*

TOTAL

Kg

REMARKS 1. THE PACKING AND SEAL MATERIAL IN CONTACT WITH THE PROCESS FLUID IS TEFLON OR KALREZ. 2. PUMP CASING AND MECHANICAL SEAL MUST BE COMPLETELY DRAINABLE. 3. LIQUID RING VACUUM PUMP SHALL BE SKID MOUNTED AND COMPLETE WITH DISCHARGE SEPERATOR, COOLER, SINLENCER, MOTOR, SEALS, VALVES, FLEXIBLE JOINTS, JUNCTION BOX AND RELATED INSTRUMENTS W/CONTROLS. 4. * VENDOR ADVISE TO THESE POINT AT QUOTATION STAGE. 1

FOR APPROVAL

VG

MSB

MSB

12/4/2017

0

FOR APPROVAL

VG

MSB

MSB

21/11/2017

PREP'D

CHK'D

APPR'D

DATE

REVISION NO.

NOTES

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No. • • • • • • • • • • • • • • • • • •

Name Quantity Tag. No. Fluid Working Capacity Gross Volume Min Stirrable Volume Liq.Density Liq.VISCOSITY Mixing scale Corrosive Vessel Int Dia Vessel Length , straight shell Support Type Baffles Insulation Location Orientation

• • • • • • • • •

Operating Press. Of Shell Operating Temp. Of Shell Design Press. Of Shell D i T Design Temp. Of Shell Sh ll External pressure on shell Code PWHT Fire Proofing Head Types

• • • • • • • •

Sweep Dia Type of agitator Number of impellers Agitator RPM Gear box Shaft Dia Sealing arrangement Make

• • • • • •

Shell Dish end Internal Coil Jacket Internal Lug support

Methanol Collector - Atmospheric M/S Gulf Stabilizers Industries Basic Engineering Package LTL-876 General :Methanol Collector :1 nos. :TP4110 :Methanol :3 :3.45 :N/A :792 :0.5 :N/A :No :1530 :1875 :Lug :N/A :Cold Insulation :Above Ground, Under Shed :Vertical

:::::::::-

:::-

Material Specification Material SS316 SS316 N/A N/A N/A CS

LTL/876- PDS - V01 PROCESS R0 8-Sep-17

KL KL KL Kg/m3 CP

mm mm 4 nos

Operating Conditions Atm 35 C FV to 6 Kg/cm2 g 60  ̊C ̊ Kg/cm2 g Atm. As per ASME Sec-VIII Div-I No No TOP :- Torispherical Dish end (10 % CR)

Agitator Detail :N/A :N/A :N/A :N/A :N/A :N/A :N/A :N/A

::-

DOC NO. DEPARTMENT REVISION DATE

Type Power Motor HP/RPM Frequency Class Area classification Make

BOTTOM :- Torispherical Dish Motor Detail :::::::-

N/A N/A N/A N/A N/A N/A N/A

Corr.Allow. NA NA NA NA NA 3 mm

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No.

N1 N2 N3 N4 N5 N6 N7 HH

Methanol Collector - Atmospheric DOC NO. M/S Gulf Stabilizers Industries DEPARTMENT Basic Engineering Package REVISION LTL-876 DATE Nozzle and Manways Service SIZE, NB Process Liquid inlet 50 Process liquid outlet 50 Level Switch 50 Temperature Transmitter 50 Level Transmitter 80 Pressure safety Valve 40 BD1 25 Handhole 150

LTL/876- PDS - V01 PROCESS R0 8-Sep-17 Rating 150# 150# 150# 150# 150# 150# 150# 150#

Note:1. All dimensions are in mm unless otherwise specified. 2. Corrosion allowance as per code. MDS to consider international codes and standards 3. ** vendor to confirm 4. Hydrotest shall required for shell, internal coil & limpet coil as per code 5. * Number of baffles & size of to be confirmed after discussion with agitator supplier 6. To be confirmed by Mechanical as per Codes. R2 R1 R0 REV

Issued for Approval Issued for Approval Issued for Approval Description

3-Dec-17 19-Sep-17 8-Sep-17 DATE

VG VG VG PREPARED BY

VG VG VG CHECKED BY

MSB MSB MSB APPROVED BY

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No. • • • • • • • • • • • • • • • • • •

Name Quantity Tag. No. Fluid Working Capacity Gross Volume Min Stirrable Volume Liq.Density Liq.VISCOSITY Mixing scale Corrosive Vessel Int Dia Vessel Length , straight shell Support Type Baffles Insulation Location Orientation

• • • • • • • • • • • • •

Operating Press. Of Shell Operating Temp. Of Shell Operating Press. Of Jacket O Operating ti Temp. T Of Jacket J k t Design Press. Of Shell Design Temp. Of Shell Design Press. Of Jacket Design Temp. Of Jacket External pressure on shell Code PWHT Fire Proofing Head Types

• • • • • • • •

Sweep Dia Type of agitator Number of impellers Agitator RPM Gear box Shaft Dia Sealing arrangement Make

• • • • • •

Shell Dish end Internal Coil Jacket Internal Lug support

Methanol Collector - Vacuum M/S Gulf Stabilizers Industries Basic Engineering Package LTL-876 General :Methanol Collector :1 nos. :TP4111 :Methanol :2 :2.3 :N/A :792 :0.5 :N/A :No :1300 :1600 :Lug :N/A :N/A :Above Ground, Under Shed :Vertical

:::::::::::::-

:::-

Material Specification Material SS316 SS316 N/A SS304 N/A CS

LTL/876- PDS - V02 PROCESS R0 8-Sep-17

KL KL KL Kg/m3 CP

mm mm 4 nos

Operating Conditions FV to Atm. 35 C 4 Kg/cm2 g -20 20 C FV to 6 Kg/cm2 g 60  ̊C 6 Kg/cm2 g (-)25 to 60  ̊C Kg/cm2 g 6 As per ASME Sec-VIII Div-I No No TOP :- Torispherical Dish end (10 % CR)

Agitator Detail :N/A :N/A :N/A :N/A :N/A :N/A :N/A :N/A

::-

DOC NO. DEPARTMENT REVISION DATE

Type Power Motor HP/RPM Frequency Class Area classification Make

BOTTOM :- Torispherical Dish Motor Detail :::::::-

N/A N/A N/A N/A N/A N/A N/A

Corr.Allow. NA NA NA NA NA 3 mm

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No.

N1 N2 N3 N4 N5 N6 N7 N8 N9 MH

Methanol Collector - Vacuum DOC NO. M/S Gulf Stabilizers Industries DEPARTMENT Basic Engineering Package REVISION LTL-876 DATE Nozzle and Manways Service SIZE, NB Process Liquid inlet 50 Process liquid outlet 50 Level Switch 50 BD1/UN 50 Level Transmitter 80 Pressure safety Valve 40 Jacket Outlet 40 Jacket Inlet 40 Jacket Drain 25 handhole 150

LTL/876- PDS - V02 PROCESS R0 8-Sep-17 Rating 150# 150# 150# 150# 150# 150# 150# 150# 150# 150#

Note:1. All dimensions are in mm unless otherwise specified. 2. Corrosion allowance as per code. MDS to consider international codes and standards 3. ** vendor to confirm 4. Hydrotest shall required for shell, internal coil & limpet coil as per code 5. * Number of baffles & size of to be confirmed after discussion with agitator supplier 6. To be confirmed by Mechanical as per Codes. R2 R1 R0 REV

Issued for Approval Issued for Approval Issued for Approval D Description i ti

3-Dec-17 19-Sep-17 8-Sep-17 DATE

VG VG VG PREPARED BY

VG VG VG CHECKED BY

MSB MSB MSB APPROVED BY

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No. • • • • • • • • • • • • • • • • • •

Name Quantity Tag. No. Fluid Working Capacity Gross Volume Min Stirrable Volume Liq.Density Liq.VISCOSITY Mixing scale Corrosive Vessel Int Dia Vessel Length , straight shell Support Type Baffles Insulation Location Orientation

• • • • • • • • • • • • •

Operating Press. Of Shell Operating Temp. Of Shell Operating Press. Of Jacket O Operating ti Temp. T Of Jacket J k t Design Press. Of Shell Design Temp. Of Shell Design Press. Of Jacket Design Temp. Of Jacket External pressure on shell Code PWHT Fire Proofing Head Types

• • • • • • • •

Sweep Dia Type of agitator Number of impellers Agitator RPM Gear box Shaft Dia Sealing arrangement Make

• • • • • •

Shell Dish end Internal Coil Jacket Internal Lug support

PP Base Collector - Vacuum M/S Gulf Stabilizers Industries Basic Engineering Package LTL-876 General :PP Base Collector :1 nos. :TP4112 :PP Base :2 :2.3 :N/A :::N/A ::1300 :1600 :Lug :N/A :N/A :Above Ground, Under Shed :Vertical

:::::::::::::-

:::-

Material Specification Material SS316 SS316 N/A SS304 N/A IS 2062

LTL/876- PDS - V03 PROCESS R0 8-Sep-17

KL KL KL Kg/m3 CP

mm mm 4 nos

Operating Conditions FV to Atm 90 C 4.5 Kg/cm2 g 80 C FV to 6 Kg/cm2 g 100  ̊C 6 Kg/cm2 g 100  ̊C Kg/cm2 g 6 As per ASME Sec-VIII Div-I No No TOP :- Torispherical Dish end (10 % CR)

Agitator Detail :N/A :N/A :N/A :N/A :N/A :N/A :N/A :N/A

::-

DOC NO. DEPARTMENT REVISION DATE

Type Power Motor HP/RPM Frequency Class Area classification Make

BOTTOM :- Torispherical Dish Motor Detail :::::::-

N/A N/A N/A N/A N/A N/A N/A

Corr.Allow. NA NA NA NA NA 3 mm

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No.

N1 N2 N3 N4 N5 N6 N7 N8 N9 N10 N11 HH

PP Base Collector - Vacuum DOC NO. M/S Gulf Stabilizers Industries DEPARTMENT Basic Engineering Package REVISION LTL-876 DATE Nozzle and Manways Service SIZE, NB Process Liquid inlet 50 Process liquid outlet 50 Extra 50 Temperature indicator 50 Level Transmitter 80 Pressure safety Valve 40 Jacket Inlet 25 Jacket Outlet 25 Jacket Drain 25 Vent 50 UN 25 Handhole 150

LTL/876- PDS - V03 PROCESS R0 8-Sep-17 Rating 150# 150# 150# 150# 150# 150# 150# 150# 150# 150# 150# 150#

Note:1. All dimensions are in mm unless otherwise specified. 2. Corrosion allowance as per code. MDS to consider international codes and standards 3. ** vendor to confirm 4. Hydrotest shall required for shell, internal coil & limpet coil as per code 5. * Number of baffles & size of to be confirmed after discussion with agitator supplier 6. To be confirmed by Mechanical as per Codes. R2 R1 R0 REV

Issued for Approval I Issued d for f Approval A l Issued for Approval Description

3-Dec-17 19-Sep-17 19 S 17 8-Sep-17 DATE

VG VG VG PREPARED BY

VG VG VG CHECKED BY

MSB MSB MSB APPROVED BY

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No. • • • • • • • • • • • • • • • • • •

Name Quantity Tag. No. Fluid Working Capacity Gross Volume Min Stirrable Volume Liq.Density Liq.VISCOSITY Mixing scale Corrosive Vessel Int Dia Vessel Length , straight shell Support Type Baffles Insulation Location Orientation

• • • • • • • • •

Operating Press. Of Shell Operating Temp. Of Shell Design Press. Of Shell D i T Design Temp. Of Shell Sh ll External pressure on shell Code PWHT Fire Proofing Head Types

• • • • • • • •

Sweep Dia Type of agitator Number of impellers Agitator RPM Gear box Shaft Dia Sealing arrangement Make

• • • • • •

Shell Dish end Internal Coil Limpet Internal Lug support

Catalyst Loading Vessel M/S Gulf Stabilizers Industries Basic Engineering Package LTL-876 General :Catalyst Loading Vessel :1 nos. :TP4114 :LiOMe :1 :1.15 :N/A :700 to 1000 :0.5 to 5 :N/A :No :1020 :1250 :Lug :N/A :N/A :Above Ground, Under Shed :Vertical

:::::::::-

:::-

Material Specification Material SS316 SS316 N/A N/A N/A CS

LTL/876- PDS - V04 PROCESS R0 8-Sep-17

KL KL KL Kg/m3 CP

mm mm 4 nos

Operating Conditions Atm. amb. C 3.5 Kg/cm2 g 60  ̊C ̊ Kg/cm2 g Atm. As per ASME Sec-VIII Div-I No No TOP :- Torispherical Dish end (10 % CR)

Agitator Detail :N/A :N/A :N/A :N/A :N/A :N/A :N/A :N/A

::-

DOC NO. DEPARTMENT REVISION DATE

Type Power Motor HP/RPM Frequency Class Area classification Make

BOTTOM :- Torispherical Dish Motor Detail :::::::-

N/A N/A N/A N/A N/A N/A N/A

Corr.Allow. NA NA NA NA NA 3 mm

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No.

N1 N2 N3 N4 N5 N6 N7 N8 N9 MH

Catalyst Loading Vessel DOC NO. M/S Gulf Stabilizers Industries DEPARTMENT Basic Engineering Package REVISION LTL-876 DATE Nozzle and Manways Service SIZE, NB Process Liquid inlet 50 Process liquid outlet 50 BD1 25 Pressure gauge 25 Nitrogen Blanketing 40 BD3 40 Level Inicator 80 Temperature Indicator 50 Weight Cell 15 Manhole 450

LTL/876- PDS - V04 PROCESS R0 8-Sep-17 Rating 150# 150# 150# 150# 150# 150# 150# 150# 150# 150#

Note:1. All dimensions are in mm unless otherwise specified. 2. Corrosion allowance as per code. MDS to consider international codes and standards 3. ** vendor to confirm 4. Hydrotest shall required for shell, internal coil & limpet coil as per code 5. * Number of baffles & size of to be confirmed after discussion with agitator supplier 6. To be confirmed by Mechanical as per Codes. R2 R1 R0 REV

Issued for Approval Issued for Approval Issued for Approval D Description i ti

3-Dec-17 19-Sep-17 8-Sep-17 DATE

VG VG VG PREPARED BY

VG VG VG CHECKED BY

MSB MSB MSB APPROVED BY

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No. • • • • • • • • • • • • • • • • • • •

Name Quantity Tag. No. Fluid Working Capacity Gross Volume Min Stirrable Volume Liq.Density Liq.VISCOSITY Mixing scale Corrosive Vessel top diameter Vesselbottom diameter Vessel Height Support Type Baffles Insulation Location Orientation

• • • • • • • • •

Operating Press. Of Shell Operating Temp. Of Shell D i P Design Press. Of Sh Shellll Design Temp. Of Shell External pressure on shell Code PWHT Fire Proofing Head Types

• • • • • • • •

Sweep Dia Type of agitator Number of impellers Agitator RPM Gear box Shaft Dia Sealing arrangement Make

• • • • • •

Shell Dish end Internal Coil Limpet Internal Lug support

Dryer Material Loading Hopper M/S Gulf Stabilizers Industries Basic Engineering Package LTL-876 General :Dryer Material Loading Hopper :1 nos. :TS4110 :Anox 20 Solids :2.5 :2.875 :N/A ::::No :1500 :1000 :1900 :Lug :N/A :N/A :Above Ground, Under Shed :Vertical

:::::::::-

:::-

Material Specification Material SS304 SS304 N/A N/A N/A CS

LTL/876- PDS - V05 PROCESS R0 19-Sep-17

KL KL KL Kg/m3 CP

mm mm mm 4 nos

Operating Conditions Atm. amb. C 03 0.3 K / 2g Kg/cm2 60  ̊C Kg/cm2 g Atm. As per ASME Sec-VIII Div-I No No TOP :-Flat

Agitator Detail :N/A :N/A :N/A :N/A :N/A :N/A :N/A :N/A

::-

DOC NO. DEPARTMENT REVISION DATE

Type Power Motor HP/RPM Frequency Class Area classification Make

BOTTOM :-Flat Motor Detail :::::::-

N/A N/A N/A N/A N/A N/A N/A

Corr.Allow. NA NA NA NA NA 3 mm

LIBRA TECHCON LIMITED

DOCUMENT CLIENT PROJECT PROJECT No.

N1 N2 N4 N5 N6 N7 N8

Dryer Material Loading Hopper DOC NO. M/S Gulf Stabilizers Industries DEPARTMENT Basic Engineering Package REVISION LTL-876 DATE Nozzle and Manways Service SIZE, NB Process Liquid inlet 250 Process liquid outlet 150 Extra 80 Extra 80 Nitrogen blanketing 25 Extra 200 Extra 200

LTL/876- PDS - V05 PROCESS R0 19-Sep-17

Side top

Rating 150# 150# 150# 150# 150# 150# 150#

VG VG CHECKED BY

MSB MSB APPROVED BY

Note:1. All dimensions are in mm unless otherwise specified. 2. Corrosion allowance as per code. MDS to consider international codes and standards 3. ** vendor to confirm 4. Hydrotest shall required for shell, internal coil & limpet coil as per code 5. * Number of baffles & size of to be confirmed after discussion with agitator supplier 6. To be confirmed by Mechanical as per Codes.

R1 R0 REV

Issued for Approval Issued for Approval Description

3-Dec-17 19-Sep-17 DATE

VG VG PREPARED BY

LIBRA TECHCON LIMITED DOCUMENT CLIENT PROJECT PROJECT No.

PDS FOR EC4610 M/S Gulf Stabilizers Industries Basic Engineering Package LTL/876

: : : : Service

LTL/876  PDS  001 LTL/876‐ PDS ‐001 PROCESS R0 13/10/2017

: : : :

Number of Units

Mass Balance Tot. Fluid Quantity

DOC NO. DEPARTMENT REVISION DATE

Process Data Feed 1807.62

units Steam/Vapour Liquid

Reflux Rate (pumparound)

kg/h

Bottom

1709.7 97.92

kg/h

-

kg/h

Feedstage

Operating Conditions Operating Temperature

Distillate

1025.82

Top 64.1

Bottom 87.8

Operating Pressure

Bar a

100 1

1

1

Density vapour / liquid

kg/m³

1.088 / 765.133

1.105 / 757.836

0.952 / 877.63

cP

0.0111 / 0.3504

0.0110 / 0.3496

0.0115 / 0.3370

0.02

0.043

°C

Viscosity vapour / liquid Surface Tension

N/m

Packing (Top/Bottom) Material/Type Column Inner Diameter (ID)

mm mm

Section Height Distributor Number/Material/Type Collector Number/Material/Type Nominal / Total Volume

m³ bar (a)

Design / Test Overpressure Design Temperature

°C

0.03 Column Internals 1" Pall Ring 1000 8260 By vendor By vendor Construction Data By vendor FV / 6 160

Material in Contact with Fluid remaining Parts Gaskets Corrosion Allowance Shell thickness Painting / Protective Inside Lining / -Thickn. Insulation Type / Thickness Weight Empty (total) Standards / Codes

mm mm - / mm - / mm kg

SS316 CS Spiral wound 0 for SS / 3mm for CS By vendor For CS part (red oxide) By vendor 2500 ASME Section VIII Div. 1

PED medium category Inspection NDE

By client As per code As per code Hydro test -Bracket support

X-Ray other NDE

Leak Test Windload / Seismic Zone Supports

Remarks: 1. Manufacturer to consider 100% gasket + 100 % spare = 200% gaskets 2. Inspection by Client 3. For formed/Spinned D/E 100% DPT on all surfaces required. 4 F 4. Fabricator b i t shall h ll provide id mechanical h i l warranty t 5. Body flanges shall be Tounge & Grove, M.O.C of Body flange is CS with SS lining. 6. Refer attached GA drawing No. 9025431-005-005 Sheet 1/2 and 2/2 for further details

R1 R0 Rev

Issued for approval Issued for approval Description

4/12/2017 13/10/2017 Date

RG/ZB RG/ZB Prepared

VG VG Chkd

MSB MSB Apvd

LIBRA TECHCON LTD. MUMBAI

SHEET: PLANT: CLIENT :

Anox20 Dryer Capacity check

Anti-oxidants plant Gulf Stabilizers Industries

As per LTL mass balance for centrifuge Wet cake from centrifuge to dryer is 13093.16 kg Solvent in wet cake is 1964 kg Solvent concentration in wet cake is 15.0 % So,wet cake contains 15% solvent(methanol) and 85% Anox20 powder Considering Product 585 kg/hr As per Mass balance, Anox 20 dry product Batch cycle time Dry Product Feed Dried Product Solvent Evaporated

11129.2 19 585.7 689.11 585.7 103.37

kg/batch hr kg/h kg/h kg/h kg/h

Specific heat of mix. Specific heat of MeOH liquid

0.6 0.6

Specific heat of MeOH vapour Latent heat of MeOH Saturation temp of MeOH at 230 mmHg pressure

0.33 303.64

kcal/kg C kcal/kg 0C kcal/kg 0C Kcal/kg

33.38

O

0

C

12

O

product temp.

64.5

O

Heat required to heat feed (wet cake) Heat required to Evap.solvent

21707.04 31386.36

Kcal/hr Kcal/hr

Total Heat Required.

53093.40

Kcal/hr

Feed inlet temp.

calculated from Antoine's equation

C C

Calculated from LMTD

20% heat loss is added

63712.08

Kcal/hr

Existing Dryer Jacket water inlet flow to dryer Feed (wet cake)

20000 547

kg/hr kg/hr hot water side 0

Zone

Inlet Temp. C

1 2 3

60 75 85

Feed Outlet 0 Temp. C 58.5 73.5 83.5

Heat supplied from hot water to one zone of dryer per zone Heat supplied from hot water to whole dryer unit Area of dryer as per data sheet

Inlet Temp. 12 37.6 52.5 Q Q (total) A

0

Outlet Temp.

ΔTLMTD C

37.6 52.5 64.5

33.00 28.68 25.39

30000 kcal/hr 90000 kcal/hr 2 71 m As per GSI datasheet.

Dryer calculation : Capacity check for MeOH as solvent considering Heat transfer coefficient Log mean temperature difference for each Zone

U ΔTLMTD 0C

50 33.00

2 O Kcal/m .hr c 28.68

Total area of Dryer as per data sheet diameter of cylindrical dryer Length of cylindrical portion only Area of cylindrical portion

A Total D L Adryer

71 2.63 6.6 54.53

m2 m

Area of Agitator

Aagitator

16.47

m2

Area calculation for each zone assuming 1) only 50% agitator is available for heat transfer as mentioned by GSI 2) the agitator area is only available in the 2nd and the 3rd zone. Zone Area

1st 18.18

2nd 20.92

3rd 23.67

Total Area 62.77

25.39

23.67 20.92 18.18 62.77 Thus, 62.76 m verses 71 m area as 50% of agitator is not working 2

Heat load available by existing dryer Q (no modifications)

2

90034.94

Kcal/hr

92122.80

Kcal/hr

Conclusion As exisiting dryer area provides heat load of 90034.94 kcal /hr which is higher than heat required to get dried product of 585 kg/hr, the dryer will be adequate for 585 kg/hr (dry product)

Calculation for Feed temperatures in each zone

LIBRA TECHCON LTD. MUMBAI

Anox20 CF4301 Capacity check

SHEET: PLANT: CLIENT :

Anti-oxidants plant Gulf Stabilizers Industries

CALCULATION OF CENTRIFUGE THROUGHPUT (Q) Q =  VS*A VS = dp2*(ρp‐ρs)*gc / 18µ Q   = Volumetric throughput

cm3/sec

VS  = Sedimentaion velocity

cm/sec

dp  = Particle diameter

cm

ρp  = Particle density

g/cc

ρs   = Solvent density

g/cc

µ   = Solvent viscosity

g/cm‐s

gc   = Gravitational constant

cm/sec2

Solvent ‐ Cyclohexane

Solvent ‐ Methanol

Solvent properties at 15 0C

Solvent at 30 0C

dp

0.01

cm

dp

0.01

cm

ρp

0.9

g/cc

ρp

0.9

g/cc

ρs

0.78

g/cc

ρs

0.80

g/cc

µ 

0.011

g/cm‐s

µ

0.006

g/cm‐s

gc

980

cm/sec2

gc

980

cm/sec2

A

31400

cm2

A

31400

cm2

VS

0.06

cm/sec

VS

0.09

cm/sec

Q (for dp = 0.1 mm)

1882.12

cm3/sec

Q(dp = 0.1 mm)

2721.00

cm3/sec

6.78

m3//hr

9.80

m3//hr

4.90

m3/cycle

3.39

3

m /cycle

For dp

0.001

cm

For dp

0.001

cm

VS

0.001

cm/sec

VS

0.001

cm/sec

Q

18.821

cm3/sec

Q

27.21

cm3/sec

0.10

m3/hr

RG/ZB Prepared

VG Chkd

0.068

3

m /hr

as per data sh

Conclusion: Keeping all other variables constant, the centrifuge should be able to handle the new load. 

R0 Rev

Issued for approval Description

1/11/2017 Date

MSB Apvd

LIBRA TECHCON LTD. MUMBAI

Anox20 ET4301 Capacity check

SHEET: PLANT: CLIENT :

Anti oxidants plant Anti-oxidants Gulf Stabilizers Industries

Existing ET4301 data Assumption, as the MeOH from TP4602 will be condensed and cooled to 35 deg C, the MeOH in storage will be at 35 deg C. The MeOH  required for cake washing in CF4301 is chilled from 35 deg C to 20 deg C. The MeOH supplied for crystallization in TR4201 will be supplied at  i df k hi i CF4301 i hill d f 35 d C t 20 d C Th M OH li d f t lli ti i TR4201 ill b li d t 35 deg C, and any variation in temperature will be taken care by the excess area available. Area Heat Transfer coefficient  Lof Mean Temperature difference Heat Exchanged

A= U= LMTD Q=

7 453 6.4 16700

m2 kcal / h m² °C 0 C kcal/hr

Heat requirement for MeOH chilling Mass of MeOH Water mix to be chilled 3000 0.608 Specific Heat of  solution= Inlet Temperature 45 20 Outlet temperature heat to be provided by RL =  45600.00 Capacity of Centrifudge =  585 Total centrifuging time per batch of Anox 20 = 1.00 heat to be provided by RL to chill =  45600.00 Specific Heat of Refrigarant Liquid =  0.85 ‐20 20 Temperature difference =   Temperature difference  Flow rate of Refrigerant liquid required to Remove heat 10729.412 Flow rate of Refrigerant liquid required to Remove heat 0.386 ConsideringHeat transfer coefficient  Log mean temperature difference 

U= LMTD

200 49.3

kcal / h m² °C 0 C

Area required = Considering 20% margin of safety

A= A=

4.62 5.55

m2 m2

kg/batch kcal/kg 0C 0 C 0 C kcal kg/hr hr kcal/hr kcal/kg 0C to  kg/hr m3/hr

as per mass balance

as mentioned by GSI Dry product basis

‐15 15 Density =

0

C 1120 kg/m3

Conclusion As per data provided by GSI, the Heat exchanger is sufficient to chill MeOH from 36 to 20 0C R2 R1 R0 Rev

Issued for approval Issued for approval Issued for approval Description

3/12/2017 22/11/2017 18/10/2017 Date

RG/ZB RG/ZB RG/ZB Prepared

VG VG VG Chkd

MSB MSB MSB Apvd

LIBRA TECHCON LTD. MUMBAI

Area Heat Transfer coefficient  Lof Mean Temperature difference Heat Exchanged

A= U= LMTD Q=

Anox20 EC4401 Capacity check

SHEET: PLANT PLANT:

A ti Anti-oxidants id t plant l t

CLIENT :

Gulf Stabilizers Industries

Existing ET4401 data 10 m2 106 kcal / h m² °C 0 19.1 C 16440 kcal/hr

Heat requirement for MeOH condensation from Dryer 1964 kg Mass of MeOH Water evaporated in DA4401 Mass of MeOH Water evaporated in DA4401 Time 19.000 hrs Mass of MeOH Water evaporated in DA4401 103.37 kg/hr 0 Specific Heat of  solution= 0.63 kcal/kg  C Latent heat of MeOH water at 230 mmbar 280.00 kcal/kg  0 Temperature of MeOH vapour p p 33.38 C 0 Final temperature 30.00  C heat to be provided by chilled water =  29162.57 kcal/hr 0 Specific Heat of chilled water=  1.00 kcal/kg  C Temperature difference =  10.00 to  Flow rate of chilled water required to Remove heat 3645.32 kg/hr 3.65 m3/hr Flow rate of chilled water required to Remove heat ConsideringHeat transfer coefficient  Log mean temperature difference 

U= LMTD

106 17.6

kcal / h m² °C 0 C

Area required = Area required = Considering 20% margin of safety

A= A=

15.64 18.8

m2 m2

18  0C Density =

1000 kg/m3

Conclusion As per data provided by GSI, the Heat exchanger is not sufficient to condense MeOH from dryer, and hence a new condenser to be designed R2 R1 R0 Rev

Issued for approval Issued for approval Issued for approval Description

4/12/2017 22/11/2017 18/10/2017 Date

RG/ZB RG/ZB RG/ZB Prepared

VG VG VG Chkd

MSB MSB MSB Apvd