Lubricants Handbook.pdf

Ethyl Corporation develops, manufactures, blends and delivers leading-edge additive technology for fuels and lubricants around the world. Our products and services provide the chemistry that makes fuels burn cleaner, engines run smoother, and machines last longer.

Specification Handbook • • • • • • •

Viscosity Crankcase Driveline Industrial Tractor Engine Tests Rig Tests

Ethyl Euro-tech Centre London Road Bracknell Berkshire RG12 2UW United Kingdom

Ethyl Corporation P.O.Box 2189 330 South 4th Street Richmond VA 23218-2189 U.S.A.

www.ethyl.com

Introduction

Since 1921, Ethyl Corporation has provided additive chemistry solutions to enhance the performance of petroleum products. Ethyl additives help lubricants protect engines and other moving parts from wear, deposits, corrosion, water and high operating temperatures. Ethyl lubricant additives are used in oils, fluids and greases around the world to meet the most stringent oil industry, government and original equipment manufacturer (OEM) specifications.

This handbook, compiled by Ethyl, aims to provide a single source for summaries of the most widely used specifications for crankcase, drivetrain, industrial and tractor oils, together with the associated bench, rig and engine test procedures.

Ethyl hope you find this handbook a useful reference tool and source of information. If you require further information about our products and services please contact your local Ethyl representative.

The information in this handbook is to our best knowledge true and accurate, but all recommendations or suggestions are made without guarantee, since the conditions of use are beyond our control. Ethyl disclaims any liability incurred in connection with the use of this data or suggestions. Furthermore, nothing contained therein shall be construed as a recommendation to use any product in conflict with existing patents covering any materials or its use.

Offices

Regional Offices Bracknell

Richmond

Ethyl Petroleum Additives, Ltd.

330 South Fourth Street

London Road, Bracknell

PO Box 2189

Berkshire RG12 2UW, England

Richmond, VA 23218-2189, USA

Phone: 44-1344-304141

Phone: 804-788-5000

Fax: 44-1344-420666

Fax: 804-788-5688

Singapore

Tokyo

Ethyl Asia Pacific Company

Ethyl Japan Corporation

111 Somerset Road #13-03

19F Shiroyama Hills, 4-chrome-3-1

Singapore 238164

Toranomon, Minato-ku

Phone: 65-732-0822

Tokyo 105-6019, Japan

Fax: 65-737-4123

Phone: 81-3-5401-3234 Fax: 81-3-5401-3368

European Sales Offices Bracknell

Brussels

Ethyl Petroleum Additives, Ltd.

Ethyl Europe, S.A

London Road, Bracknell

Woluwe Garden, Woluwedal 26

Berkshire RG12 2UW, England

1932 St. Stevens Woluwe, Belgium

Phone: 44-1344-304141

Phone: 32-2-715-2211

Fax: 44-1344-420666

Fax: 32-2-715-2210

Hamburg

Paris

Ethyl Mineraloel-Additive GmbH

Succursale d’Ethyl Europe SA

Oberstrasse 14B

33 Quai de Dion Bouton

D-20144 Hamburg, Germany

92814 Puteaux Cedex, France

Phone: 49-40-4292900

Phone: 33-1-46939180

Fax: 49-40-42929032

Fax: 33-1-47788717

Viscosity

Contents

Viscosity

SAE J300 Viscosity Grades for Engine Oils ISO Viscosity Grade Conversions Viscosity Ranges for AGMA Lubricant Numbers Axle and Manual Transmission Lubricant Viscosity Classification • SAE Classification • MIL-L-2105E Specification Comparison of Viscosity Classifications Viscosity Equivalents at Same Temperature Two Components Viscosity Blending Chart (cSt) Base Stocks Viscosities Conversion Factors

SAE J300 Viscosity Grades for Engine Oils - December 1999 SAE Viscosity Grade

Low Temperature (°C) Cranking Viscosity(1), cP Max.

0W 5W 10W 15W 20W 25W 20 30

6200 at 6600 at 7000 at 7000 at 9500 at 13000 at -

-35 -30 -25 -20 -15 -10

Low Temperature (°C) Pumping Viscosity(2), cP Max. with No Yield Stress 60 60 60 60 60 60

000 at 000 at 000 at 000 at 000 at 000 at -

-40 -35 -30 -25 -20 -15

Kinematic Viscosity(3) (cSt) at 100°C Min.

Kinematic Viscosity(3) (cSt) at 100°C Max.

3.8 3.8 4.1 5.6 5.6 9.3 5.6 9.3

< 9.3 < 12.5

2.6 2.9 2.9 (0W-40, 5W-40, and 10W-40 grades)

40

-

-

12.5

< 16.3

40

-

-

12.5

< 16.3

50 60

-

-

16.3 21.9

< 21.9 < 26.1

All values are critical specifications as defined by ASTM D 3244. 1 cP=1 mPa.s; 1 cSt=1 mm2s-1 Notes: (1) ASTM (2) ASTM (3) ASTM (4) ASTM

D D D D

5293. 4684. Note that the presence of any yield stress detectable by this method constitutes a failure regardless of viscosity. 445. 4683, CEC L-36-A-90 (ASTM D 4741), or ASTM D 5481.

04/02 - Viscosity

High-Shear Viscosity(4) (cP) at 150°C and 106 s-1 Min.

3.7 (15W-40, 20W-40, 25W-40, 40 grades) 3.7 3.7

ISO Viscosity Grade Conversions ISO Viscosity Grade

Mid-point Kinematic Viscosity

2 3 5 7 10 15 22 32 46 68 100 150 220 320 460 680 1000 1500

2.2 3.2 4.6 6.8 10 15 22 32 46 68 100 150 220 320 460 680 1000 1500

04/02 - Viscosity

Kinematic Viscosity Limits cSt at 40°C (104°F) Min.

Max.

1.98 2.88 4.14 6.12 9.00 13.5 19.8 28.8 41.4 61.2 90.0 135 198 288 414 612 900 1350

2.42 3.52 5.06 7.48 11.0 16.5 24.2 35.2 50.6 74.8 110 165 242 352 506 748 1100 1650

ASTM, Saybolt Viscosity Number 32 36 40 50 60 75 105 150 215 315 465 700 1000 1500 2150 3150 4650 7000

Saybolt Viscosity SUS 100°F (37.8°C) Min.

Max.

34.0 36.5 39.9 45.7 55.5 72 96 135 191 280 410 615 900 1310 1880 2800 4100 6100

35.5 38.2 42.7 50.3 62.8 83 115 164 234 345 500 750 1110 1600 2300 3400 5000 7500

Viscosity Ranges for AGMA Lubricant Numbers Rust and Oxidation Inhibited Gear Oils

Viscosity Range

AGMA Lubricant No. 1 2 3 4 5 6 7 Compounded 8 Compounded 8A Compounded

cSt (mm2/s) at 40°C 41.4 to 50.6 61.2 to 74.8 90 to 110 135 to 165 198 to 242 288 to 352 414 to 506 612 to 748 900 to 1100

Notes: Viscosity ranges for AGMA Lubricant Numbers will henceforth be identical with those of the ASTM system. Oils compounded with 3% to 10% fatty or synthetic fatty oils.

04/02 - Viscosity

Equivalent ISO Grade

Extreme Pressure Gear Lubricants AGMA Lubricant No.

46 68 100 150 220 320 460 680 1000

2 EP 3 EP 4 EP 5 EP 6 EP 7 EP 8 EP 8A EP

Axle and Manual Transmission Lubricant Viscosity Classification

SAE J306 Automotive Gear Viscosity Classification 70W Viscosity at 100°C min, mm2/s max, mm2/s Viscosity of 150,000 mPa.s, max temp °C 20 hr. KRL Shear (CRC L-45-T-93), KV100 after Shear, mm2/s

85W

80

85

90

140

250

4.1

75W

4.1 7.0 No requirement

80W

11.0

7.0 11.0

11.0 13.5

13.5 24.0

24.0 41.0

41.0 No req.

-55

-40

-26

-12

4.1

4.1

7.0

11.0

24.0

41.0

No requirement 7.0

11.0

13.5

MIL-PRF-2105E Specification Viscosity at 100°C min, mm2/s max, mm2/s Viscosity of 150,000 mPa.s, max temp °C Channel Point, min, °C Flash Point, min, °C

04/02 - Viscosity

75W

80W-90

85W-140

4.1 -

13.5 24.0

24.0 41.0

-40

-26

-12

-45 150

-35 165

-20 180

Approximate Equivalents

Comparison of Viscosity Classifications Kinematic Viscosities cSt/ 40°C cSt/ 100°C 2000 1000 800 600 500 400 300

70 60 50 40 30

60 50 40 30 20 10 8 6 5 4 3 2

04/02 - Viscosity

10000 8000

300

6000 5000 4000

200

10 9 8 7 6

1000 800 600 500 400 300 200

5

150

4

100 80 70 60 50

AGMA Grades SUS @ 100°F

250 8A

680

8 140 7

320 100 90 80 70

50

150

40

100

60 55

68

50

46

45

32

40

6

220

30

90 85W

5 4 3

80W

2

20 1 10W

75W

22 5W 15 10 7

40 3 32

SAE Grades Gear Oils cSt @ 100°C

1500

5

35

SAE Grades Crankcase Oils cSt @ 100°C

460

2000

20

ISO VG cSt @ 40°C

1000

3000

1500

200 100 80

Saybolt Viscosities SUS/ 100°F SUS/ 210°F

2

Viscosities can be related horizontally only. Viscosities based on 95 VI single grade oils. ISO grades are specified at 40°C. AGMA grades are specified at 100°F. SAE 75W, 80W, 85W, and 5W & 10W specified at low temperature. Equivalent viscosities for 100° & 210°F are shown.

Approximate Equivalents

Viscosity Equivalents at Same Temperature Kinematic (Centistokes)

Saybolt Universal (Seconds)

Redwood No.1 (Seconds)

Engler (Degrees)

Saybolt Furol (Seconds)

Redwood No.2 (Seconds)

Kinematic (Centistokes)

Saybolt Universal (Seconds)

Redwood No.1 (Seconds)

Engler (Degrees)

Saybolt Furol (Seconds)

Redwood No.2 (Seconds)

1.8 2.7 4.2 5.8 7.4 8.9 10.3 11.7 13.0 14.3 15.6 16.8 18.1 19.2 20.4 22.8 25.0 27.4 29.6 31.8 34.0 36.0 38.4 40.6 42.8 47.2 51.8 55.9 60.2 64.5 69.9 75.3 80.7 86.1 91.5

32 35 40 45 50 55 60 65 70 75 80 85 90 95 100 110 120 130 140 150 160 170 180 190 200 220 240 260 280 300 325 350 375 400 425

30.8 32.2 36.2 40.6 44.9 49.1 53.5 57.9 62.3 67.6 71.0 75.1 79.6 84.2 88.4 97.1 105.9 114.8 123.6 132.4 141.1 150.0 158.8 167.5 176.4 194.0 212 229 247 265 287 309 331 353 375

1.14 1.18 1.32 1.46 1.60 1.75 1.88 2.02 2.15 2.31 2.42 2.55 2.68 2.81 2.95 3.21 3.49 3.77 4.04 4.32 4.59 4.88 5.15 5.44 5.72 6.28 6.85 7.38 7.95 8.51 9.24 9.95 10.70 11.40 12.10

23.0 25.3 27.0 28.7 30.5 32.5 35.0 37.2 39.5 42.0 44.2

-

96.8 102.2 107.6 118.4 129.2 140.3 151 162 173 183 194 205 215 259 302 345 388 432 541 650 758 866 974 1,082 1,190 1,300 1,405 1,515 1,625 1,730 1,840 1,950 2,055 2,165

450 475 500 550 600 650 700 750 800 850 900 950 1,000 1,200 1,400 1,600 1,800 2,000 2,500 3,000 3,500 4,000 4,500 5,000 5,500 6,000 6,500 7,000 7,500 8,000 8,500 9,000 9,500 10,000

397 419 441 485 529 573 617 661 705 749 793 837 882 1,058 1,234 1,411 1,587 1,763 2,204 2,646 3,087 3,526 3,967 4,408 4,849 5,290 5,730 6,171 6,612 7,053 7,494 7,934 8,375 8,816

12.8 13.5 14.2 15.6 17.0 18.5 19.8 21.3 22.7 24.2 25.6 27.0 28.4 34.1 39.8 45.5 51 57 71 85 99 114 128 142 156 170 185 199 213 227 242 256 270 284

47.0 49 51 56 61 66 71 76 81 86 91 96 100 121 141 160 180 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1,000

104 122 138 153 170 215 255 300 345 390 435 475 515 580 600 645 690 730 770 815 855

04/02 - Viscosity

Two Components Viscosity Blending (cSt)

Component A

0%

10%

20%

30%

40%

50%

60%

70%

80%

90%

100% 4000 3000 2000

1500

1500

1000 800 600 500 400

1000 800 600 500 400

300

300

200

200

150

150

100 90 80 70 60

100 90 80 70 60

50

50

40

40

30

30

20

20

15

15

10 9.0

10 9.0

8.0

8.0

7.0

7.0

6.0

6.0

5.0

5.0

4.0

4.0

3.0

3.0

2.0

2.0 100%

90%

Component B 04/02 - Viscosity

80%

70%

60%

50%

40%

30%

20%

10%

0%

Viscosity Centistrokes

Viscosity Centistrokes

4000 3000 2000

Approximate Equivalents

Base Stocks Viscosities Neutrals 40°C 70N 80N 90N 100N 140N 150N 160N 170N 180N 200N 250N 300N 315N 330N 350N 400N 450N 500N 600N 650N 700N

cSt 13.3 15.6 18.0 21.5 30.7 31.6 33.7 34.0 38.5 44.5 56.1 61.3 70.0 70.9 76.0 86.0 98.0 107.0 130.4 141.0 151.0

100°C SUS 70.8 80.3 89.0 104.0 144.0 148.0 158.0 159.0 181.0 204.0 257.0 285.0 315.0 328.0 358.0 398.6 454.0 496.0 604.0 665.0 668.0

cSt 3.0 3.35 3.4 4.0 4.5 4.9 5.2 5.4 5.7 6.2 6.5 7.0 7.9 8.4 8.8 9.8 10.5 11.0 12.1 13.8 14.0

SUS 37.0 37.3 37.5 39.0 41.0 42.4 43.3 44.0 44.9 46.0 47.0 49.0 52.0 53.7 55.0 58.0 61.0 64.0 66.0 71.0 73.0

Brights 40°C 135 145 150 160 175 185 225

04/02 - Viscosity

Brt Brt Brt Brt Brt Brt Brt

cSt 413.2 523.3 568.0 600.0 616.0 654.7 1030.0

100°C SUS 1875.0 2425.0 2632.0 2800.0 2855.0 3034.0 4800.0

cSt 28.6 30.9 33.0 35.2 36.0 37.6 49.3

SUS 135.0 145.0 155.0 166.0 169.7 177.0 229.0

Conversion Factors

Linear Measurement

1 1 1 1 1 1 1 1

yd m ft m in cm mile km

= = = = = = = =

0.9144 m 1.0936 yd 0.3048 m 3.28 ft 2.54 cm 0.3937 in 1.6093 km 0.6214 mile

Area Measurement

1 1 1 1

sq sq sq sq

yd m in cm

= = = =

0.8361 sq m 1.1960 sq yd 6.452 sq cm 0.155 sq in

Cubic Measurement

1 1 1 1 1 1

cu cc cu cu cu cu

in ft m yd m

= = = = = =

16.3872 cc 0.0610 cu in 0.02832 cu m 35.314 cu ft 0.7646 cu m 1.3079 cu yd

Volumetric Measurement

1 1 1 1

imp gall litre imp gall litre

= = = =

4.54596 litre 0.21998 imp gall 1.201 US gall 1.76 pints

Weight Measurement

1 1 1 1

oz g lb kg

= = = =

28.3495 g 0.03527 oz 453.59 g 2.20462 lbs

Weights per Volume

1 1 1 1

g/litre oz/imp gall g/litre lb/imp gall

= = = =

0.16035 oz/imp gall 6.236 g/litre 0.01002 lb/imp gall 99.8003 g/litre

Temperature Conversions Gravity Conversion Weight/Volume Conversion (for additive blending)

°C °F

= (°F - 32) x 5/9 = (°C x 9/5) + 32

API gravity, deg

= (141.5/sp.gr. @ 60/60°F) - 131.5

% volume of additive

= % weight of additive x density of finished oil density of additive (typical finished oil density = 0.88 g/ml)

04/02

Viscosity

Crankcase

Contents

Crankcase

API Service Classification API Commercial Classification API Gasoline Engine Performance Criteria API Diesel Engine Performance Criteria ACEA 2002 Service Fill Oils for: Gasoline Engines Light Duty Diesel Engines Heavy Duty Diesel Engines ILSAC Specifications: GF-1 GF-2 GF-3 US Military Specifications: Engine Test Requirements Japanese Automotive Diesel Engine Oil Standard: JASO DH-1 Global Performance Specification for Diesel Engine Oil: Global DHD-1 Two-Stroke Classifications: API TC ISO/JASO TISI 1040 NMMA TC-W3 OEM Specifications: Mercedes-Benz Engine Test Requirements for Diesel Engine Oils Mercedes-Benz Sheet 229.1 for Passenger Car Engine Oils Mercedes-Benz Sheet 229.3 for Passenger Car Engine Oils Mercedes-Benz Sheet 229.5 for Passenger Car Engine Oils MAN 270, MAN 271 Specifications MAN M 3275 Specification MAN M 3277 Specification Volkswagen 500.00, 501.01, 505.00, 502.00 Specifications Volkswagen 503.00, 506.00 Specifications

Contents

Crankcase

Volvo Drain Specifications: VDS VDS-2 VDS-3 MTU MTL 5044 Mack EO-K/2 Mack EO-L / EO-L Plus Mack EOM / EOM Plus Cummins 20071 / 20072 Cummins 20076 / 20077 European OEM Seal Test Requirements for Automotive Engine Oils

API Service Classification “S” Service

“S” Service - (Service Stations, Garages, New Car Dealers etc.) The following descriptions of the categories in the API Engine Service Classification System are intended as guides to aid in the selection of proper engine oils for significantly different engine service conditions. The performance requirements for these categories are technically described in SAE J183-June 1991, Engine Oil Performance and Engine Service Classification (except for SH). SA

Formerly for Utility Gasoline and Diesel Engine Service Service typical of older engines operated under such mild conditions that the protection afforded by compounded oils is not required. This category should not be used in any engine unless specifically recommended by the equipment manufacturer.

SB

For Minimum Duty Gasoline Engine Service Service typical of older gasoline engines operated under such mild conditions that only minimum protection afforded by compounding is desired. Oils designed for this service have been used since the 1930’s and provide only antiscuff capability and resistance to oil oxidation and bearing corrosion. They should not be used in any engine unless specifically recommended by the equipment manufacturer.

SC

For 1964 Gasoline Engine Warranty Maintenance Service Service typical of gasoline engines in 1964 through 1967 models of passenger cars and some trucks operating under engine manufacturers’ warranties in effect during those model years. Oils designed for this service provide control of high and low temperature deposits, wear, rust and corrosion in gasoline engines.

SD

For Gasoline Engine Warranty Maintenance Service Service typical of gasoline engines in 1968 through 1970 models of passenger cars and some trucks operating under engine manufacturers’ warranties in effect during those model years. Also may apply to certain 1971 and/or later models as specified (or recommended) in the owners’ manuals. Oils designed for this service provide more protection against high and low temperature engine deposits, wear, rust and corrosion in gasoline engines than oils which are satisfactory for API Engine Service Category SC and may be used when API Engine Service Category SC is recommended.

SE

For 1972 Gasoline Engine Warranty Service Service typical of gasoline engines in passenger cars and some trucks beginning with 1972 and certain 1971 models operating under engine manufacturers’ warranties. Oils designed for this service provide more protection against oil oxidation, high temperature engine deposits, rust and corrosion in gasoline engines than oils which are satisfactory for API Engine Service Categories SD or SC and may be used when either of these classifications is recommended.

04/02

Crankcase

API Service Classification “S” Service

SF

For 1980 Gasoline Engine Warranty Maintenance Service Service typical of gasoline engines in passenger cars and some trucks beginning with the 1980 model year operating under manufacturers’ recommended maintenance procedures. Oils developed for this service provide increased oxidation stability and improved anti-wear performance relative to oils which meet the minimum requirements for API Service Category SE. The oils also provide protection against engine deposits, rust and corrosion. Oils meeting API Service Classification SF may be used where API Service Categories SE, SD or SC are recommended. Oils meeting the performance requirements measured in the following gasoline engine tests: The IID gasoline engine test has been correlated with vehicles used in short-trip service prior to 1978, particularly with regard to rusting. The IIID gasoline engine test has been correlated with vehicles used in high temperature service prior to 1978, particularly with regard to oil thickening and valve train wear. The V-D gasoline engine test has been correlated with vehicles used in stop-and-go service prior to 1978, particularly with regard to varnish, sludge and valve train wear. The L-38 gasoline engine test requirement provides a measurement of copper-lead bearing weight loss under high-temperature operating conditions.

SG

For 1989 Gasoline Engine Warranty Maintenance Service Service typical of gasoline engine in passenger cars, vans and light trucks beginning with the 1989 model year operating under manufacturers’ recommended maintenance procedures. Category SG quality oils include the performance properties of API service category CC. (Certain manufacturers of gasoline engines require oils also meeting API Category CD). Oils developed for this service provide improved control of engine deposits, oil oxidation and engine wear relative to oils developed for previous categories. These oils also provide protection against rust and corrosion. Oils meeting API Service Category SG may be used where API Service Categories SF, SF/CC, SE or SE/CC are recommended. Oils meeting the performance requirements measured in the following gasoline and diesel engine tests:

• • • • •

04/02

The IID gasoline engine test has been correlated with vehicles used in short-trip service prior to 1978, particularly with regard to rusting. The IIIE gasoline engine test has been correlated with vehicles used in high-temperature service prior to 1988, particularly with regard to oil thickening and valve train wear. The VE gasoline engine test has been correlated with vehicles used in stop-and-go service prior to 1988, particularly with regard to sludge and valve train wear. The L-38 gasoline engine test requirement provides a measurement of copper-lead bearing weight loss and piston varnish under high temperature operating conditions. The 1-H2 diesel engine test requirement provides a measurement of high-temperature deposits.

Crankcase

API Service Classification “S” Service

SH

For 1992 Gasoline Engine Warranty Maintenance Service Category SH covers the performance requirements of SG oils tested to the latest CMA protocol on engine testing. In addition, SH oils must meet various bench test requirements including volatility, filterability and foaming tests.

SJ

For 1997 Gasoline Engine Warranty Maintenance Service API Service Category SJ was adopted for use in describing engine oils available in 1996. These oils are for use in service typical of gasoline engines in current and earlier passenger-car, sport utility vehicle, van, and light truck operations under vehicle manufacturers’ recommended maintenance procedures. Engine oils that meet API Service Category SJ designation may be used where API Service Category SH and earlier Categories have been recommended. Engine oils that meet the API Service Category SJ designation have been tested in accordance with the CMA Code, may use the API Base Oil Interchangeability Guidelines and the API Guidelines for SAE ViscosityGrade Engine Testing. Engine oils that meet these requirements may display API Service Category SJ in the upper portion of the API Service Symbol.

SL

For 2001 Gasoline Engine Warranty Maintenance Service API Service Category SL was adopted for use in describing engine oils available in 2001. These oils are for use in service typical of gasoline engines in current and earlier passenger cars, sport utility vehicles, vans, and light-duty trucks operating under vehicle manufacturers’ recommended maintenance procedures. Engine oils that meet API Service Category SL designation may be used where API Service Category SJ and earlier Categories have been recommended. Engine oils that meet the API Service Category SL designation have been tested in accordance with the ACC Code and may use the API Base Oil Interchangeability Guidelines and the API Guidelines for SAE Viscosity-Grade Engine Testing. Starting July 1, 2001, engine oils that meet these requirements may display API Service Category SL in the upper portion of the API Service Symbol.

04/02

Crankcase

API Commercial Classification “C” Commercial

“C” Commercial - (Fleets, Contractors, Farmers, etc.) CA

For Light Duty Diesel Engine Service Service typical of diesel engine operated in mild to moderate duty with highquality fuels and occasionally has included gasoline engines in mild service. Oils designed for this service provide protection from bearing corrosion and from ring belt deposits in some naturally aspirated diesel engines when using fuels of such quality that they impose no unusual requirements for wear and deposit protection. They were widely used in the late 1940’s and 1950’s but should not be used in any engine unless specifically recommended by the equipment manufacturer.

CB

For Moderate Duty Diesel Engine Service Service typical of diesel engines operated in mild to moderate duty, but with lower-quality fuels which necessitate more protection for wear and deposits. Occasionally has included gasoline engines in mild service. Oils designed for this service provide necessary protection from bearing corrosion and from ring belt deposits in some naturally aspirated diesel engines with higher sulphur fuels. Oils designed for this service were introduced in 1949.

CC

For Moderate Duty Diesel and Gasoline Engine Service Service typical of many naturally aspirated diesel engines operated in moderate to severe-duty service and certain heavy-duty gasoline engines. Oils designed for this service provide protection from high temperature deposits and bearing corrosion and low temperature deposits in gasoline engines. These oils were introduced in 1961.

CD

For Severe Duty Diesel Engine Service Service typical of certain naturally aspirated, turbocharged or supercharged diesel engines where highly effective control of wear and deposits is vital, or when using fuels of a wide quality range including high sulphur fuels. Oils designed for this service were introduced in 1955 and provide protection from bearing corrosion and from high temperature deposits in these diesel engines. Oil meeting the performance requirements measure in the following diesel and gasoline engine tests: The 1-G2 diesel engine test has been correlated with indirect injection engines used in heavy-duty operation, particularly with regard to piston and ring groove deposits. The L-38 gasoline engine test requirement provides a measurement of copper-lead bearing weight loss and piston varnish under high-temperature operating conditions.

04/02

Crankcase

API Commercial Classification “C” Commercial

CD-II

For Severe Duty 2-Stroke Diesel Engine Service Service typical of 2-stroke cycled engines requiring highly efficient control over wear and deposits. Oils designed for this service also meet the performance requirements of API service category CD. Oils meeting the performance requirements measured in the following diesel and gasoline engine tests: The 1-G2 diesel engine test has been correlated with indirect injection engines used in heavy-duty operation, particularly with regard to piston and ring groove deposits. The 6V-53T diesel engine test has been correlated with vehicles equipped with two-stroke cycle diesel engines in high-speed operation prior to 1985, particularly with regard to ring and liner distress. The L-38 gasoline engine test requirement provides a measurement of copper-lead bearing weight loss and piston varnish under high-temperature operating conditions.

CE

For High Performance Diesel Engine Service Service typical of many turbocharged or supercharged high performance diesel engines, operated under both low speed - high load and high speed - high load conditions. Oils designed for this service have been available since 1984 and provide improved control of oil consumption, oil thickening and piston assembly deposits and wear relative to the performance potential offered by oils designed for Category CD Service. Oils meeting the performance requirements of the following diesel and gasoline engine tests: The 1-G2 diesel engine test has been correlated with indirect injection engines used in heavy-duty service, particularly with regard to piston and ring groove deposits. The T-6, T-7 and NTC-400 are direct injection diesel engine tests. The T-6 has been correlated with vehicles equipped with engines used in high-speed operation prior to 1980, particularly with regard to deposits, oil consumption and wear. The T-7 test has been correlated with vehicles equipped with engines used in lugging operation prior to 1984, particularly with regard to oil thickening. The NTC-400 diesel engine test has been correlated with vehicles equipped with engines in highway operation prior to 1983, particularly with regard to oil consumption, deposits and wear. The L-38 gasoline engine test requirement provides a measurement of copper-lead bearing weight loss under high-temperature operating conditions.

04/02

Crankcase

API Commercial Classification “C” Commercial

CF

For Indirect Injected Diesel Engine Service API Service Category CF denotes service typical of indirect injected diesel engines, and other diesel engines which use a broad range of fuel types including those using fuel with higher sulphur content, for example, over 0.5% wt. Effective control of piston deposits, wear and copper - containing bearing corrosion is essential for these engines which may be naturally aspirated, turbocharged or supercharged. Oils designated for this service have been in existence since 1994. Oils designated for this service may also be used when API service category CD is recommended.

CF-2

For Two-Stroke Cycle Diesel Engine Service API Service category CF-2 denotes service typical of two-stroke cycle engines requiring highly effective control over cylinder and ring-face scuffing and deposits. Oils designated for this service have been in existence since 1994 and may also be used when API Service Category CD-II is recommended. These oils do not necessarily meet the requirements of CF or CF-4 unless passing test requirements for these categories.

CF-4

For High Performance Diesel Engine Service This category was adopted in 1990 and describes oils for use in high speed, four-stroke diesel engines. API CF-4 oils exceed the requirements of the CE category, providing improved control of oil consumption and piston deposits. Oils meeting the performance requirements in the following diesel and gasoline engine tests: The T-6, T-7, NTC 400 and L-38 engines: See API CE Category above for explanation. The 1K diesel engine test, which has been correlated with direct injection engines used in heavy-duty service prior to 1990, particularly with regard to piston and ring groove deposits. It has been demonstrated that the 1K test, in combination with test method D5968, the bench corrosion test, can be substituted for the NTC-400 test as an acceptable means to demonstrate performance against this category. Test method D6483, the T-9 diesel engine test can be used as an alternate for the T-6 test and its limits. Test method D5967, the F8A version, and its limits can be used as an alternate for the T-7 test and its limits.

04/02

Crankcase

API Commercial Classification “C” Commercial

CG-4

For Severe Duty Diesel Engine Service API Service Category CG-4 describes oils for use in high speed four stroke-cycle diesel engines used on both heavy-duty on-highway (less than 0.05% wt. sulphur fuel) and off highway (less than 0.5% wt. sulphur fuel) applications. CG-4 oils provide effective control over high temperature piston deposits, wear, corrosion, foaming, oxidation stability and soot accumulation. These oils are especially effective in engines designed to meet 1994 exhaust emission standards and may also be used in engines requiring API Service Categories CD, CE and CF-4. Oils designated for this service have been in existence since 1994.

CH-4

For 1998 Severe Duty Diesel Engine Service API Service Category CH-4 describes oils for use in high-speed, four-stroke diesel engines designed to meet 1998 exhaust emissions standards as well as for previous model years. CH-4 oils are specifically compounded for use with diesel fuels ranging in sulphur content up to 0.5 percent weight. These oils are especially effective to sustain engine durability even under adverse applications that may stress wear control, high temperature stability, and soot handling properties. In addition, optimum protection is provided against non-ferrous corrosion, oxidative and insoluble thickening, foaming, and viscosity loss due to shear. These oils also have the performance capability to afford a more flexible approach to oil drain intervals in accordance with the recommendations of the individual engine builders for their specific engines. CH-4 oils are superior in performance to those meeting API CF-4 and API CG-4 and can effectively lubricate engines calling for those API Service Categories.

04/02

Crankcase

API Gasoline Engine Performance Criteria Test

Primary Performance Criteria

SA

None

None

SB

L-4 or L-38 Sequence IV

SC

Sequences IIA and IIIA

Bearing Weight Loss, mg. max. Cam Scuffing Lifter Scuff Rating, max. Cam and Lifter Scuffing Avg. Cam plus Lifter Wear, in. max. Avg. Rust Rating, min. Avg. Sludge Rating, min. Avg. Varnish Rating, min. Cam Scuffing Lifter Scuff Rating, max. Total Engine Sludge Rating, min. Avg. Piston Skirt Varnish Rating, min. Total Engine Varnish Rating, min. Avg. Intake Valve Tip Wear, in. max. Ring Sticking Oil Ring Clogging, %. max. Oil Screen Plugging, %. max. Bearing Weight Loss, mg. max. Top Groove Filling, % vol. max. Second Groove and Below Cam and Lifter Scuffing Avg. Cam and Lifter Wear, in. max. Avg. Rust Rating, min. Avg. Sludge Rating, min. Avg. Varnish Rating, min. Cam Scuffing Lifter Scuff Rating, max. Total Engine Sludge Rating, min. Avg. Piston Skirt Varnish Rating, min. Total Engine Varnish Rating, min. Avg. Intake Valve Tip Wear, in. max. Oil Ring Clogging, %. max. Oil Screen Plugging, %. max. Bearing Weight Loss, mg. max.

Sequence IV Sequence V

SD

L-38 L-1 (0.95% min. sulphur fuel) Sequences IIB and IIIB

Sequence IV Sequence VB

L-38 L-1(0.95% min. S. fuel) or 1-H Falcon

04/02 - Crankcase

Top Groove Filling, % vol. max. Second Groove and Below Weighted Total Demerits Avg. Engine Rust Rating, min.

Limits L-4 500 None 2 None 0.0025 8.2 9.5 9.7 None 2 40 7.0 35 0.0020 None 20 20 50 25 Clean None 0.0030 8.8 9.6 9.6 None 1 42.5 8.0 37.5 0.0015 5 5 40 L-1 25 9

L-38 500

1-H 30 Clean 140

API Gasoline Engine Performance Criteria Test SE

Primary Performance Criteria

Sequence IIC or IID Avg. Engine Rust Rating, min. Lifter Sticking Sequence IIIC or IIID Viscosity Increase @ 100°F. and 40 test hrs, %. max. Viscosity Increase @ 40°C. and 40 test hrs, %. max. Avg. Piston Skirt Varnish Rating, min. Ring Land Face Varnish Rating, min. Avg. Sludge Rating, min. Ring Sticking Lifter Sticking Cam & Lifter Scuffing Cam & Lifter Wear, in. average Cam & Lifter Wear, in. max. Sequence VC or VD

SF

CRC L-38 Sequence IID Sequence IIID

Sequence VD

CRC L-38 Note: * Suggested performance - not pass/fail limit.

04/02 - Crankcase

Avg. Engine Sludge Rating, min. Avg. Piston Skirt Varnish Rating, min. Avg. Engine Varnish Rating, min. Oil Ring Clogging, %. max. Oil Screen Plugging, %. max. Compression Ring Sticking Cam Wear, in. average Cam Wear, in. max. Bearing Weight Loss, mg. max. Avg. Engine Rust Rating, min. Lifter Sticking Viscosity Increase at 40°C. and 64 test hrs, %. max. Avg. Piston Skirt Varnish Rating, min. Ring Land Face Varnish Rating, min. Avg. Sludge Rating, min. Ring Sticking Lifter Sticking Cam & Lifter Scuffing Cam & Lifter Wear, in. average Cam & Lifter Wear, in. max. Avg. Engine Sludge Rating, min. Avg. Piston Skirt Varnish Rating, min. Avg. Engine Varnish Rating, min. Oil Ring Clogging, %. max. Oil Screen Plugging, %. max. Compression Ring Sticking Cam Wear, in. average Cam Wear, in. max. Bearing Weight Loss, mg. max.

IIC 8.4 None IIIC

IID 8.5 None IIID

400

-

-

375

9.3 6.0 9.2 None None None 0.0010 0.0020 VC 8.7 7.9 8.0 5 5 None 40 8.5 None

9.1 4.0 9.2 None None None 0.0040 0.0100 VD 9.2 6.4 6.3 10 10 None 0.0020* 0.0040*

375 9.2 4.8 9.2 None None None 0.0040 0.0080 9.4 6.7 6.6 10 7.5 None 0.0010 0.0025 40

API Gasoline Engine Performance Criteria

SG

Test

Primary Performance Criteria

Sequence IID

Avg. Engine Rust Rating, min. Lifter Sticking Viscosity Increase at 40°C. and 64 test hrs, %. max. Avg. Piston Skirt Varnish Rating, min. Avg. Sludge Rating, min. Ring Land Face Varnish Rating, min. Ring Sticking Lifter Sticking Cam & Lifter Scuffing Cam & Lifter Wear, µm. average Cam & Lifter Wear, µm. max. Avg. Engine Sludge Rating, min. Rocker Arm Cover Sludge Rating, min. Avg. Piston Skirt Varnish Rating, min. Avg. Engine Varnish Rating, min. Oil Ring Clogging, %. max. Oil Screen Plugging, %. max. Compression Ring Sticking Cam Wear, µm. average Cam Wear, µm. max. Bearing Weight Loss, mg. max. Top Groove Filling, % vol. max. Weighted Total Demerits

Sequence IIIE

Sequence VE

CRC L-38 1H2 SH

Sequence IID Sequence IIIE Sequence VE CRC L-38 SAE (J300) CEC L-40-A-93/ L-40-T-87 (Noack), % Phosphorus, % m. Flash Point (ASTM D92), °C. Foaming (Tendency/Stability) Sequence I, max. Sequence II, max. Sequence III, max. Sequence IV Homogeneity/Miscibility GM EOFT Filterability, Flow Reduction, %

04/02 - Crankcase

8.5 None 375 8.9 9.2 3.5 None None None 30 64 9.0 7.0 6.5 5.0 15 20 None 122 381 40 45 140

API SG limits apply Tested according to CMA Code of Practice 5W30

10W30

15W40

All Others

25 max.

20 max.

18 max.

-

0.12 max.

0.12 max.

-

-

200 min.

205 min.

215 min.

-

10/0 50/0 10/0 Report Pass

10/0 50/0 10/0 Report Pass

10/0 50/0 10/0 Report Pass

-

50 max.

50 max.

-

-

API Gasoline Engine Performance Criteria Test SJ

04/02 - Crankcase

Sequence IID Sequence IIIE Sequence VE CRC L-38 SAE (J300) CEC L-40-A-93/ L-40-T-87 (Noack), % Phosphorus, % m. Flash Point (ASTM D92), °C. Foaming (Tendency/Stability) Sequence I, max. Sequence II, max. Sequence III, max. High Temp. (ASTM 1392), max. Homogeneity/Miscibility GM EOFT Filterability, Flow Reduction, % High Temp. Deposits (TEOST) mg. Gelation Index

Primary Performance Criteria API SG limits apply Tested according to CMA Code of Practice 0W20, 5W20, 5W30, 10W30

All Others

22 max.

20 max.

0.10 max.

-

200 min. 205 min. (10W-30)

-

10/0 50/0 10/0

10/0 50/0 10/0

200/50

200/50

Pass

Pass

50 max.

50 max.

60 max.

60 max.

12 max.

-

API Gasoline Engine Performance Criteria

SL

Test

Primary Performance Criteria

ASTM Ball Rust Test Sequence IIIF

Avg. Grey Value, min. Viscosity Increase (KV 40°C), %. max. Avg. Piston Skirt Varnish, min. Weighted Piston Demerit Rating, min. Hot Stuck Piston Rings Avg. Cam and Lifter Wear, µm. max. Oil Consumption Low Temp. Viscosity Cam Wear Average µm. max. Cam Wear Average µm. max. Avg. Cam Wear µm, max. Avg. Engine Sludge Rating, min. Rocker Cover Sludge Rating, min. Average Engine Varnish Rating, min. Average Piston Skirt Varnish, min. Oil Screen Clogging, max. Hot Stuck Compression Ring Cold Stuck Rings Oil Screen Debris (%) Oil Ring Clogging Bearing Wt. Loss, mg. max.

100 275 9.0 4.0 None 20 5.2 Report (1) 127 380 120 7.8 8.0 8.9 7.5 20 None Rate & Report Rate & Report Rate & Report 26.4

15

15

10

10

0W20, 5W20, 5W30, 10W30 0.10 max.

All Others -

200 min. 205 min. (10W-30)

-

10/0 50/0 10/0

10/0 50/0 10/0

100/10

100/10

Pass

Pass

50

50

45

45

12

-

Stay-in-grade

Stay-in-grade

Sequence VE (2) Sequence IVA Sequence VG

Sequence VIII Volatility Loss ASTM D5800, %. max. Volatility Loss at 37°C ASTM D6417, %. max. SAE (J300) Phosphorus, % m. Flash Point (ASTM D92), °C. Foaming (Tendency/Stability) Sequence I, max. Sequence II, max. Sequence III, max. High Temp. (ASTM 1392), max. Homogeneity/Miscibility GM EOFT Filterability, Flow Reduction, %. max. High Temp. Deposits (TEOST) mg. max. Gelation Index, max. Shear Stability - Seq. VIII 10hr. Stripped KV100°C.

Limits

Notes: (1) The 80 hour test sample shall be evaluated by test method D4684 (MRV TP-1) at the temperature indicated by the low-temperature grade of oil as determined on the 80 hour sample by test method D5293 (CCS Viscosity). (2) Not required for oils containing a minimum of 0.08% phosphorus in the form of ZDDP.

04/02 - Crankcase

API Diesel Engine Performance Criteria Test

L-38

Bearing Weight Loss, mg. max. Piston Skirt Varnish Rating, min. Top Groove Filling, % vol. max. Second Groove and below Same as CA Same as CA, except Top Groove Filling, % vol. max.

120-135 9.0

50 9.0

L-38

Bearing Weight Loss, mg. max. Piston Skirt Varnish Rating, min.

LTD or Modified LTD

Piston Skirt Varnish Rating, min. Total Engine Varnish Rating, min. Total Engine Sludge Rating, min. Oil Ring Plugging, %. max. Oil Screen Clogging, %. max.

IIC or IID 1-H2

Avg. Engine Rust Rating, min. Top Groove Fill, % vol. max. Weighted Total Demerits, max. Ring Side Clearance Loss, in. max. Top Groove Fill, % vol. max. Weighted Total Demerits, max. Ring Side Clearance Loss, in. max. Bearing Weight Loss, mg. max. Piston Skirt Varnish Rating, min. Top Groove Fill, % vol. max. Weighted Total Demerits, max. Ring Side Clearance Loss, in. max. Bearing Weight Loss, mg. max. Piston Varnish Rating, min. Piston Area Weighted Total Demerits, avg. max. Hot Stuck Rings 2 and 3 Ring Face Distress avg. Demerits, max.

50 9.0 LTD 7.5 35 25 25 IIC 7.6 45 140 0.0005 80 300 0.0005 50 9.0 80 300 0.0005 50 9.0

L-4 or L-38

CB

L-1 (0.35% min. sulphur fuel) L-4 or L-38 L-1 (0.95% min. sulphur fuel)

CD

1-G2

L-38 CD-II

I-G2

L-38 6V-53T

Liner and Head Area Liner Distress, avg. % Area, max. Valve Distress

04/02 - Crankcase

Limits L-4

CA

CC

Primary Performance Criteria

25 Essentially clean

30

400 None 13

12 None

Mod LTD 7.5 42 42 10 10 IID 7.7

API Diesel Engine Performance Criteria CE

Test

Primary Performance Criteria

Limits

1G2

Top Groove Fill, % vol. max. Weighted Total Demerits, max. Ring Side Clearance loss, in. max. Bearing Weight Loss, mg. max. Merit Rating, min. Avg. Rate of Viscosity increase during last 50 hrs, cSt. 100°C/hr. max.

80 300 0.0005 50 90

L-38 T-6 T-7 NTC-400

Oil Consumption

Camshaft Roller Follower Pin Wear average, max. mm. (in). Crownland (Top Land) Deposits, % area covered with heavy carbon, average, max. Piston Deposits, Third Ring Land, total CRC demerits for all six pistons, max.

04/02 - Crankcase

0.040 Candidate oil consumption second order regression curve must fall completely below the published mean plus one standard deviation curve for the applicable reference oil 0.051 (0.002) 25

40

API Diesel Engine Performance Criteria Test

Primary Performance Criteria

CF

1M-PC

CF-2

L-38 1M-PC 6V-92TA

Top Groove Filling (TGF), % vol. max. Weighted Total Demerits (WTD), max. Ring Side Clearance Loss, mm. max. Piston Ring Sticking Piston, Ring and Liner Scuffing Bearing Weight Loss, mg. max. Weighted Total Demerits (WTD), max. Cylinder Line Scuffing, %. max. Port Plugging, %. max. Average Single Cylinder Piston Ring Face Distress Demerits, max. No. 1 (Fire Ring) Avg. No. 2 & 3 Bearing Weight Loss, mg. max. A 1-K test programme with a minimum of two tests, acceptable to the limits shown in the columns to the right, is required to demonstrate performance for this category Weighted Demerits (WDK), max. Top Groove Carbon Fill (TGF), % vol. max. Top Land Heavy Carbon (TLHC), %. max. Avg. Oil Consumption, g/kW-h. (0-252hr) max. Final Oil Consumption, g/kW-h. (228-252hr) max. Scuffing, (piston-rings-liner)

CF-4

L-38 1-K

T6 or T9 (D6483) T7 or T8A (D5967) L-38 CBT (D5968)

Merit Rating (*), min. or Top Piston Ring wt. loss, avg. mg. max. Linear Wear, µm. max. Average rate of KV inc. during last 50hrs. max. or Average rate of KV inc. 100-150 hrs. max. Bearing Weight Loss, mg. max. Copper, mg/kg. (ppm) increase, max. Lead, mg/kg. (ppm) increase, max. Tin, mg/kg. (ppm) increase, max. Copper Corrosion, max.

Note: * Requires greater than zero unit on all individual rating.

04/02 - Crankcase

Number of Test Runs 1

2

3

70 240 0.013 None None 43.7 100 45.0

70 240 0.013 None None 48.1 100 48.0

70 240 0.013 None None 50.0 100 50.0

2 5

2 5

2 5

0.23 0.20 43.7

0.24 0.21 48.1

0.26 0.22 50.0

Number of Test Runs 2 3 4 332 339 342 24 26 27 4 4 5 0.5 0.5 0.5 0.27 0.27 0.27 None None None Limits (1 test) 90 150 40 0.040 0.20 50 20 60 Report 3

API Diesel Engine Performance Criteria Test CG-4

1N

Primary Performance Criteria WDN (Weighted Demerits-1N), avg. max. TGF (Top Groove Fill), % vol. avg. max. TLHC (Top Land Heavy Carbon), % avg. max.

T-8

IIIE L-38

6.2L Foam

Bench Corrosion Test

Oil Consumption, g/kW-h. avg. max. Scuffing, Piston-Rings-Liner Number of Tests Allowed Stuck Rings Viscosity Increase @ 3.8% soot, cSt. avg. max. Filter Plugging, Differential Pressure, kPa. avg. max. Oil Consumption, g/kW-h. avg. max. Hours to 375% Viscosity Increase, avg. min. Bearing Weight Loss, mg. avg. max. Used Oil Viscosity, cSt. greater than SAE J300 lower limit for Grade, avg. min. Wear, µm. (mils), avg. max. Foaming/Settling, ml. max. Sequence I Sequence II Sequence III ppm. Increase, max. Copper Lead Tin Copper Corrosion, max. D130

Note: Limits do not apply to monograde oils

04/02 - Crankcase

Number of Test Runs 1

2

3

286.2

311.7

323.0

20

23

25

3

4

5

0.5

0.5

0.5

None None

None None

None None

11.5

12.5

13.0

138

138

138

0.304

0.304

0.304

67.5

65.1

64.0

43.7

48.1

50.0

0.5

0.5

0.5

11.4 (0.45) 12.4 (0.49) 12.7 (0.50) 10/0 20/0 10/0 20 60 50 3

API Diesel Engine Performance Criteria Test

Primary Performance Criteria

1P

WDP (Weighted Demerits - 1P), max. TGC (Top Groove Carbon), % vol. max. TLC (Top Land Carbon), %. max. Avg. Oil Consumption, 0-360 hours Final Oil Consumption, 336-360 hours Crosshead Weight Loss, 4.5% soot mg. max. Sludge, min. Differential Pressure/Oil Filter, kPa. max. Avg. Liner Wear, µm. max. Top Ring Weight Loss, mg. max. Increase in Lead Content, ppm. max. Viscosity Increase, 3.8% soot cSt. max. Relative Viscosity, 4.8% soot max. WDK (Weighted Demerits - 1K), max. TGF (Top Groove Fill), % vol. max. TLHC (Top Land Heavy Carbon), %. max. Oil Consumption, g/bhp-hr. max. Piston, Ring and Liner Scuffing Pin Wear, mils. max. Viscosity Increase, %. max. Aeration Volume, %. max. Copper, ppm. Increase, max. Lead, ppm. Increase, max. Tin, ppm. Increase, max. Copper Corrosion, ASTM D130. max.

Number of Test Runs 1

CH-4

M-11

T-9

T8-E 1K

6.5L IIIE HEUI Bench Corrosion

04/02 - Crankcase

350 36 40

6.5 8.7 79 25.4 120 25 11.5 2.1 332 24 4 0.5 None 0.30 200 8.0 20 120 50 3

2

3

378 390 39 41 46 49 11.0 max./test 10.0 max./test 7.5 8.0 8.6 8.5 93 100 26.6 27.1 136 144 32 36 12.5 13.0 2.2 2.3 347 353 27 29 5 5 0.5 0.5 None None 0.33 0.36 200 200 8.0 8.0 20 20 120 120 50 50 3 3

Laboratory Tests

ACEA 2002 Service Fill Oils for Gasoline Engines Requirements

Method

Properties Unit

Limits

1.1

Viscosity Grade

1.2

Shear Stability

CEC L-14-A-93 (Bosch injector)

Viscosity after 30 cycles measured at 100°C.

1.3

Viscosity High Temperature High Shear Rate Evaporative Loss (Noack)

CEC L-36-A-97 (Ravenfield)

Viscosity at 150°C. and 106s-1 shear rate

CEC L-40-A-93

Max. weight loss after 1hr. at 250°C.

1.5

Sulphated Ash

ASTM D874

1.6 1.7 1.8 1.9

Sulphur Phosphorus Chlorine Oil/Elastomer Compatibility See Notes (1)

1.4

SAE J 300 Latest active issue

CEC L-39-T-96

Max. variation of characteristics after immersion for 7 days in fresh oil without pre-ageing Hardness DIDC Tensile strength Elongation rupture Volume variation

A1-02 A2-96 Issue 3 A3-02 A5-02 No restriction except as defined by shear stability and HTHS requirements. Manufacturers may indicate specific viscosity requirements related to ambient temperatures. XW-20: stay-in-grade XW-30 ≥ 8.6 XW-30 ≥ 9.0 mm2/s. All grades to be All grades to be XW-40 ≥ 12.0 XW-40 ≥ 12.0 stay-in-grade stay-in-grade XW-50 ≥ 15.0 max 3.5 min 2.9 mPa.s XW-20 min 2.6 > 3.5 > 3.5 max 3.5 All others min 2.9 ≤ 15 for 10W-X % ≤ 15 or lower. ≤ 13 ≤ 13 ≤ 13 for others % m/m ≤ 1.3 ≤ 1.5 ≤ 1.5 ≤ 1.5 The following sections apply to all Sequences ppm m/m Report ppm m/m Report ppm m/m Report Elastomer type points % % %

1.10 Foaming Tendency

ASTM D892 without option A

Tendency - stability

ml.

1.11 High Temperature Foaming Tendency

ASTM D6082 High Tendency - stability Temp foam test

ml.

RE1 -1/+5 -40/+10 -50/+10 -1/+5

RE2-99 RE3 RE4 -5/+8 -25/+1 -5/+5 -15/+18 -45/+10 -20/+10 -35/+10 -20/+10 -50/+10 -7/+5 -1/+30 -5/+5 Sequence I (24°C) 10 - nil Sequence II (94°C) 50 - nil Sequence III (24°C) 10 - nil

AEM (VAMAC) As per Daimler Chrysler

Sequence IV (150°C) 100 - nil

Notes: (1) Use either complete Daimler Chrysler requirements (VDA 675301, 7 days, ±2 hr, 4 materials (NBR; NBR34 DIN 53538 T3 (100ºC +/- 2ºC); FPM: AK6 (150ºC +/- 2ºC); ACM: E7503 (150ºC +/- 2ºC); AEM: D8948/200.1 (150ºC +/- 2ºC) + RE3 according to requirement 1.9 above or complete requirements according to 1.9 above plus DC requirements for AEM. New CEC RE3 material and limits are to be developed and added to Sequences as soon as possible. 04/02 - Crankcase

Laboratory Tests

ACEA 2002 Service Fill Oils for Gasoline Engines Requirements

Method

Properties Unit

Limits

1.1

Viscosity Grade

1.2

Shear Stability

CEC L-14-A-93 (Bosch injector)

Viscosity after 30 cycles measured at 100°C.

1.3

Viscosity High Temperature High Shear Rate Evaporative Loss (Noack)

CEC L-36-A-97 (Ravenfield)

Viscosity at 150°C. and 106s-1 shear rate

CEC L-40-A-93

Max. weight loss after 1hr. at 250°C.

1.5

Sulphated Ash

ASTM D874

1.6 1.7 1.8 1.9

Sulphur Phosphorus Chlorine Oil/Elastomer Compatibility See Notes (1)

1.4

SAE J 300 Latest active issue

CEC L-39-T-96

Max. variation of characteristics after immersion for 7 days in fresh oil without pre-ageing Hardness DIDC Tensile strength Elongation rupture Volume variation

A1-02 A2-96 Issue 3 A3-02 A5-02 No restriction except as defined by shear stability and HTHS requirements. Manufacturers may indicate specific viscosity requirements related to ambient temperatures. XW-20: stay-in-grade XW-30 ≥ 8.6 XW-30 ≥ 9.0 mm2/s. All grades to be All grades to be XW-40 ≥ 12.0 XW-40 ≥ 12.0 stay-in-grade stay-in-grade XW-50 ≥ 15.0 max 3.5 min 2.9 mPa.s XW-20 min 2.6 > 3.5 > 3.5 max 3.5 All others min 2.9 ≤ 15 for 10W-X % ≤ 15 or lower. ≤ 13 ≤ 13 ≤ 13 for others % m/m ≤ 1.3 ≤ 1.5 ≤ 1.5 ≤ 1.5 The following sections apply to all Sequences ppm m/m Report ppm m/m Report ppm m/m Report Elastomer type points % % %

1.10 Foaming Tendency

ASTM D892 without option A

Tendency - stability

ml.

1.11 High Temperature Foaming Tendency

ASTM D6082 High Tendency - stability Temp foam test

ml.

RE1 -1/+5 -40/+10 -50/+10 -1/+5

RE2-99 RE3 RE4 -5/+8 -25/+1 -5/+5 -15/+18 -45/+10 -20/+10 -35/+10 -20/+10 -50/+10 -7/+5 -1/+30 -5/+5 Sequence I (24°C) 10 - nil Sequence II (94°C) 50 - nil Sequence III (24°C) 10 - nil

AEM (VAMAC) As per Daimler Chrysler

Sequence IV (150°C) 100 - nil

Notes: (1) Use either complete Daimler Chrysler requirements (VDA 675301, 7 days, ±2 hr, 4 materials (NBR; NBR34 DIN 53538 T3 (100ºC +/- 2ºC); FPM: AK6 (150ºC +/- 2ºC); ACM: E7503 (150ºC +/- 2ºC); AEM: D8948/200.1 (150ºC +/- 2ºC) + RE3 according to requirement 1.9 above or complete requirements according to 1.9 above plus DC requirements for AEM. New CEC RE3 material and limits are to be developed and added to Sequences as soon as possible. 04/02 - Crankcase

Engine Tests

ACEA 2002 Service Fill Oils for Gasoline Engines Requirements

Method

Properties

Unit

Limits A1-02

2.1

2.3

Ring Sticking (each part) Piston Varnish (6 elements) average of 4 pistons Absolute Viscosity Increase at 40°C. between min. and max. values during test Oil Consumption ASTM D6593-00 Average Engine Sludge Rocker Cover Sludge (Sequence VG) Average Piston Skirt Varnish Average Engine Varnish Under protocol & Comp. Ring (hot stuck) requirements for API SJ Oil Screen Clogging See Note(2)

High Temp. CEC L-88-T-xx deposits (TU5JP - L4) Ring Sticking 72 hour test Oil Thickening

Low Temp. Sludge

CEC L-38-A-94 (TU3M)

2.4

Valve Train Scuffing Wear

2.5 2.6

Black Sludge CEC L-53-T-95 (M111) Fuel Economy CEC L-54-T-96 (M111) See Note(3)

Cam Wear, average Cam Wear, max. Pad Merit (avg. of 8 pads) Engine Sludge, average Fuel Economy Improvement vs. Reference Oil RL 191 (15W-40)

A2-96 Issue 3

A5-02

≤0.8 x RL216

≤0.8 x RL216

≥ 9.0

merit

≥ RL216

mm2/s.

≤ RL216

≤1.5 x RL216

kg/test merit merit merit merit %

Report ≥ 7.8 ≥ 8.0 ≥ 7.5 ≥ 8.9 None ≤ 20

µm. µm. merit merit

≤ 10 ≤ 15 ≥ 7.5 ≥ RL140

%

≥ 2.5

-

Notes: (2) The limits shown are based upon those applied in U.S. market requirements. ACEA will continuously review the situation to ensure that these limits are appropriate for European vehicles and lubricants. (3) ACEA considers the CEC L-54-T-96 test the only valid comparator against which claims of lubricant fuel economy improvement should be made.

04/02 - Crankcase

A3-02

merit

-

≥ 2.5

Laboratory Tests

ACEA 2002 Service Fill Oils for Light Duty Diesel Engines Requirements 1.1

Viscosity Grade

1.2

Shear Stability

Method

Properties SAE J 300 Latest active issue

CEC L-14-A-93 (Bosch injector)

Viscosity after 30 cycles measured @ 100°C.

Viscosity High Temperature High Shear Rate Evaporative Loss (Noack)

CEC L-36-A-97 (Ravenfield)

Viscosity @ 150°C. and 106s-1 shear rate

CEC L-40-A-93

Max. weight loss after 1hr. @ 250°C.

1.5

Sulphated Ash

ASTM D874

1.6 1.7 1.8 1.9

Sulphur Phosphorus Chlorine Oil/Elastomer Compatibility See Notes (1)

1.3

1.4

Unit

mm2/s.

mPa.s

% % m/m ppm m/m ppm m/m ppm m/m

CEC L-39-T-96

Max. variation of characteristics after immersion for 7 days in fresh oil without pre-ageing Hardness DIDC points Tensile strength % Elongation rupture % Volume variation %

1.10 Foaming Tendency

ASTM D892 without option A

Tendency - stability

ml.

1.11 High Temperature Foaming Tendency

ASTM D6082 High Tendency - stability Temp foam test

ml.

Limits B1-02 B2-98 Issue 2 B3-98 Issue 2 B4-02 B5-02 No restriction except as defined by shear stability and HTHS requirements. Manufacturers may indicate specific viscosity requirements related to ambient temperatures. XW-20: stay-in-grade XW-30 ≥ 8.6 XW-30 ≥ 9.0 All grades All grades All grades XW-40 ≥ 12.0 XW-40 ≥ 12.0 to be to be to be XW-50 ≥ 15.0 stay-in-grade stay-in-grade stay-in-grade max 3.5 min 2.9 XW-20 min 2.6 > 3.5 > 3.5 >3.5 max 3.5 All others min 2.9 ≤ 15 for 10W-X ≤ 15 or lower. ≤ 13 ≤ 13 ≤ 13 ≤ 13 for others ≤ 1.3 ≤ 1.8 ≤ 1.5 ≤ 1.6 ≤ 1.6 The following sections apply to all Sequences Report Report Report Elastomer type RE1 -1/+5 -40/+10 -50/+10 -1/+5

RE2-99 RE3 RE4 -5/+8 -25/+1 -5/+5 -15/+18 -45/+10 -20/+10 -35/+10 -20/+10 -50/+10 -7/+5 -1/+30 -5/+5 Sequence I (24°C) 10 - nil Sequence II (94°C) 50 - nil Sequence III (24°C) 10 - nil

AEM (VAMAC) As per Daimler Chrysler

Sequence IV (150°C) 100 - nil

Notes: (1) Use either complete Daimler Chrysler requirements (VDA 675301, 7 days, ±2 hr, 4 materials (NBR; NBR34 DIN 53538 T3 (100ºC +/- 2ºC); FPM: AK6 (150ºC +/- 2ºC); ACM: E7503 (150ºC +/- 2ºC); AEM: D8948/200.1 (150ºC +/- 2ºC) + RE3 according to requirement 1.9 above or complete requirements according to 1.9 above plus DC requirements for AEM. New CEC RE3 material and limits are to be developed and added to Sequences as soon as possible. 04/02 - Crankcase

Engine Tests

ACEA 2002 Service Fill Oils for Light Duty Diesel Engines Requirements

Method

Properties

Unit

Limits B1-02

2.1

2.2

Ring Sticking and CEC L-46-T-93 Piston Cleanliness (VW 1.6 TC D) See Note (4) Medium Temp. CEC L-56-T-98 Dispersivity (XUD11BTE)

2.3

Wear, Viscosity Stability & Oil Consumption

2.4

DI Diesel CEC L-78-T-99 Piston Cleanliness (VW DI) & Ring Sticking

2.5

Fuel Economy See Note (3)

CEC L-51-A-98 (OM 602A)

CEC L-54-T-96 (M111E)

B4-02

B5-02

Ring Sticking

merit

≥ RL148

≥ RL148

≥ RL148

-

-

Piston Cleanliness

merit

≥ RL148

≥ RL148

≥ RL148

-

-

≤ 0.50 x RL197 result

≤ 0.90 x RL197 result

≤ 0.50 x RL197 result

≤ 0.50 x RL197 result

≤ 0.50 x RL197 result

≥ (RL197 minus 6 pts)

≥ (RL197 minus 6 pts)

≥ RL197

≥ RL197

≥ RL197

Absolute Viscosity Increase @ 100°C. and 3% soot (measurement with mm2/s. CEC L-83-A-97 method) Piston Merit (5 elements) merit average for 4 pistons Cam Wear, avg. Viscosity Increase at 40°C. Bore Polishing Cylinder Wear, avg. Oil Consumption

B2-98 Issue 2 B3-98 Issue 2

µm. % % µm. kg/test

≤ 50.0 ≤ 90 ≤ 7.0 ≤ 20.0 ≤ 10.0

Piston Cleanliness

merit

-

-

-

≥ (RL206 minus 3 points)

> RL20

Ring Sticking (Rings 1 & 2) Avg. of all 8 rings Max. for any 1st ring Max. for any 2nd ring Fuel Economy Improvement vs. Ref. Oil RL191 (15W-40)

ASF ASF ASF

-

-

-

≤ 1.2 ≤ 2.5 ≤ 0.0

≤ 1.2 ≤ 2.5 ≤ 0.0

%

≥ 2.5

-

-

-

≥ 2.5

Notes: (3) ACEA considers the CEC L-54-T-96 test the only valid comparator against which claims of lubricant fuel economy improvement should be made. (4) A passing result in the CEC L-78-T-99 test (VW Di) to the B4 requirements may be used in place of the CEC L-46-T-93 test.

04/02 - Crankcase

Laboratory Tests

ACEA 2002 Service Fill Oils for Heavy Duty Diesel Engines Requirements

Method

Properties

Unit

1.1 Viscosity SAE J300 Latest active issue 1.2 Shear Stability

CEC L-14-A-93 (Bosch injector) measured @ 100°C.

1.3 Viscosity High Temperature High Shear Rate 1.4 Evaporative Loss 1.5 Sulphated Ash

CEC L-36-A-97 (Ravenfield)

1.6 Oil/Elastomer Compatibility

CEC L-39-T-96

Viscosity after 30 cycles

mm2/s.

Limits E2-96 Issue 3 E3-96 Issue 3 E4-99 E5-02 No restriction except as defined by shear stability and HTHS requirements. Manufacturers may indicate specific viscosity requirements related to ambient temperatures. XW-30 ≥ 9.0 XW-40 ≥ 12.0 Stay-in-grade XW-50 ≥ 15.0 No requirements for single grades ≥ 3.5

mPa.s Viscosity @ 150°C. and 106s-1 shear rate CEC L-40-A-93 (Noack) Max. weight loss after 1hr. @ 250°C. % ASTM D874 % m/m.

1.7 Foaming Tendency

ASTM D982 without option A

1.8 High Temperature Foaming Tendency 1.9 Oxidation 1.10 Corrosion (HTCBT)

ASTM D6082 High temp. CEC L-85-T-99 (PDSC) ASTM D5968 (Test temperature 135°C)

Max. variation of characteristics after immersion for 7 days in fresh oil without pre-ageing Hardness DIDC Tensile Strength Elongation Rupture Volume Variation

≤ 13 ≤ 2.0 The following sections apply to all Sequences Elastomer type

points % % %

RE1 -1/+5 -50/+10 -60/+10 -1/+5

RE2-99 RE3 RE4 -5/+8 -25/+1 -5/+5 -15/+18 -45/+10 -20/+10 -35/+10 -20/+10 -50/+10 -7/+5 -1/+30 -5/+5 Sequence I (24°C) 10-nil Sequence II (94°C) 50-nil Sequence III (24°C) 10-nil

AEM (VAMAC) As per Daimler Chrysler

Tendency - stability

ml.

Tendency - stability

ml.

Oxidation Induction Time Used oil lead conc.

min.

-

-

-

≥ 35

ppm.

-

-

-

≤ 100

Sequence IV (150°C) 200-50

Notes: (1) Use either complete Daimler Chrysler requirements (VDA 675301, 7 days, ±2 hr, 4 materials (NBR; NBR34 DIN 53538 T3 (100ºC +/- 2ºC); FPM: AK6 (150ºC +/- 2ºC); ACM: E7503 (150ºC +/- 2ºC); AEM: D8948/200.1 (150ºC +/- 2ºC) + RE3 according to requirement 1.9 above or complete requirements according to 1.9 above plus DC requirements for AEM. New CEC RE3 material and limits are to be developed and added to sequences as soon as possible. 04/02 - Crankcase

Engine Tests

ACEA 2002 Service Fill Oils for Heavy Duty Diesel Engines Requirements

Method

Properties Bore Polishing Piston Cleanliness Average Cylinder Wear Sludge Oil Consumption Cam Wear average Viscosity Increase @ 40°C. Bore Polishing Cylinder Wear, avg. Oil Consumption Relative Viscosity, 4.8% soot 1 test 2 test average 3 test average Viscosity Increase, 3.8% soot 1 test 2 test average 3 test average Filter Plugging Differential Pressure Oil Consumption Bore Polishing Piston Cleanliness Boost Pressure Loss at 400 hours Oil Consumption

2.1

Bore Polishing/ Piston Cleanliness

CEC L-42-T-99 (OM 364LA)

2.2

Wear (OM 602A)

CEC L-51-A-97

2.3

Soot in Oil

ASTM D5967 (Mack T-8E) (300 hours) ASTM D4485 (Mack T-8) (250 hours)

2.4

Bore Polishing CEC L-52-T-97 Piston Cleanliness (OM 441LA) Turbo Charger Deposits

04/02 - Crankcase

Unit

Limits

% merit µm. merit kg/test µm. % % µm. kg/test

E2-96 Issue 3 ≤ 3.5 ≥ 40.0 ≤ 3.5 ≥ 9.4 ≤ 16.0 ≤ 50.0 -

E3-96 Issue 3 ≤ 1.0 ≥ 45.0 ≤ 3.0 ≥ 9.5 ≤ 12.0 ≤ 50.0 -

E4-99 ≤ 50.0 ≤ 90 ≤ 7.0 ≤ 20.0 ≤ 10

E5-02 ≤ 50.0 ≤ 90 ≤ 7.0 ≤ 20.0 ≤ 10

-

-

-

≤ 2.1 ≤ 2.2 ≤ 2.3

≤ 2.1 ≤ 2.2 ≤ 2.3

cSt. cSt. cSt. kPa. g/kWh. % merit % kg/test

-

≤ 11.5 ≤ 12.5 ≤ 13.0 ≤ 138 ≤ 0.304 -

≤ 11.5 ≤ 12.5 ≤ 13.0 ≤ 138 ≤ 0.304 ≤ 2.0 ≥ 40.0 ≤4 ≤ 40

≤ 11.5 ≤ 12.5 ≤ 13.0 ≤ 138 ≤ 0.304 ≤ 2.0 ≥ 25.0 ≤4 ≤ 40

Engine Tests

ACEA 2002 Service Fill Oils for Heavy Duty Diesel Engines Requirements 2.5

2.6

Soot Induced Wear

Wear (liner ring-bearings)

04/02 - Crankcase

Method (Cummins M11) ASTM RR: D2 - 1440

(Mack T-9) ASTM D6483

Properties Rocker Pad Average Weight Loss @ 4.5% soot 1 test 2 test average 3 test average Oil Filter Differential Pressure EOT 1 test 2 test average 3 test average Engine Sludge 1 test 2 test average 3 test average Avg. Liner Wear normalised to 1.75% soot 1 test 2 test average 3 test average Avg. Top Ring Weight Loss 1 test 2 test average 3 test average Used Oil Lead Content Increase Used Oil Lead Content Increase at 300-400 hr.

Unit

Limits E2-96 Issue 3

E3-96 Issue 3

E4-99

E5-02

mg. mg. mg.

-

-

-

≤ 6.5 ≤ 7.5 ≤ 8.0

kPa. kPa. kPa.

-

-

-

≤ 79 ≤ 93 ≤ 100

merit merit merit

-

-

-

≥ 8.7 ≥ 8.6 ≥ 8.5

µm. µm. µm.

-

-

-

≤ 25.4 ≤ 26.6 ≤ 27.1

µm. µm. µm. ppm.

-

-

-

≤ 100 ≤ 115 ≤ 130 ≤ 20

ppm.

-

-

-

≤ 10

ILSAC Specifications: GF-1 Test Viscosity Requirements Engine Test Requirements Bench Test Requirements

Limits As defined by SAE J300 Sequence IID, Sequence IIIE, Sequence VE, CRC L-38

API SG Limits apply. Tested according to CMA Code of Practice 6 -1

HTHS Viscosity @ 150°C. and 10 s

Volatility Sim. dis. (ASTM D2887) or Evaporative Loss (CEC L-40-T-87) SAE 0W and 5W multigrades All other SAE viscosity grades GM EOFT Filterability Foaming (Tendency/Stability) ASTM D892 (Option A) Sequence I, max. Sequence II, max. Sequence III, max. Sequence IV, max. Flash Point ASTM D92 or ASTM D93 Shear Stability L-38 10 hour stripped viscosity Homogeneity and Miscibility Federal test method 791B, method 3470

Additional Requirements

04/02 - Crankcase

Sequence VI, EFEI Catalyst Compatibility Phosphorus Content, %. wt. SAE J 300 Low Temperature Viscosity, mPa.s Cranking Pumping

2.9 min. (for all viscosity grades)

20% max. at 371°C. 25% max. 1 hr. at 250°C. 17% max. at 371°C. 20% max. 1 hr. at 250°C. 50% max. flow reduction

10/0 50/0 10/0 Report & Report 185°C. min. 200°C. min. Must stay-in-grade Shall remain homogeneous and when mixed with SAE reference oils, shall remain miscible 2.7% min. 0.12% max. 3500 max. at -20°C. 30000 max. at -25°C.

ILSAC Specifications: GF-2

ILSAC GF-2 is applicable to SAE viscosity grades 0W-X, 5W-X and 10W-X grades only. Oils can be licensed with the API Engine Oil Licensing and Certification System (EOLCS) from 15 October 1996. The Sequence VI fuel economy engine test from ILSAC GF-1 is replaced with the Sequence VI-A. Three categories of fuel economy improvement are possible with ILSAC GF-2. ILSAC GF-2 oils have a phosphorus limitation of 0.10% maximum compared with 0.12% maximum for GF-1. Test Viscosity Requirements Engine Test Requirements Bench Test Requirements

Additional Requirements

04/02 - Crankcase

Limits 0W-X, 5W-X, 10W-X Sequence IID, Sequence IIIE, Sequence VE, CRC L-38 CEC L-40-A-93/L-40-T-87 (Noack), % Phosphorus, % m. Flash Point (ASTM D92), °C. Foaming (Tendency/Stability) Sequence I, max. Sequence II, max. Sequence III, max. High temp. (ASTM 1392), max. Homogeneity/Miscibility GM EOFT Filterability Flow reduction, % GM EOFT Modified 0.6/1.0% water 2.0/3.0% water High Temp. Deposits (TEOST) Deposit wt. mg. Gelation Index Sequence VI-A Fuel Economy SAE 0W-20, 5W-20 Other SAE 0W-X, 5W-X SAE 10W-X

As defined by SAE J 300 API SG Limits apply. Tested according to CMA Code of Practice 22 max. 0.10 max. 200 min. 10/0 50/0 10/0 200/50 Pass 50 max. Rate & Report Rate & Report 60 max. 12.0 max. 1.4% min. 1.1% min. 0.5% min.

ILSAC Specifications: GF-3

ILSAC GF-3 is applicable to SAE viscosity grades 0W-X, 5W-X and 10W-X grades only. Oils can be licensed with the API Engine Oil Licensing and Certification System (EOLCS) from 15 October 1996. The Sequence VI-A fuel economy engine test from ILSAC GF-2 is replaced with the Sequence VI-B. Three categories of fuel economy improvement are possible with ILSAC GF-3. ILSAC GF-3 oils maintain a phosphorus limitation of 0.10% maximum established in ILSAC GF-2 to maintain acceptable catalyst protection. Test Viscosity Requirements Engine Test Requirements Bench Test Requirements

Additional Requirements

Limits 0W-X, 5W-X, 10W-X Sequence IIIF, Sequence IVA, Sequence VG, Sequence VIII, BRT Evaporation Loss (ASTM D5800) Simulated Distillation (ASTM D6417) Phosphorus, % m. Foaming (Tendency/Stability) Sequence I, max. Sequence II, max. Sequence III, max. High temp. (ASTM 1392), max. Homogeneity/Miscibility GM EOFT Filterability Flow reduction, % GM EOFT Modified (EOWTT) (*) 0.6/1.0% water 2.0/3.0% water High Temp. deposits (TEOST-MHT-4) Deposit wt. mg. Gelation Index Sequence VI-B Fuel Economy SAE 0W-20, 5W-20 Other SAE 0W-30, 5W-30 SAE 10W-30 & all other viscosity grades

As defined by SAE J 300 API SL Limits apply. Tested according to ACC Code of Practice 15% max. 1hr. at 250ºC. 10% max. at 371ºC. 0.10 max. 10/0 50/0 10/0 100/0 Pass 50 max. 50 max. 50 max.

FE1 (16hr) 2.0 min 1.6 min. 0.9 min.

Notes: (*) Test formulation with highest additive (DI/VI) concentration. Read across results to all other base oil/viscosity grade formulations using same or lower concentration of identical additive (DI/VI) combination.. Each different DI/VI combination must be tested.

04/02 - Crankcase

45 max. 12.0 max. FE2 (96hr) 1.7 min. 1.3 min. 0.6 min.

Sum FE1/FE2 3.0 min. 1.6 min.

US Military Specifications: Engine Test Requirements MIL-L L-38 IID IIIE

VE

1-H2 1-G2

Bearing Weight Loss, mg. max. Avg. Rust, min. Stuck Lifters Viscosity Increase 64 hrs. 40°C. %. max. Piston Varnish, min. Oil Ring Land Varnish, min. Sludge, min. Ring Sticking Lifter Sticking Cam or Lifter Scuffing Cam plus Lifter Wear, avg. max. µm. max. µm. Avg. Sludge, min. Rocker Cover Sludge, min. Avg. Varnish, min. Piston Varnish, min. Oil Ring Clogging, %. max. Oil Screen Plugging, %. max. Ring Sticking Cam Wear, avg. max. µm. max. µm. TGF, vol. %. max. WTD, max. TGF, vol. %. max. WTD, max.

04/02 - Crankcase

46152D

46152E

2104E

40 8.5 None 375 8.9 3.5 9.2 None None None 30 64 9.0 7.0 5.0 6.5 15 20 None 127

40 8.5 None 375 8.9 3.5 9.2 None None None 30 64 9.0 7.0 5.0 6.5 15 20 None 127

50 8.1 None None 64 178 8.5 6.5 4.2 6.0 15 23 None 203

381 45 140 -

381 45 140 -

457 80 300

Additional Test Requirements for MIL-L-2104E Test

Parameter

Detroit Diesel 6V-53T (FTM 355T)

Piston Area Avg. total deposits, max. Hot stuck rings Avg. Ring Face Distress, demerits, %. max. Fire ring No.’s 2 and 3 compression Liner and Head Area Avg. liner scuffing, %. max. Valve distress Port plugging, % Total Immersion (Buna N) Volume change, % Hardness change, points Dip Cycle (Polyacrylate) Volume change, % Hardness change, points Tip Cycle (Silicone) Volume change, % Hardness change, points Slip Time at 5500 cycles max. Torque, Nm. at 0.2s. slip time, min. ∆ between 1500 & 5500 cycles, max. Stopping Time Increase, %. max. Avg. Total Wear, µm. max.

Allison C-3 (Seal)

C-3 (Time/Torque) Caterpillar TO-2 Notes: (1) 20% max. for 10W (2) In duplicate tests

04/02 - Crankcase

MIL-L-2104E 400 None Report 13.0 12.0 None Report 0 to +5 -5 to +5 0 to 10 10 to 0 0 to +5 -10 to 0 0.85 101.7 40.7 15(1), (2) 350

MIL-L-2104F Engine Test Requirements Number of Tests Run 1K

IIIE

L-38 Mack T7 6V-92TA

04/02 - Crankcase

Top Groove Fill (TGF) %. max. WDK Demerits, max. Top Land Heavy Carbon (TLHC) %. max. Oil Consumption, g/kWhr. max. Scuffing and Ring Sticking Viscosity Increase, 40°C. %. max. Oil Ring Land Deposits, min. Piston Skirt Varnish, min. Sludge, min. Stuck Rings Stuck Lifters Cam and Lifter Scuffing Cam plus Lifter Wear: Avg. max. µm. Maximum, µm. Bearing Weight Loss, mg. max. Piston Skirt Varnish, min. Avg. rate of Viscosity Increase, last 50hr. cSt. @ 100°C./hr. max. Skirts, Tin Removed Wrist Pin Slipper Bushing, Copper removed Ring Face Distress, demerits, max. Fire Ring No. 2 & 3 Compression Rings Broken Rings Cylinder Liner scuffing, %. max. Port Plugging, % area, max. Average Single Cylinder

1

2

3

24 332 4 0.5 None

27 347 5 0.5 None 750 1.5 8.7 9.0 None None None

29 353 5 0.5 None

Report Report

64 145 50 9.0 0.040 Report Report

Report Report

0.33 0.28 None 60.0

0.34 0.29 None 63.5

0.36 0.30 None 65.0

2 5

2 5

2 5

MIL-L-2104F Transmission Test Requirements Graphite Allison C-4 Friction Seals

Slip Time at Cycles, secs. max. Mid-Point Co-efficient of Friction at Cycles min. Total Immersion (Buna N) Volume change, % Hardness change, pts. Dip Cycle (Polyacrylate) Volume change, % Hardness change, pts. Tip Cycle (Silicone) Volume change, % Hardness change, pts. Total Immersion (Flouroelastomer) Volume change, % Hardness change, pts.

Paper

5500

0 -5,000

0.74 0.097

0.67 0.066

04/02 - Crankcase

0.56 0.086

0 to +5 -5 to +5 0 to +10 0 to +5 0 to +5 -10 to 0 0 to +4 -4 to +4 Sequence 1220

Cat TO-4 Average Dynamic Co-efficient, % After 3,000 cycles After 8,000 cycles After 15,000 cycles After 25,000 cycles Average Static Co-efficient, % Disc Wear, mm. max. 0.04 Energy Limit, % 25 Cat TO-3 Stopping Time Increase, % Average Total Wear, µm. Seals

5,000 - 10,000

90 - 140

Sequence FRRET

-

91 - 127

85 90 90 95

-

130 125 125 125

95 - 120 Report Report Report

Japanese Automotive Diesel Engine Oil Standard - JASO DH-1 Test

Performance Criteria

Nissan TD25 Piston Detergency

TGF (Top Groove Fill), % vol. Piston Ring Sticking Deposits on Ring Lands, merit rating Cam Diameter Loss, µm. (Normalized at 4.5 mass % Carbon Residue Increase)

Mitsubishi 4D34T4 Valve Train Wear Protection Mack T8A Soot Dispersency Sequence IIIE High Temperature Oxidation Stability JASO Hot Tube Test Hot Surface Deposit Control Foaming

Volatility Anti-corrosion

Shear Stability

Total Base Number Seal Compatibility

95.0 max.

Viscosity Increase (100-150hr) at 100°C. mm2/s/h.

0.2 max.

Viscosity Increase at 40°C. %

200 max.

At 280°C. merit rating

7.0 min.

Sequence I 10/0 max. Sequence II Tendency / Stability, ml/ml 50/0 max. Sequence III 10/0 max. Evaporation Loss at 250°C. mass % 18.0 max. Copper, mass ppm. 20 max. Lead, mass ppm. 120 max. Tin, mass ppm. 50 max. Discoloration of Copper Coupon after Test at 135°C. 3 max. Stay-in-grade of virgin oil Kinetic Viscosity of Oil after Test at 100°C. mm2/s. viscosity classification in SAE J300 mgKOH/g. (*) 10.0 min. RE1 (Flouro) Hardness Change Point -1/+5 Tensile Strength %, Rate of Change -40/+10 Elongation Rate of Change, % -50/+10 Volume Rate of Change, % -1/+5 RE2-99 (Acrylic) Hardness Change Point -5/+8 Tensile Strength %, Rate of Change -15/+18 Elongation Rate of Change, % -35/+10 Volume Rate of Change, % -7/+5 RE3 (Silicon) Hardness Change Point -25/+1 Tensile Strength %, Rate of Change -45/+10 Elongation Rate of Change, % -20/+10 Volume Rate of Change, % -1/+30 RE4 (Nitrile) Hardness Change Point -5/+5 Tensile Strength %, Rate of Change -20/+10 Elongation Rate of Change, % -50/+10 Volume Rate of Change, % -5/+5

Note: (*)According to JIS K2501 or ASTM D-4739 test method. 04/02 - Crankcase

Limits 60.0 max. All free Report

Global Engine Oil Service Specification DHD-1 Test

Performance Criteria

Caterpillar 1R (1)

Weighted Demerits (WDR), max. Total Groove Carbon, %. max. Top Land Carbon, %. max. Oil Consumption g./hr. Initial max./Final max. Oil Filter Diff. Press. kPa. max. Eng. Sludge, CEC Merits, min. Rocker Pad Average Weight Loss, Normalized to 4.5% soot mg. max. Used Oil Lead, ppm. max. TAN Increase at EOT, max. Average Wear Normalized to 1.75% soot Liner µm. max. Top Ring Wt Loss, mg. max. Relative Viscosity at 4.8% soot Pin Wear, µm. max. Kv 40C Viscosity Increase, %. max. Aeration, vol. %. max. Bore Polish, % Area. max. Boost Pressure Loss at 400 Hours, %. max. Weighted Merits, min. Oil Consumption, kg./test max. Avg. Cam Lobe Wear, µm.

Cummins M11 HST

Mack T-9

Mack T-8E 6.5L RFWT Seq IIIF, 60 hrs. (2) HEUI Mercedes Benz OM 441LA

Mitsubishi 4D34T4 160 hrs.

Note: (1) The requirements for this characteristic may be met with a CH-4 level passing result in an original API CH-4 qualification. (2) Lead Maximum 25 ppm if fresh oil has TBN (ASTM D4739) greater than 10.

04/02 - Crankcase

Engine Tests Limits 397 / 416 / 440 40 / 42 / 44 37 / 42 / 46 13.1 / 1.5 X Initial 79 / 93 / 100 8.7 / 8.6 / 8.5 6.5 / 7.5 / 8.0 15 (2) 2.0 25.4 / 26.6 / 27.1 120 / 136 / 144 2.1 / 2.2 / 2.3 7.6 / 8.4 / 9.1 200 8.0 2.0 4 25.0 40 95.0

Laboratory Tests

Global Engine Oil Service Specification DHD-1 Test

Performance Criteria

Limits

Corrosion Bench Test Used Oil Element Content above Baseline, ppm, max. Elastomer Compatibility *

Variation after 7 days fresh oil, No pre-aging Hardness DIDC, points, max. Tensile Strength, %. max. Elongation rupture, %. max. Volume variation, %. max.

Foaming Tendency

Tendency / Stability, ml. max. after 1 min. settling

Foaming - High Temperature PDSC Shear Stability Bosch Injector Test Sulphated Ash

Tendency / Stability, ml. max. after 1 min. settling Oxid. Induction Time, min. min. Viscosity after 30 Cycles, measured at 100°C. Mass %. max.

HT/HS Viscosity Tapered Bearing High Tempeature / High Shear Rate Simulator / Ravenfield Viscosity, cP. min. NOACK Volatility % Mass Loss, max.

Copper 20, Lead 120, Tin 50 RE 1 -1/+5 -50/+10 -60/+10 -1/+5

Elastomer Type RE 2 RE 3 -5/+5 -25/+1 -15/+10 -45/+1 -35/+10 -20/+10 -5/+5 -1/+30

Sequence I (24°C) 10 - nil Sequence II (94°C) 50 - nil Sequence III (24°C) 10 - nil Sequence IV (150°C) 200 - 50 35 stay-in-grade 2.0 35 15

Note: (*) The Elastomer Compatability Limits are those stated in ACEA 1999 European Oil Sequences and apply to the elastomer batches available at that time. Consult the most recent ACEA Oil Sequence publication for the information on the limits with more recent elastomer batches.

04/02 - Crankcase

RE 4 -5/+5 -20/+10 -50/+10 -5/+5

Global Engine Oil Service Specification DHD-1 Test

Performance Criteria

Caterpillar 1R (1)

Weighted Demerits (WDR), max. Total Groove Carbon, %. max. Top Land Carbon, %. max. Oil Consumption g./hr. Initial max./Final max. Oil Filter Diff. Press. kPa. max. Eng. Sludge, CEC Merits, min. Rocker Pad Average Weight Loss, Normalized to 4.5% soot mg. max. Used Oil Lead, ppm. max. TAN Increase at EOT, max. Average Wear Normalized to 1.75% soot Liner µm. max. Top Ring Wt Loss, mg. max. Relative Viscosity at 4.8% soot Pin Wear, µm. max. Kv 40C Viscosity Increase, %. max. Aeration, vol. %. max. Bore Polish, % Area. max. Boost Pressure Loss at 400 Hours, %. max. Weighted Merits, min. Oil Consumption, kg./test max. Avg. Cam Lobe Wear, µm.

Cummins M11 HST

Mack T-9

Mack T-8E 6.5L RFWT Seq IIIF, 60 hrs. (2) HEUI Mercedes Benz OM 441LA

Mitsubishi 4D34T4 160 hrs.

Note: (1) The requirements for this characteristic may be met with a CH-4 level passing result in an original API CH-4 qualification. (2) Lead Maximum 25 ppm if fresh oil has TBN (ASTM D4739) greater than 10.

04/02 - Crankcase

Engine Tests Limits 397 / 416 / 440 40 / 42 / 44 37 / 42 / 46 13.1 / 1.5 X Initial 79 / 93 / 100 8.7 / 8.6 / 8.5 6.5 / 7.5 / 8.0 15 (2) 2.0 25.4 / 26.6 / 27.1 120 / 136 / 144 2.1 / 2.2 / 2.3 7.6 / 8.4 / 9.1 200 8.0 2.0 4 25.0 40 95.0

Two-Stroke Classification: API TC

API TC (CEC TSC-3)

Engine

Parameter

Limits

Yamaha CE 50S Yamaha CE 50S Yamaha 350 M2

Tightening, Mean Torque Drop Pre-ignition, occurences Piston Varnish Ring Sticking Piston Deposits Piston Scuffing

≤ Ref. Oil 1 max. in 50 hr. test

Better than or equal to ref. oil

Notes: TA (TSC-1) not released as a full specification, but the test methods are recognised by ASTM as valid for assessing the capabilities of two stroke oils. TB (TSC-2) not released as a full specification due to the withdrawal of the supporting OEM. No new work is in progress.

04/02 - Crankcase

Two-Stroke Classification: API TC

API TC (CEC TSC-3)

Engine

Parameter

Limits

Yamaha CE 50S Yamaha CE 50S Yamaha 350 M2

Tightening, Mean Torque Drop Pre-ignition, occurences Piston Varnish Ring Sticking Piston Deposits Piston Scuffing

≤ Ref. Oil 1 max. in 50 hr. test

Better than or equal to ref. oil

Notes: TA (TSC-1) not released as a full specification, but the test methods are recognised by ASTM as valid for assessing the capabilities of two stroke oils. TB (TSC-2) not released as a full specification due to the withdrawal of the supporting OEM. No new work is in progress.

04/02 - Crankcase

Two-Stroke Classification: ISO/JASO ISO

-

EGB

EGC

EGD

JASO Lubricity Torque Index Detergency Piston Skirt Deposits Exhaust Smoke

FA 90 min. 98 min. 80 min. 40 min.

FB 95 min. 98 min. 85 min. 85 min. 45 min.

FC 95 min. 98 min. 95 min. 90 min. 85 min.

95 min. 98 min. 125 min. 95 min. 85 min.

Exhaust Blocking

30 min.

45 min.

90 min.

90 min.

Notes: All limits are indices relative to reference oil, JATRE-1 Test Engines Honda DIO AF27 Lubricity Torque Index Detergency, Piston Skirt Varnish Suzuki SX800R Exhaust Smoke Exhaust Blocking Piston Skirt Deposits rating not required by JASO

04/02 - Crankcase

Two-Stroke Classification: TISI 1040 Test

Parameter

Bench Tests

Viscosity, 100°C. cSt. Viscosity Index Flash Point, °C. Pour Point, °C. Sulphated Ash, % wt. Metallic Element content, % wt. Piston Seizure and Ring Scuffing at fuel-oil ratio of 200:1 Detergency (general cleanliness) Ring Sticking Piston Cleanliness Exhaust Port Blocking Exhaust Smoke

Kawasaki KH 125M

Suzuki SX 800R (JASO M 342-92)

Note: Since mid-1991, all two-stroke oils used in Thailand are required to meet TISI requirements.

04/02 - Crankcase

Limits 5.6 - 16.3 95 min. 70 min. -5 max. 0.5 max. Report No seizure

8 merit min. 48 merit min. None 85 min.

Two-Stroke Classification: NMMA TC-W3 Test

Parameter

Limits

ASTM Lubricity NMMA Detergency

Torque Drop, average Top Ring Sticking, average Piston Deposits, average Spark Plug Fouling, occurrences Exhaust Port Blocking Pre-ignition, occurrences Pre-ignition (major), occurrences Decrease in Flow Rate, %

≤ Ref. Oil Max. 0.6 points below ref. oil Max. 0.6 points below ref. oil Max. 1 more than ref. oil Max. 10% greater than ref. oil ≤ Ref. oil Max. of 1 in 100 hr. test Equal or better than ref. oil Category 3 or 4 of SAE J1536 20 max.

ASTM Pre-ignition NMMA Rust Test SAE Miscibility Fluidity NMMA Filterability

Note: This specification was introduced in April 1992 to replace NMMA TC-W2 and offers improved ring-stick protection and lubricity, with higher anti-scuff performance.

04/02 - Crankcase

OEM Specification: Mercedes-Benz Engine Test Requirements for Diesel Engine Oils Sheet Number

227.0

227.1

228.0

228.1

228.2

228.3

228.5

Viscosity Grade

Mono

Multi

Mono

Multi

Mono

Multi

Multi

OM 602A (After 11.6.97, Euroval tappets) Piston Cleanliness (No ring sticking) Bore Polishing, %. (23mm) Cylinder Wear, avg. µm. (new/old) Cam Wear, avg. µm. (new/old) Oil Consumption, kg. Viscosity Increase, 40°C. % Engine Sludge, avg. OM 364A/OM 364LA Bore Polishing, %. max. Piston Cleanliness, min. Cylinder Wear, avg. µm. max. Engine Sludge, avg. min. Oil Consumption, kg. max. OM 441LA Euro II Bore Polishing, % Piston Cleanliness Cylinder Wear, avg. µm. Engine Sludge, avg. Engine Deposits demerit Wear Rating demerit Ring Sticking, ASF Oil Consumption, g/hr. Boost Pressure loss, 400 hrs. % Note: (*) For OM 441LA tests started after 1.9.1999.

04/02 - Crankcase

20 min. 7.0 max. 20.0 max./12.0 max. 50.0 max./30.0 max. 10.0 max. 90 max. 8.8 min. OM 364A/OM 364LA 14.0/6.0 24.0/35.0 8.0/4.0. 9.0/9.3 25.0/20.0

22 min. 6.0 max. 18.0 max./11.0 max. 50.0 max./29.0 max. 10.0 max. 80 max. 8.9 min. OM 364A/OM 364LA 8.0/3.5 31.0/40.0 7.0/3.5 9.0/9.4 18.0/16.0

24 min. 4.5 max. 15.0 max./10.0 max. 45.0 max./28.0 max. 10.0 max. 70 max. 8.9 min. OM 364A/OM 364LA 2.5/1.0 35.0/45.0 6.0/3.0 9.5/9.5 12.0/12.0

26 min. 3.0 max. 15.0 max./10.0 max. 45.0 max./28.0 max. 10.0 max. 60 max. 9.0 min. OM 364A/OM 364LA 1.0/0.5 50.0/50.0 3.0/2.5 9.5/9.6 10.0/10.0

2.0 max. 25.0 max. 8.0 max. 9.0 max. 3.0 max. 2.5 max. 1.0 max. 100.0 max.

2.0 max. 40.0 min 8.0 max. 9.0 min. 3.0 max. 2.5 max. 1.0 max. 100.0 max.

4.0 max. (*)

4.0 max. (*)

OEM Specification: Mercedes-Benz Engine Test Requirements for Diesel Engine Oils Sheet Number

227.0

227.1

228.0

228.1

228.2

228.3

228.5

Viscosity Grade

Mono

Multi

Mono

Multi

Mono

Multi

Multi

OM 602A (After 11.6.97, Euroval tappets) Piston Cleanliness (No ring sticking) Bore Polishing, %. (23mm) Cylinder Wear, avg. µm. (new/old) Cam Wear, avg. µm. (new/old) Oil Consumption, kg. Viscosity Increase, 40°C. % Engine Sludge, avg. OM 364A/OM 364LA Bore Polishing, %. max. Piston Cleanliness, min. Cylinder Wear, avg. µm. max. Engine Sludge, avg. min. Oil Consumption, kg. max. OM 441LA Euro II Bore Polishing, % Piston Cleanliness Cylinder Wear, avg. µm. Engine Sludge, avg. Engine Deposits demerit Wear Rating demerit Ring Sticking, ASF Oil Consumption, g/hr. Boost Pressure loss, 400 hrs. % Note: (*) For OM 441LA tests started after 1.9.1999.

04/02 - Crankcase

20 min. 7.0 max. 20.0 max./12.0 max. 50.0 max./30.0 max. 10.0 max. 90 max. 8.8 min. OM 364A/OM 364LA 14.0/6.0 24.0/35.0 8.0/4.0. 9.0/9.3 25.0/20.0

22 min. 6.0 max. 18.0 max./11.0 max. 50.0 max./29.0 max. 10.0 max. 80 max. 8.9 min. OM 364A/OM 364LA 8.0/3.5 31.0/40.0 7.0/3.5 9.0/9.4 18.0/16.0

24 min. 4.5 max. 15.0 max./10.0 max. 45.0 max./28.0 max. 10.0 max. 70 max. 8.9 min. OM 364A/OM 364LA 2.5/1.0 35.0/45.0 6.0/3.0 9.5/9.5 12.0/12.0

26 min. 3.0 max. 15.0 max./10.0 max. 45.0 max./28.0 max. 10.0 max. 60 max. 9.0 min. OM 364A/OM 364LA 1.0/0.5 50.0/50.0 3.0/2.5 9.5/9.6 10.0/10.0

2.0 max. 25.0 max. 8.0 max. 9.0 max. 3.0 max. 2.5 max. 1.0 max. 100.0 max.

2.0 max. 40.0 min 8.0 max. 9.0 min. 3.0 max. 2.5 max. 1.0 max. 100.0 max.

4.0 max. (*)

4.0 max. (*)

OEM Specification: Mercedes-Benz Sheet 229.1 for Passenger Car Engine Oils Sheet Number ACEA Viscosity Grades, SAE

Sulphated Ash Relative Permittivity Seals Tests Engine Tests M111E Sludge Engine Sludge, avg. Cam Wear, avg. µm. OM 602A Piston Cleanliness (no ring sticking) Bore Polishing, % (23mm) Cylinder Wear, avg. µm. (new/old) Cam Wear, avg. µm. (new/old) Oil Consumption, kg. Viscosity Increase, 40°C. % Engine Sludge, avg.

04/02 - Crankcase

229.1 A3-96 B3-96 5W-30, 5W-40, 5W-50, 10W-30, 10W-40, 10W-50, 10W-60, 15W-40, 15W-50, 20W-40, 20W-50 1.5 max. Rate & Report See last page of this section

RL 140 + 2 std. deviation 5.0 max. 20 min. 7.0 max. 20.0 max./12.0 max. 50.0 max./30.0 max. 10.0 max. 90 max. 8.8 min.

OEM Specification: Mercedes-Benz Sheet 229.3 for Passenger Car Engine Oils Sheet Number ACEA Viscosity Grades, SAE Chlorine, ppm. Sulphur, wt. % Seals Tests Engine Tests M111E Sludge Engine Sludge, avg. Cam Wear, avg. µm. M111E Fuel Economy OM 602A Piston Cleanliness Bore Polishing, % Cylinder Wear, avg. µm. (new/old) Cam Wear, avg. µm. (new/old) Oil Consumption, kg. Viscosity Increase, 40°C. % Engine Sludge, avg. VW PV 1449 (VW T4)

04/02 - Crankcase

229.3 A3-98, B3-98, B4-98 0W-X, 5W-X 100 max. 0.5 max. See last page of this section

RL 140 + 3 std. deviation (Batch 2 fuel) RL 140 + 2 std. deviation (Batch 1 fuel) 3.0 max. 1.0 % min. 24 min. 4.5 max. 15.0 max. 45.0 max./10.0 max. 10.0 max./28.0 max. 70 max. 8.9 min. To VW 502.00 limits

OEM Specification: Mercedes-Benz Sheet 229.5 for Passenger Car Engine Oils Sheet Number ACEA Viscosity Grades, SAE Chlorine, ppm. Sulphur wt. % Seals Tests Engine Tests M111E Sludge Engine Sludge, avg. Cam Wear, avg. µm M111E Fuel Economy OM 602A Piston Cleanliness (no ring sticking) Bore Polishing, % (23mm) Cylinder Wear, avg. µm. (new/old) Cam Wear, avg. µm. (new/old) Oil Consumption, kg. Viscosity Increase, 40°C. % Engine Sludge, avg. VW PV 1449 (VW T4) VW TDI or PV 1452 Wartung 2000 Tests (Note a) Bench Tests @ DC:M111 E23 (Prufstand-Snail-Programme-PSP) OM 611 DE 22LA (12 Pkt DL) M166 E16 (12 Pkt DL) M111 E23ML (40 Pkt DL) Field Tests (S=Snail, B=Barracuda):S: 1 x A140; 1x C230T Kompressor B: 1 x E220T CDi 99; 1 x A170 CDi

229.5 A3-98, B3-98, B4-98 0W-X, 5W-X, 10W-X 50 max. 0.5 max. See last page of this section

n.n. (439 hr) (Note a) 5.0 max. (439 hr) 1.8% min. 26 min. 3.0 max. 15.0 max./10.0 max. 45.0 max./28.0 max. 10.0 max. 60.0 max. 9.0 min. To VW 502.00 limits To B4 or VW 506.00 limits

Yes Yes Yes Yes Yes Yes

Note a: For sheet 229.5 please contact EP/MPO before starting tests. Further requirements are listed in the performance standard. Approvals will not be given before 3/2002. 04/02 - Crankcase

OEM Specifications: MAN 270, MAN 271 Requirements Performance Level: ACEA SAE Viscosity Grades (J300)(1) Viscosity after Shear, mm2./sec. min. HTHS, mPa.s, min. Zinc, % wt. min. Ethylene Glycol, % wt. max. Foaming Tendency, max. ml. Foam Stability, nil after (s) max. NBR-28 Compatibility (100°C/7 days) Change in Hardness (Shore A), max. Tensile Strength, % change, max. Elongation Change, % of %, max. Volume Change, % FPM-AK6 Compatibility (150°C/7 days) Change in Hardness (Shore A) Tensile Strength, % change, max. Elongation Change, % of %, max. Volume Change, %

MAN 270

MAN 271

E2-96

0.08 0.05 10/50/10 180/90/180

E2-96 10W-40 15W-40 20W-50 12.0(2) 3.5 0.08 0.05 10/50/10 180/90/180

-10 -20 -30 0/+10

-10 -20 -30 0/+10

-5/+5 -30 -40 -2/+5

-5/+5 -30 -40 -2/+5

10W, 20W-20 20W-30, 30, 40

Note: (1) Other viscosities need MAN agreement, 10W-40 must contain 25% of unconventional base stocks. (2) 15 min. for SAE 20W-50.

04/02 - Crankcase

OEM Specifications: MAN 270, MAN 271

Additional Notes 1.

MWM ‘B’ tests are no longer required or accepted for new oil approvals. Approvals based on MWM ‘B’ tests invalid after 31 May 1996.

2.

Evaporation loss, pour point and flash point limits:

SAE SAE SAE SAE SAE SAE SAE SAE

3.

04/02

10-W 10W-40 15W-40 20W-20 20W-30 20W-50 30 40

Evaporation Loss %. max.

Pour Point max. °C.

Flash Point (COC) min. °C.

15 13 13 13 13 13 10 10

-33 -30 -27 -24 -24 -24 -18 -15

205 215 215 210 210 215 220 225

Base oil blends to meet requirements of MAN N699. Un-conventional base oils may require additional testing.

Crankcase

OEM Specification: MAN M 3275 Requirements SAE Viscosity Grades (J300)

MAN M 3275 5W-30 5W-40

HTHS Viscosity, mPa.s Viscosity after Shear, mm2/s. Noack Evaporation Loss, % Flash Point (COC), °C. Pour Point, °C. Zinc, % m. Ethylene Glycol, % m. Foaming Tendency, ml. Foam Stability, nil after s. Seal Tests NBR 28, AK6 Engine Tests OM 602A Cam Wear, av. µm. Viscosity Increase @ 40°C. Bore Polishing, % Cylinder Wear, av. µm. Oil Consumption, kg. OM 441LA Bore Polishing, % Piston Cleanliness Boost Pressure Loss @ 400hrs. Oil Consumption, kg/test

-40 max.

10W-30 10W-40 3.5 min. XW-30 9 min. XW-40 12 min. 13 max. 215 min. -30 max. 0.08 min. 0.05 max. 10/50/10 max. (Seq I/II/III) 180/90/180 max. (Seq I/II/III) Pass (See last page of this section)

50 max. 90 max. 7.0 max. 20 max 10.0 max. 2.0 max. 25.0 min. 4 max. 40 max.

Note: Viscosity Grades: Generally SAE 15W-40 with mineral base oil. Other viscosity grades may be approved by agreement e.g. SAE 10W-40 with unconventional base oil (minimum 25% in fully formulated oil), SAE 5W-30, 5W-40 (unconventional base oil only).

04/02 - Crankcase

15W-30 15W-40

-27 max.

OEM Specification: MAN M 3277 Requirements SAE Viscosity Grades (J300) HTHS Viscosity, mPa.s

MAN M 3277 5W-X

Viscosity after Shear, mm2/s. Noack Evaporation Loss, % Flash Point (COC), °C. Pour Point, °C. Zinc, % m. Sulphated Ash, % m. Ethylene Glycol, % m. Foaming Tendency, ml. Foam Stability, nil after s. Seal Tests NBR 28, AK6 Turbocharger Deposits (MTU), mg. Engine Tests OM 441LA Viscosity Increase, 100°C. % Soot in oil, % Piston Cleanliness Bore Polishing, % Visual Wear, points Cylinder Wear, mm. Total Deposits, points Sludge Oil Consumption, g/hr. OM 602A Viscosity Increase, 40°C. % Viscosity Increase, 100°C. % Soot in oil, % Bore Polishing, % Piston Cleanliness Sludge Cylinder Wear, avg. µm. Cam Wear, avg. µm. Oil Consumption, kg.

-40 max.

10W-X 3.5 min. XW-30 9 min. XW-40 12 min. 13 max. 215 min. -30 max. 0.08 min. 2.0 max. 0.05 max. 10/50/10 max. (Seq I/II/III) 180/90/180 max. (Seq I/II/III) Pass 120 max.

15W-X

-27 max.

Rate & Report Rate & Report 40 min. 2.0 max. 2.5 max. 0.008 max. 3.0 max. 9.0 min. 100 max. 60 max. Rate & Report Rate & Report 3.0 max. 26 min. 9.0 min. 10 max. 28.0 max 10 max.

Note: Viscosity Grades Generally SAE 10W-40 using a minimum 25% of unconventional base oil. SAE 5W-X to use unconventional base oil only.

04/02 - Crankcase

OEM Specifications: Volkswagen 500.00, 501.01, 505.00, 502.00 Requirements Performance Level, CCMC, min. ACEA, min. Viscosity Grades, SAE

Sulphated Ash, % m. HTHS, 150°C. 106s-1 Seal Compatibility, PV-3344 Valve Train Wear, PV-5106 Piston Cleanliness/Wear, PV-9800 (VW 1302) PV-1449 (VW T4) Piston Cleanliness, PV-1435 (b) Piston Cleanliness, Intercooled T/C Diesel Sludge, M102E Sludge, M111E Evaporation Loss, %

VW 500.00

VW 501.01

VW 505.00

VW 502.00

G5

G4

PD-2

A2-96 or A3-96

5W-30 5W-40 10W-30 10W-40 1.5 max. 3.5 min. ✔ ✔ ✔ ✔ ✔ -

1.5 max. 3.5 min. ✔ ✔ ✔ ✔ ✔ -

3.5 min. ✔ ✔ (a) ✔ (a) -

13 max.

(c)

(c)

As listed in Note (c) below

Notes: (a) Only required when sulphated ash is less than 1.5%. (b) Not required when Intercooled T/C Diesel data is available. (c) 13 max for SAE 5W-50, 10W-50/60, 15W-40/50, 20W-40/50; 15 max for SAE 5W-30/40, 10W-30/40.

04/02 - Crankcase

0W-30, 0W-40, 5W-30, 5W-40, 5W-50 10W-30,10W-40,10W-50,10W-60 15W-40,15W-50, 20W-40, 20W-50 1.5 max. 3.5 min. ✔ ✔ ✔ ✔ 0W-X, 15 max. 5W-X, 10W-X, 15 max. 15W-X, 20W-X, 13 max.

OEM Specifications: Volkswagen 503.00, 506.00 Requirements Performance Level, ACEA Viscosity Grades, SAE HTHS, 150°C. 106 s-1 Sulphated Ash, % m. Evaporation Loss, % m. M111E Sludge VW T4 (PV 1449) Fuel Economy (PV 1451) Cam and Tappet (PV 5106) RNT Wear Test VW DI Diesel (PV 1452) Seals Tests AK6 ACM VAMAC

VW 503.00

✓ ✓ ✓

Notes: Based on Factory Fill Oil specification VW 521 73. VW 503.00 is Service Fill for gasoline engines with extended drain capability 30,000km. or two years, from May 1999 (2000 model year). VW 506.00 is Service Fill for diesel engines with extended drain capability 50,000km. or two years, from May 1999 (2000 model year).

04/02 - Crankcase

VW 506.00

A3-98 B4-98 0W-30, 0W-40, 5W-30, 5W-40, 10W-30, 10W-40 2.9 - 3.4 1.5 max. 13.0 max. ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓ ✓

Volvo Drain Specification (VDS)

Performance Requirements

API CD/CE

Field Trial Requirements

Minimum of three trucks required equipped with Volvo 12 litre intercooled engine. Field trial shall run for minimum 300,000 km. with 50,000 km. oil and filter changes. Test vehicles should be run on fuel with max. 0.7% by weight sulphur. Oil samples taken after 15,000, 30,000 and 50,000 km. of the change interval are tested for viscosity at 100°C (ASTM D445). The values must not be less than:

Viscosities shall be 10W-30 or 15W-40, (10W-30 approval includes 15W-40 but not vice versa).

9 cSt for 10W-30 12 cSt for 15W-40 TBN (ASTM D2896) value must not be less than 50% of the fresh oil value. Wear rate must not increase during the test. Oil consumption must not increase during the test. Bore polishing to be 300 cm2 max. for the entire engine (100 cm2 max. for any individual liner).

04/02

Crankcase

Volvo Drain Specification (VDS)

Performance Requirements

API CD/CE

Field Trial Requirements

Minimum of three trucks required equipped with Volvo 12 litre intercooled engine. Field trial shall run for minimum 300,000 km. with 50,000 km. oil and filter changes. Test vehicles should be run on fuel with max. 0.7% by weight sulphur. Oil samples taken after 15,000, 30,000 and 50,000 km. of the change interval are tested for viscosity at 100°C (ASTM D445). The values must not be less than:

Viscosities shall be 10W-30 or 15W-40, (10W-30 approval includes 15W-40 but not vice versa).

9 cSt for 10W-30 12 cSt for 15W-40 TBN (ASTM D2896) value must not be less than 50% of the fresh oil value. Wear rate must not increase during the test. Oil consumption must not increase during the test. Bore polishing to be 300 cm2 max. for the entire engine (100 cm2 max. for any individual liner).

04/02

Crankcase

Volvo Drain Specification - 2 (VDS-2)

Oils meeting VDS-2 are recommended for Volvo truck engines meeting the 1996 European emission requirements. To meet the requirements of “Volvo Drain Specification-2” a field test as specified below is necessary. Upon completion of the test, various engine parts shall be inspected and evaluated. Test Conditions

Field test to involve a minimum of three trucks. Test oil shall be minimum ACEA E3 or API CG-4 of viscosity 5W30, 5W40, 10W30, 10W40 or 15W40. Other viscosity grades can be accepted after agreement with Volvo. Trucks used for the test to be equipped with Volvo TD 123 Series, 12 litre intercooled engine.

Field Test

Field test to be run for minimum of 300,000 km. with 60,000 km. oil change intervals. During the test, oil samples are taken after 15,000, 30,000, 45,000 and 60,000 km. of the change interval and checked with respect to:Viscosity at 100°C: (ASTM D445)

To be between 9 cSt. and 140% of the fresh oil value for XW-30 oils, and between 12 cSt. and 140% of the fresh oil value for XW-40 oils.

TBN (ASTM D4739):

Value must not be less than 50% of the fresh oil value, or below 4, whichever is the greater.

TAN (ASTM D664):

Report

Pentane Insolubles:

Report

Wear Metals:

Concentration must not increase during the test.

Additive elements:

Report

In addition, oil and fuel consumption are measured during the test, oil consumption must not increase. Inspection and Evaluation

Upon completion of the field test, the following engine components are inspected:Pistons, Piston rings, Cylinder liners, Tappets, Camshaft, Rocker arms, Valves, Bearings. Cleanliness of covers and oil sump also inspected. For oils qualified to VDS-2, “read-across” to other viscosity grades, VI improvers or base oils than those used in the field test can be accepted after agreement with Volvo.

04/02

Crankcase

Volvo Drain Specification - 3 (VDS-3)

VDS-3 is the oil quality intended for Volvo Truck Euro 3 engines. Engine: Field Test: Test Length and Drain Intervals:

D12C (any version > 400 hp) fitted to FH12 or FM12 trucks. European Long Haul Service only, two trucks minimum. GVW up to 44t:

3 x 100,000 km oil drains with oil samples taken at 0, 25,000, 50,000, 75,000 and 100,000 km.

GVW over 44t:

4 x 75,000 km oil drains with oil samples taken at 0, 25,000, 50,000 and 75,000 km.

Field test to commence before engine reaches 50,000 km. Limits:

On completion of field trial, engine parts will be inspected for piston cleanliness, bore polish and ring wear. Limits are tiered according to two or three truck tests and cover Volvo VDS-2 and VDS-3 approval categories.

Draft Limits VDS-3: Piston Cleanliness (1st G + 2nd G + 2nd L) Ring Riding (max. %) (avg. %) 2 Bore Polish (Total, cm ) Draft Limits VDS-2: Piston Cleanliness (1st G + 2nd G + 2nd L) Ring Riding (max. %) (avg. %) 2 Bore Polish (Total, cm ) Other Requirements:

Average 2 trucks

Average 3 trucks

Max liner/piston per engine

40 min. 25 max. 12 max. 100 max.

35 min. 30 max. 15 max. 120 max.

30 max. 30 max.

Average 2 trucks

Average 3 trucks

Max liner/piston per engine

30 min. 35 max. 20 max. 120 max.

25 min. 40 max. 25 max. 140 max.

40 max. 35 max.

For VDS-3 oils sold in Europe, ACEA E5-99 or DHD-1 performance to be demonstrated. For VDS-3 oils sold outside Europe, DHD-1 performance to be demonstrated for global markets or API CH4 for US market. For new VDS-3 trials to start - Mack EO-M+ limits in the Mack T9.

04/02

Crankcase

OEM Specification: MTU MTL 5044 Engine Test Requirements

Bore Polishing, % Piston Cleanliness Cylinder Wear, avg. µm. Cam Wear, avg. µm. Engine Sludge Oil Consumption, kg. Viscosity Increase, 40°C. %

OM 364A Type 1/1*

Type 2

Type 1/1*

Type 2

14.0 max. 24 min. 8 max. 9.0 min. 25.0 max. -

2.5 max. 35 min. 6 max. 9.5 min. 12.0 max. -

7.0 max. 20 min. 12.0 max. 30.0 max. 8.8 min. 10 max. 90 max.

4.5 max. 24 min. 10.0 max. 28.0 max. 8.9 min. 10 max. 70 max.

Chemical - Physical Requirements Oil Types 1, 1*, 2 Viscosity, SAE HTHS, 150°C. 106s-1 Flash Point (COC), °C. Evaporation Loss, % m. Sulphated Ash, % m. TBN, mg KOH/g Viscosity after Shear, cSt. Chlorine, ppm. Zinc, % m. Deposits, MTV5040, mg. Seals, NBR 28, AK6

OM 602A

Single Grade 30

Multigrade 40

5W-30, 10W-30, 15W-30

225 min. 10 max. 1.0 - 2.0 8 min. 150 max. 0.035 min. See last page

Classification of Engine Oils: Oil Type 1: Normal quality (ACEA E1-96, E2-96) Oil Type 1*: Type 1 with increased corrosion inhibition. Type 1* oils also require corrosion testing, Hydrobromic Acid/Sea Water. Oil type 2: High quality (SHPD, ACEA E3-96) Other tests required, Rate and Report only.

04/02 - Crankcase

5W-40, 10W-40, 15W-40 3.5 min. 215 min. 13 max. 1.0 - 2.0 8 min.

9 min.

12 min. 150 max. 0.035 min. 100 max. See last page

OEM Specification: Mack EO-K/2 Test Mack T-6

Mack T-7 Field Test

Parameter Oil Consumption (2100 rpm), lb/BHP hr. avg. max. Ring Weight Loss (Nos. 1 and 2 avg), mg. max. Ring Proudness, inches, max. Viscosity Increase @ 99°C. cSt. max. Piston Demerits, max. * Total Merits, min. Rate of Viscosity Increase, 100 - 150 hr. cSt/hr. max. To involve more than one vehicle, using the product in Mack engines at Mack’s recommended drain intervals for 200,000 miles.

Note: * Mack Merit Rating System - Relative Importance of Test Criteria and Merit Calculations. Oil Consumption Ring Weight Loss Proudness Viscosity Increase Piston Demerits

04/02 - Crankcase

% of Total Merits 25 25 20 20 10

Limits Absolute 0.0014 200 0.020 14 650 90 0.04

Preferred 0.0010 150 0.015 5.5 600 100 -

OEM Specification: Mack EO-L / Mack EO-L Plus Test

Parameter

Mack T-6

Oil Consumption (2100 rpm), lb/BHP hr. avg. max. Ring Weight Loss (Nos. 1 and 2 avg), mg. max. Ring Proudness, inches, max. Viscosity Increase, 100°C. cSt. max. Piston Demerits, max. Total Merits, min.* TGA soot at end of test, min. % Pressure differential across oil filter assembly, PSI. max. Oil Viscosity Increase, 100°C. from minimum during test. Total number of tests 1 2 3 Oil Consumption, lb/BHP hr. max. End of Test Oil Viscosity, TGA soot level

Mack T-8

Mack T-9

Top ring weight loss, mg. max. Cylinder liner wear, av. mls. max. PPM lead in 500hr oil analysis, max. EOT TBN (ASTM D4739), min.

Limits EO-L 0.0010 150 0.015 5.0 600 110 3.8 20 Viscosity increase 11.5 cSt. max. 12.5 cSt. max. 13.0 cSt. max. 0.0005 Report

11.5 cSt. max. 12.5 cSt. max. 13.0 cSt. max. 0.0005 Report

-

120 1.2 40 2.00

Note: * See EO-K/2 specification for explanation of Mack Merit Rating System. Approvals: Preferred viscosity: SAE 15W-40 for Mack EO-L; 15W-40 or 5W-40 (formulated with high VI base oil) for Mack EO-L Plus. Base Oil Characterisation Analysis: Data to be presented. Read across requests are evaluated on an individual basis depending on additive package, VI Improver and base-stock properties. Approved lubricant supplier agrees to participate in the Mack EO-L Monitoring Program. Application:

04/02 - Crankcase

1997 Vehicle Model Year V-MAC II engines, 6.0 min. Miles per Gallon Mack Centri-Max Rotor & Oil Filtration System

EO-L Plus 0.0010 100 0.015 5.0 600 120 3.8 20

OEM Specification: Mack EOM / Mack EOM Plus Test

Parameter

Mack T-8E (300 hr)

Viscosity Increase, 3.8% soot, cSt. Relative Viscosity, 4.8% soot Slope @ 4.8% soot Slope @ 275 hours or 5.8% soot Top Ring Weight Loss, mg. max. Cylinder Liner Wear, µm. Increase in Lead concentration, ppm. Increase in Lead, 400-500 hr. ppm. Increase in TAN Increase in TBN Cross Head Wear, 4.5% soot, mg. Filter Delta P. KPa. Avg. Sludge Rating Cross Head Wear, 6.5% soot, mg. Viscosity Increase, 64 hrs. %

Mack T-9

Cummins M11 (200 hr)

Cummins M11 (300 hr) Sequence IIIE Note: (1) According to ring batch Application:

V-MAC Engines Mack Centri-Max Rotor & Oil Filtration System.

Viscosity Grades:

SAE 10W-30, 15W-40 or SAE 5W-30, 5W-40, 10W-40 using unconventional base oils.

04/02 - Crankcase

Limits EOM 11.5 max. 2.1 max. 0.75 max. 1.00 max. 120 25.4 max. 25 max. 6.5 max. 79 8.7 -

EOM Plus 11.5 max. 1.8 max. 0.5 max. 0.75 max. 100/75(1) 25.4 max. 20 max. 10 max. 3.0 max. Rate & Report

12.0 max. 100 max.

Cummins Engine Oil Specifications CES

20071

API ACEA SAE Viscosity Grades

CH-4

Sulphated Ash, %. max. Tests Cummins M11 (200 hrs) Cummins M11 (300 hrs) Caterpillar 1P Caterpillar 1K Mack T-9 Mack T-8 (250 hrs) Mack T-8E (300 hrs) Roller Follower Wear Test Sequence IIIE HEUI Corrosion Bench Test OM 364A/LA OM 441LA OM 602A PDSC

20072

15W40 1.5 ✓

✓

✓ ✓ ✓

XW30 XW40 1.85

E5-99 10W30 10W40 15W40 1.85

✓ ✓ ✓ ✓

✓

✓ ✓ ✓ ✓ ✓

✓

✓

✓ ✓ ✓ ✓ ✓ ✓

✓ ✓ ✓

Cummins 20071 • Test limits as per AP1 CH4 category except Caterpillar IP with relaxed oil consumption limits. Cummins 20072 • Test limits as per ACEA E3-96 plus Cummins M11 HST test to API CH4 limits. Cummins 20076 • Test limits as per API CH4 category with the following modifications (ref table attached). Cummins 20077 • Test limits as per E5-99 category with the following modifications. Mack T8E - Relative viscosity at 4.8% soot to Cummins 20076 limits (1 test: 1.8 max. 2 test: 1.9 max. 3 test: 2.0 max.) OM602A - Cam Wear to 45.0 µm. max. Cummins M11 - Extended test limits for crosshead wear as per Cummins 20076. Crosshead Wear avg. mg. at 6.5% soot - 12.0 max.

04/02 - Crankcase

20077

CH4+ E3-96 10W30 10W40 15W40 1.85

10W30

20076

✓ ✓ ✓ ✓

Cummins 20076 Engine Performance Criteria Test

Primary Performance Criteria

1P

WDP (Weighted Demerits - 1P), max. TGC (Top Groove Carbon), % vol. max. TLC (Top Land Carbon), %. max. Avg. Oil Consumption, 0-360 hours Final Oil Consumption, 336-360 hours Crosshead Weight Loss, 6.5% soot mg. max. Sludge, min. (200hrs) Differential Pressure/Oil Filter, kPa. max. (200hrs) Avg. Liner Wear, µm. max. Top Ring Weight Loss, mg. max. Increase in Lead Content, ppm. max. Lead Increase from 400-500hrs max. ppm. Viscosity Increase, 3.8% soot cSt. max. Relative Viscosity, 4.8% soot max. WDK (Weighted Demerits - 1K), max. TGF (Top Groove Fill), % vol. max. TLHC (Top Land Heavy Carbon), %. max. Oil Consumption, g/bhp-hr. max. Piston, Ring, Liner Scuffing Pin Wear, mils. max. Viscosity Increase, %. max. Aeration Volume, %. max. Copper, ppm. Increase, max. Lead, ppm. Increase, max. Tin, ppm. Increase, max. Copper Corrosion, ASTM D130, max.

Number of Test Runs 1

CES 20076

M-11 (300hrs extended) T-9

T8-E 1K

6.5L IIIE HEUI Bench Corrosion

04/02 - Crankcase

8.7 79 25.4 120 20 11.5 1.8 332 24 4 0.5 None 0.30 100 8.0 20 120 50 3

2 Report Report Report Report Report 12.0 8.6 93 26.6 136 27 10 12.5 1.9 347 27 5 0.5 None 0.33 100 8.0 20 120 50 3

3

8.5 100 27.1 144 31 13.0 2.0 353 29 5 0.5 None 0.36 100 8.0 20 120 50 3

European OEM Seal Test Requirements for Automotive Engine Oils Test Conditions OEM Mercedes Benz

MAN

Volkswagen

Specs Sheets 229.1, 229.3 227.0/1 228.0/1 228.2/3 228.5 270, 271 M 3275 M 3277 500.00 501.01 502.00 505.00 503.00 506.00

04/02 - Crankcase

Test Method

Test Limits Hardness (Shore-A)

Volume (%)

Cracking

-20% max. -40% max.

-8/+2 -5/+5

0/+10 0/+5

-

-45 max.

-30% max.

-2/+6

-3/+10

-

168

-45 max.

-35% max.

-5/+5

0/+15

-

100

168

-30 max.

-20 max.

-10 max

0/+10

AK6

150

168

-40 max.

-30 max.

-5/+5

-2/+5

PV 3344

AK6

150

282

160 min.

8.0 MPa min.

Report

-

No cracks, 100% elongation after 30 mins.

PV 3344

AK6 ACM VAMAC

150 150 150

168 500 500

160 min. -40 max. -40 max.

7.0 MPa min. -40 max. -40 max.

-4/+10 -4/+10

-

None -

VDA 675301 Closed test cup

Elastomer

Temp. (°C)

Time (Hrs)

Elongation Tensile (%) Strength (%)

NBR 34 AK6 ACM E7503 EAM D8948-200

100 150

168 168

-35 max. -50 max.

150

168

150

NBR 28 DIN 53521

-

Driveline

Contents

Driveline

Automotive Gear: API Lubricant Service Designations SAE J306 Automotive Gear Viscosity Classification MIL-L-2105D Viscosity Classification Defence Standard 91-59/1 MACK GO-H Requirements MACK GO-J and GO-J PLUS Requirements MACK TO - A PLUS Requirements MAN 341 Specification MAN 342 Specification MAN 3343 Specification MIL-L-2105D/E Performance Requirements MT-1 Category Tests and Acceptance Criteria Scania STO: 1 Volvo Transmission Oil Specification 1273.07 and 1273.12 ZF Specifications: Master List

Industrial Gear: AGMA 9005-D94 Viscosity Grades and Specification A.F. Flender AG Approval Requirements David Brown Number S1.53 101 Specification DIN 51517 Part 3 Specification AISE (US Steel) 224 Requirements Comparison of Industrial Gear Oil Specifications

Automatic Transmission Fluids: Caterpillar TO - 4 Requirements Ford MERCON® Specification General Motors Allison C-4 Specification General Motors DEXRON® II, IIE and III Specifications

API Lubricant Service Designation for Automotive Manual Transmission(1) & Axles

This material was prepared by the Lubricants service Classification Task Force of the Fuels and Lubricants Committee, Marketing Department, American Petroleum Institute, to assist manufacturers and users of automotive equipment in the selection of transmission and axle lubricants for the operating conditions as described. In transmissions, and particularly in rear axles, gears of different designs are available for a variety of different service conditions. Selection of a lubricant for specific applications involves careful consideration of the operating conditions and the chemical and physical characteristics of the lubricant to meet these service conditions. Until recently, transmission and differential lubricants were described in qualitative terms and by a variety of designations, each one attempting to describe both the lubricant and the service conditions under which the lubricant must perform. Consideration of these lubricant designations to a minimum number was deemed highly desirable in the light of present day technology. The American Petroleum Institute, therefore, prepared six lubricant service designations for automotive manual transmissions and axles, each designation referring to the performance required of a gear lubricant for a specific type of automotive service. These designations also recognise the possibility that lubricant may be developed for more than one service classification and as a result may be so designated. In developing the language for the service classifications, a need was recognised to supplement the descriptions for certain gear lubricants, particularly those for hypoid gears, by referring to a series of tests which would serve as a “test language” to provide more detailed information on the performance requirements of such lubricant. This “test language” was developed by Section III of Technical Division B on Automotive Lubricants of ASTM Committee D-2, and reference is made to these test procedures in the API service designations described below. This system of designations replaced all previous API gear lubricant designations and became effective May 1, 1969. These designations are as follows:API-GL-1

Designates the type of service characteristic of automotive spiral-bevel and worm-gear axles and some manually operated transmissions operating under such mild conditions of low unit pressures and sliding velocities, that straight mineral oil can be used satisfactorily. Oxidation and rust inhibitors, defoamers, and pour depressants may be utilised to improve the characteristics of lubricants for this service. Frictional modifiers and extreme pressure agents shall not be utilised.

API-GL-2

Designates the type of service characteristic of automotive type worm-gear axles operating under such conditions of load temperature and sliding velocities, that lubricants satisfactory for API-GL-1 service will not suffice.

API-GL-3

Designates the type of service characteristic of manual transmissions and spiral-bevel axles operating under moderately severe conditions of speed and load. These service conditions require a lubricant having load carrying capacities greater than those which will satisfy API-GL-1 service, but below the requirements of lubricants satisfying API-GL-4 service.

04/02

Driveline

API Lubricant Service Designation

API-GL-4

This classification is still used commercially to describe lubricants, but the equipment required for the anti-scoring test procedures to verify lubricant performance is no longer available. Designates the type of service characteristic of gears, particularly hypoid(2) in passenger cars and other automotive type of equipment operated under high-speed, low-torque, and low-speed, high-torque conditions. Lubricants suitable for this service are those which provide anti-score protection equal to or better than that defined by CRC Reference Gear Oil RGO-105 and have been subjected to the test procedures and provide the performance levels described in ASTM STP-512A, dated March 1987(3).

API-GL-5

Designates the type of service characteristic of gears, particularly hypoid in passenger cars and other automotive equipment operated under high-speed, shock-load; high-speed, low-torque; and low-speed, high-torque conditions. Lubricants suitable for this service are those which provide anti-score protection equal to or better than that defined by CRC Reference Gear Oil RGO-110 and have been subjected to the test procedures and provide the performance levels described in ASTM STP-512A dated March 1987(2).

API-GL-6

This category is obsolete and is listed for historical reference only. The equipment used to measure performance is no longer available.

Footnotes:

(1). Automatic or semi-automatic transmissions, fluid couplings, torque converters, and tractor hydraulic systems usually require special lubricants. For the proper lubricant to be used, consult the manufacturer or lubricant supplier. (2). Limited - slip differentials generally have special lubricant requirements. The lubricant supplier shall be consulted regarding the suitability of their lubricant for such differentials. Information helpful in evaluating lubricants for this type of service may be found in the latest edition of ASTM & STP-512A. (3). The complete publication is titled “Laboratory Performance Tests for Automotive Gear Lubricants intended for API-GL-5 Service.”

Note:

04/02

API GL-4 oils are not suitable for highly-loaded hypoid axles. API GL-4 oils are used in synchronised manual transmissions and transaxles as well as in mild hypoid and spiral bevel axles.

Driveline

Axle and Manual Transmission Lubricant Viscosity Classification

SAE J306 Automotive Gear Viscosity Classification 70W Viscosity at 100°C min, mm2/s max, mm2/s Viscosity of 150,000 mPa.s, max temp °C 20 hr. KRL Shear (CRC L-45-T-93), KV100 after Shear, mm2/s

85W

80

85

90

140

250

4.1

75W

4.1 7.0 No requirement

80W

11.0

7.0 11.0

11.0 13.5

13.5 24.0

24.0 41.0

41.0 No req.

-55

-40

-26

-12

4.1

4.1

7.0

11.0

24.0

41.0

No requirement 7.0

11.0

13.5

MIL-PRF-2105E Specification Viscosity at 100°C min, mm2/s max, mm2/s Viscosity of 150,000 mPa.s, max temp °C Channel Point, min, °C Flash Point, min, °C

04/02 - Driveline

75W

80W-90

85W-140

4.1 -

13.5 24.0

24.0 41.0

-40

-26

-12

-45 150

-35 165

-20 180

DEF STAN 91-59/1 Lubricating Oil, Extreme Pressure Grades 75W and 80W90: Joint Service Designation OEP-38 and OEP-220 Respectively Property

Limits OEP-38 OEP-220 Clear homogenous and free from visual impurities

Appearance

Test Method Visual Examination

2

Kinematic Viscosity mm /s @100°C min. max. Viscosity Index, min. Low Temperature Viscosity: mPa.s @ -26°C max. @ -40°C max. Detection of Copper Corrosion Copper Strip Classification max Condition of Copper Strip Detection of Steel Corrosion Appearance of test piece Foaming tendency and stability characteristics: Sequence I, ml, max. Sequence II, ml, max. Sequence III, ml, max. Additive Elements Extreme Pressure Properties Mean Hertz Load, kg, min. Average Wear Scar Diameter mm max.

Thermal oxidation stability (TOST) Kinematic viscosity @ 100°C increase percent, max. Change in total acid number mg KOH/g, max. Pentane Insolubles % m/m, max. Toluene Insolubles % m/m, max. High Torque test Condition of Gear Teeth Condition of Half-Shaft and Axle Housing High speed shock

Storage Stability Solid % m/m, max. Liquid % volume, max.

4.1 85

13.5 24.0 -

150 000

150 000 -

3 No pitting or etching No rusting or pitting

20/0 20/0 50/0 50/0 20/0 20/0 See clause 6.1 75 0.5

100 3.0 3.0 2.0 The performance of the oil shall be superior to that of the CRC reference oil RGO 104 The performance of the oil shall be superior to that of the CRC reference oil RGO 110 0.25 0.50

BS 2000 Part 71 or ASTM D445: IP 71 ASTM 2270, IP 226 ASTM D2983 BS 2000 Part 154 or ASTM D130: IP 154 3 hrs at 121°C BS 2000 Part 135 ASTM D665: IP 135 Procedure A BS 2000 Part 146 ASTM D892/IP 146 See clause 6.1 IP 239 10 second run Ball Pot Maintained at 75 ± 1°C Load 40 kg Running Period 60 mins Annex A BS 2000: Part 71 or ASTM D445: IP 71 BS 2000: Part 177 or ASTM D664: IP 177 ASTM D 893 Procedure B ASTM D 893 Procedure B IP 232 Procedure B (1)

The Chrysler Avenger test rig has been found suitable (1)

Annex B

Note: (1) Test facilities for these tests are available at DQA/TS Woolwich. The above requirements are absolute and not subject to correction for tolerance of test method. This specification is currently (March 2000) under review.

04/02 - Driveline

MACK GO-H Test Power Divider Snap Test 5GT11

MIL-L-2105D Test for Transmission and Carrier Radial Lip Seal 5 GT 75

Timken Bearing Corrosion 09196 Thermal Oxidation Stability

Gear Oil Spalling Test 5 GT 71A Transmission Test for Evaluation of Thermally Stable Gear Oils 5 GT 73

Covering SAE 90, SAE 140, SAE 80W-90 and SAE 85W-140 oils Parameters Condition of cams and divider wedges: Breakage Chipping Scoring Hard snaps during test Full approval required Immersion at 93°C for 100 hours: Appearance Blistering Gum Tackiness Brittleness Swelling Sample heated for 6 hours at 150°C. Bearing dipped in sample and drained for 1 hr Bearing placed in humidity cabinet for 3 hrs @ 60°C in 100% humidity. Rust at end of test, max. 200g/sample in uncovered 400 ml. beaker for 100 hrs. at 150°C in a gravity convection oven Evaporation Loss, max, % Viscosity Increase at 99°C, max, % Precipitation Number, max. Minimum B 10 life of 50% above the GO-G reference No missed shifts and no measurable shifter fork wear at the centre of the pads

Note: The lubricant must be a blend from well-refined virgin base stocks (high viscosity index - 95 min.) compounded with load-carrying and lubricity ingredients. The oil shall be stable and contain no abrasive or corrosive ingredients.

04/02 - Driveline

Limits none none none none

as original none none none none none

none 10 15 0.65 160 hours minimum Minimum 65,000 cycles

Gear Oil Requirements

MACK GO-J and GO-J Plus

B)(1)

Highway (Class A, Vocational (Class AA, BB, C, CC)(1) Off-Road (Class D)(1) Test Rust Protection Copper Corrosion Foaming Tendencies Oil Seal Compatibility PG2 Oil Seal Compatibility Thermal Capability SS+C Storage Stability Compatibility Surface Protection Surface Protection Cyclic Durability Test Power Divider Snap Test Tapered Bearing Shear Spalling Test Wet Axle Gear Durability Field Testing Monitoring Program

Standard Drain (GO-J)

500,000 Miles or 3 Years 80,000 Miles or 1 Year 6 Months

250,000 Miles or 2 Years 40,000 Miles or 1 Year 6 Months

Procedure

Extended Drain Limits

Standard Drain Limits

ASTM L33 ASTM D130 ASTM D892 ASTM D5662 ASTM D5662 ASTM L-60-1 Fed. Test No. 791C Method 3440.1 Method 3430.2 ASTM L42 ASTM L37 ASTM D5579 MAT 700 WI DIN 51 350 Part 6, Test C

(2)

(2)

(2)

(2)

(2)

(2)

(2)

(2)

MAT 701 WI ASTM L-37 (Modified) MAT XXX WI -

Notes: (1) Vehicle classification as determined for Mack Trucks’ vehicle warranty. (2) ML-PRF-2105E Limits

04/02 - Driveline

Extended Drain (GO-J Plus)

(2)

(2)

100 hr. test -

(2)

(2)

(2)

(2)

(2)

(2)

(2)

-

Comment Section Section Section Section Section

3.3 3.4

(2)

(2)

1.5 times(2) Stay in Grade 17% Max. Change -

(2)

Stay in Grade 17% Max. Change -

(2)

Not Required

Section 3.9

500,000 miles Required

* Required

Section 3.10 Section 3.11

3.5 3.6 3.7

Section 3.8

Transmission Oil Requirements

MACK TO - A Plus

Extended Drain (TO-A Plus) A,B)(1)

Highway (Class Vocational (Class AA, BB, C, CC)(1) Off-Road (Class D)

Test Copper Corrosion Foaming Tendencies Oil Seal Compatibility Thermal Capability Cyclic Durability Compatibility Tapered Bearing Shear Scuffing Resistance (FZG) Field Test Monitoring Program Pour Point

500,000 Miles or 3 Years 80,000 Miles or 1 Year Not Available

Procedure

Extended Drain Limits

ASTM D130 ASTM D892 ASTM D5662 ASTM L-60-1 ASTN D5579 Fed. Test No. 791C Method 3430.2 DIN 51 350 Part 6, Test C ASTM D5182 ASTM D97

ASTM D5760 Limits ASTM D5760 Limits ASTM D5760 Limits 1.5 X ASTM D5760 Limits MIL-PRF-2105E Limits Stay in Grade, 17% Max. Change ASTM D5760 Limit 500,000 miles Required -40°C minimum

Note: (1) Vehicle classification as determined for Mack Trucks’ warranty.

04/02 - Driveline

Comment Section Section Section Section -

3.2

3.3 3.4 3.5

MAN 341 Specification Type SAE Viscosity Class Density at 15°C, g/ml Maximum Temperature at which the Brookfield Viscosity is 150,000 mPa.s,°C Kinematic Viscosity at 40°C, mm2/s Kinematic Viscosity at 100°C, mm2/s, min. Viscosity at 100°C after Shear (20hr. KRL), mm2/s Flash Point, °C, min. Pour Point, °C, max. Total Acid No., mg KOH/g Boron Content, mg/kg Phosphorus, % mass Chlorine, mg/Kg, max. Oxidation Stability (160°C/200hr) - CEC-L-48 Viscosity Increase @ 100°C, mm2/s Change in TAN, mg KOH/g Sludge Formation Steel Corrosion (DIN 51355 Method B), max. Copper Corrosion (3 hrs at 120°C), max. Foaming Tendency/Stability, ml, max. Sequence I Sequence II Sequence III MAN Seal Tests (168hr: 100°C NBR-28, 150°C AK6 & ACM 121433)

N and ML

SL

80W

80W90

85W90

90

Report -26 Report 7.0

Report -26 Report 13.5

Report Report 13.5

190 -27 Report Report Report 50

190 -27 Report Report Report 50

Report -12 Report 13.5 Stay in Grade 200 -21 Report Report Report 50

200 -21 Report Report Report 50

190 -40 Report Report Report 50

Report Report Report 1 1B

Report Report Report 1 1B

Report Report Report 1 1B

Report Report Report 1 1B

2 max 2 max None 1 1B

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

Testing Required for new Additive Technologies API GL-4 Performance FZG Pitting (C/8.3/90), 3 Runs, Hours, min. FZG Micropitting Test (C/8.3/90) FZG PITS Test (Ci80 TS) Field Test for SL Grades (half with retarders) Note: (1) Must be in grade: SAE 75W80W = 7.0 to 10.99 mm2/s. SAE 75W85W = 11.0 to 13.49 mm2/s. 04/02 - Driveline

Meet 90 Report > 2 x Reference Oil (Mobil NB80) 400,000 Km

75W80W 75W85W Report -40 Report (1)

MAN 342 Specification Type SAE Viscosity Class Density at 15°C, g/ml Maximum Temperature at which the Brookfield Viscosity is 150,000 mPa.s,°C Kinematic Viscosity at 40°C, mm2/s Kinematic Viscosity at 100°C, mm2/s, min. Viscosity at 100°C after Shear (20hr KRL), mm2/s Flash Point, °C, min. Pour Point, °C, max. Total Acid No., mg KOH/g Boron Content, mg/kg Phosphorus, % mass Chlorine, mg/kg, max. Oxidation Stability (160°C/200hr) -CEC-L-48 Viscosity Increase @ 100°C, mm2/s Change in Total Acid Number, mg KOH/g Sludge Formation Steel Corrosion (DIN 51355 Method B) Copper Corrosion (3 hrs at 120°C), max. Foaming Tendency/Stability, ml, max. Sequence I Sequence II Sequence III MAN Seal Tests (168hr: 100°C NBR-28, 150°C AK6 & ACM 121433)

N and ML 80W Report -26 Report 7.0

80W90 Report -26 Report 13.5

190 -27 Report Report Report 50

SL 90 Report Report 13.5

75W90 Report -40 Report 13.5

190 -27 Report Report Report 50

85W90 Report -12 Report 13.5 Stay in Grade 200 -21 Report Report Report 50

200 -21 Report Report Report 50

190 -40 Report Report Report 50

Report Report Report 1 1B

Report Report Report 1 1B

Report Report Report 1 1B

Report Report Report 1 1B

2 max. 2 max. None 1 1B

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

Testing Required for new Additive Technologies API GL-5 Performance FZG Pitting (C/8.3/90), 3 Runs, Hours, min. FZG Micropitting Test (C/8.3/90) FZG PITS Test (Ci80 TS) Field Test for SL Grades samples every 50,000 Km

04/02 - Driveline

Meet 90 Report > 2 x Reference Oil (Mobil NB80) 400,000 Km

MAN 3343 Specification Type SAE Viscosity Class Density at 15°C, g/ml Maximum Temperature at which the Brookfield Viscosity is 150,000 mPa.s,°C Kinematic Viscosity at 40°C, mm2/s Kinematic Viscosity at 100°C, mm2/s, min. Viscosity at 100°C after Shear (20hr KRL), mm2/s Flash Point, °C, min. Pour Point, °C, max. Total Acid No., mg KOH/g Boron Content, mg/kg Phosphorus, % mass Chlorine, mg/kg, max. Oxidation Stability (160°C/200hr) - CEC-L-48 Viscosity Increase @ 100°C, mm2/s Change in Total Acid Number, mg KOH/g Sludge Formation Steel Corrosion (DIN 51355 Method B), max. Copper Corrosion (3 hrs ar 120°C), max. Foaming Tendency/Stability, ml, max. Sequence I Sequence II Sequence III MAN Seal Tests (168hr: 100°C NBR-28, 150°C AK6 & ACM 121433)

N and ML 80W Report -26 Report 7.0

80W90 Report -26 Report 13.5

190 -27 Report Report Report 50

SL 90 Report Report 13.5

75W90 Report -40 Report 13.5

190 -27 Report Report Report 50

85W90 Report -12 Report 13.5 Stay in Grade 200 -21 Report Report Report 50

200 -21 Report Report Report 50

190 -40 Report Report Report 50

Report Report Report 1 1B

Report Report Report 1 1B

Report Report Report 1 1B

Report Report Report 1 1B

2 max 2 max None 1 1B

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

20/0 50/0 20/0 Pass

Testing Required for new Additive Technologies API GL-5 Performance FZG Pitting (C/8.3/90), 3 Runs, Hours, min. FZG Micropitting Test (C/8.3/90) FZG PITS Test (Ci80 TS) Field Test for SL Grades (half with retarders)

04/02 - Driveline

Meet 90 Report > 2 x Reference Oil (Mobil NB80) 400,000 Km

August 1987

Performance Requirements for MIL-L-2105D (GL-5) Lubricants SAE Viscosity Grade CRC L-60 Thermal Oxidation Stability

CRC L-33, 7 Day Moisture Corrosion CRC L-37 High Speed - Low Torque High Torque - Low Speed CRC L-42 High Speed-Shock Loading Axle Test ASTM D-130 Copper Strip Corrosion

75W

80W-90

85W-140

100 3 2

100 3 2

100 3 2

0 1

0 1

0 1

“Green” Gears “Lubrited” Gears

Pass Pass

Pass Pass

NR NR

Ring & Pinion Tooth Scoring, max. %

Equal to or better than RGO 110-90

100°C Viscosity Increase @ 50 hrs, max, % Pentane Insolubles, max, % Toluene Insolubles, max, % Rust on Gear Teeth Bearings, max. % Rust on Coverplate, max. %

Strip Rating, max.

Notes: NR: Not Required, if 80W90 passes in the same base stock. Lower L-37 and L-42 test temperatures are required for 75W oils.

04/02 - Driveline

3

3

NR

3

November 1997

Performance Requirements for MIL-L-2105E Lubricants SAE Viscosity Grade CRC L-60-1 Thermal Oxidation Stability

CRC L-33, 7 Day Moisture Corrosion CRC L-37 High Speed - Low Torque High Torque - Low Speed CRC L-42 High Speed-Shock Loading Axle Test Cycle Durability MACK Cycling Test ASTM D-130 Copper Corrosion/3 hrs @ 121°C Elastomer Compatibility Polyacrylate + Fluoroelastomer @ 150°C for 240 hrs ASTM D892 Foam Tendency/Stability, ml, max.

SS&C FTM 791 Storage Stability & Compatibility

100°C Viscosity Increase @ 50 hrs, max., % Pentane Insolubles, max., % Toluene Insolubles, max., % Carbon Varnish, min., Rating Sludge, max, Rating Rust on Gear Teeth Bearings, max., % Rust on Coverplate, max., % “Green Gears” “Lubrited” Gears Ring and Pinion Tooth Scoring, max., % No. of Cycles Strip Rating, max.

80W90

85W140

100 3 2 7.5 9.4

100 3 2 7.5 9.4

100 3 2 7.5 9.4

0 1

0 1

0 1

Pass Pass

Pass Pass

NR NR

Equal to or better than TMC 110

NR

Equal to or better than average of past 5 reference runs.

Elongation Change, min, % Hardness Change, Points Volume Change, %

3 Polyacrylate -60 -25 to + 5 -5 to + 30

Sequence I Sequence II Sequence III

20/0 50/0 20/0

20/0 50/0 20/0

20/0 50/0 20/0

Method 3340

Pass

Pass

Pass

Notes: NR: Not required, if 80W90 passes in the same base stock. Lower L-37 and L-42 Test Temperatures are required for 75W oils.

04/02 - Driveline

75W

3

3 Fluoroelastomer -75 -5 to + 10 -5 to + 15

MT-1 Category Tests and Acceptance Criteria Test Test method for Evaluation of the Thermal and Oxidative Stability of Lubricants used for Manual Transmissions and Final Drive Axles L-60-1 Viscosity Increase, % Pentane Insolubles, % Toluene Insolubles, % Carbon/Varnish Rating Sludge Rating Test method for determining Automotive Gear Oil compatibility with Typical Oil Seal Elastomers Polyacrylate @ 150°C, 240 hours Elongation change, % Hardness change, points Volume change, % Fluoroelastomer @ 150°C, 240 hours Elongation change, % Hardness change, points Volume change, % Test method for evaluating the thermal stability of manual transmission lubricants in a Cyclic Durability Test Cycles to fail Test method D130 for detection of copper corrosion from petroleum products by the Copper Strip Tarnish Test, 121°C, 3 hours Test Method D5182 for evaluating the scuffing (scoring) load capacity of oils Failing load stage Test Method D892 for foaming characteristics of lubricating oils (tendency only) Sequence I, ml Sequence II, ml Sequence III, ml Federal Test Method 791C, Method 3430.2, for compatability characteristics of Universal Gear Lubricant Federal Test Method 791C, Method 3440.1, for storage solubility characteristics of Universal Gear Lubricant

Minimum

Maximum

7.5 9.4

100 3.0 2.0 -

No limits +5.0 +30

-60 -20 -5

No limits +10 +15

-75 -5 -5

Better than passing reference oil

-

-

2a

11

-

Compatible with MIL-L-2105D oils(1)

20 50 20

Pass(2)

-

-

Notes: (1) Shall be compatible with specific reference oils when tested in accordance with Federal Test Method 3430.2. Reference oils may be obtained from SAE, 400 Commonwealth Drive, Warrendale, Pennsylvania, 15096. (2) Shall pass the performance requirements as specified in the MIL-L-2105D specification when tested in accordance with Federal Test Method 3440.1.

04/02 - Driveline

Scania STO: 1 Type

Requirements

Gear Oil

API

GL-5

STO(1) 1:0

API Shear Stability 20 hr KRL Shear (CRC-L-45-T-93)

GL-5

Filterability Thermal and Oxidation Stability, ASTM L-60-1(2) Notes: (1) Scania Gear Oil (2) MIL-PRF-2105E Limits

04/02 - Driveline

Limits

Viscosity change (%) less than or equal to RL181 Minimum 90% in stage 2 of CETOP RP124H using 5µm filter and 1.0 bar pressure Carbon varnish = 7.5 min. (on large gear only) Sludge = 9.4 min. (on both gears)

Volvo Transmission Oil Specification 1273.07 Test 3

Density, kg/m

Flash Point, COC, min, °C Pour Point, max, °C Viscosity at 100°C, mm2/s min. max. Viscosity Loss after Shearing, 20h, max, %

Limits

Test Method

To be stated

ASTM D1298

200 -48 9 12

ASTM D92 ASTM D97

5

Viscosity at -40°C, mPa.s, max. Oxidation Stability after 160°C/200h Viscosity Increase, 100°C, max, % Tan Increase, mg KOH/mg, max. Insoluble in Pentane, % by mass, max. Copper Corrosion, 3h, max, 150°C Rust Protection 24h

150,000

Rust Protection after Oxidation

No rust

Foaming Tendency, ml/ml Sequence I/II/III, max. Water Content, ppm, max. Solid Particles, code, max. Synchronization Properties Seal Compatibility Load Carrying Capacity, load stage, min. Surface Fatigue, gears Field Tests

10 1.0 0.1 1B No rust

50/0 200 18/13,

ASTM D445 ASTM D445 CEC L-45-T-93 ASTM D2983

CEC L-48-A-95

ASTM D130 ASTM D665 A ASTM D665 A CEC L-48-A-95 ASTM D892 ASTM D1744 ISO 4406

(1)

Pass 12 + 50% better than reference oil

VTM-02-95(2) CEC L-07-A-95

400,000 km

VTM-03-95(2)

VTM-01-96(2)

Notes: (1) The oil shall be tested in the Volvo test rig with approved results after 300,000 engagements (2) Volvo Test Method

04/02 - Driveline

Volvo Transmission Oil Specification 1273.12 Test kg/m3

Density, Flash Point, COC, min, °C Pour Point, max, °C Viscosity at 100°C, mm2/s, min. max.

Limits

Test Method

To be stated 200 -48 13.5 18

ASTM D1298 ASTM D92 ASTM D97

Viscosity Loss after Shearing, 20h, max, %

5

Viscosity at -40°C, mPa.s max. Oxidation Stability after 120°C/200h Viscosity Increase, 100°C, max, % Tan Increase, mg KOH/mg, max. Insoluble in pentance, % by mass, max. Copper Corrosion, 3h, max, 120°C Rust Protection 24h

150,000

Rust Protection after Oxidation

No rust

Foaming Tendency, ml/ml Sequence I/II/III, max. Water Content, ppm, max. Solid Particles, code, max. API Seal Compatibility Surface Fatigue, gears Field Tests Note: (1) Volvo Test Method

04/02 - Driveline

10 1.0 0.2 1B No rust

50/0 200 18/13 GL-5 Pass 50% better than reference oil 400,000 km

ASTM D445 ASTM D445 CEC L-45-T-93 ASTM D2983

CEC L-48-A-95

ASTM D130 ASTM D665 A ASTM D665 A CEC L-48-A-95 ASTM D892 ASTM D1744 ISO 4406 VTM-02-95(1) VTM-01-96(1) VTM-03-95(1)

ZF Specifications: Master List ZF List

Description

Required Performance

TE-ML 01

Manual non-synchronised API GL-4, MIL-L-2105 or API GL-5, constant-mesh transmissions MIL-L-2105D for commercial vehicles API CD / CE / CF / SF / SG, MIL-L2104C/D/E, MIL-L46152C/D/E TE-ML 02 Manual and automatic transmissions for trucks and buses Class 02A API GL-4, MIL-L-2105 Class 02B Gear oils in accordance with ZFN 13019 Class 02C Class 02D Class 02F TE-ML 03 Torque convertor transmissions for off-road vehicles and machinery (construction plant, special vehicles, lift trucks) TE-ML 04 Marine transmissions Class 04A

Class 04B Class 04C TE-ML 05 Axles for off-road vehicles Class 05A Class 05B Class 05C Class 05D TE-ML 06

SAE 30 / 40

SAE 80W / 80W85W/80W90 SAE 80W / 80W85W / 80W90 / 75W80 / 75W85 / 75W90 Engine oils in accordance with ZFN 13020 SAE 30 / 40 Semi-synthetic & synthetic gear oils SAE 75W80 / 75W85 / 75W90 in accordance with ZFN 13010 ATF in accordance with ZFN 13015 API CD / CE / CF / SF / SG, SAE 10W / 10W30 / 10W40 / MIL-L-2104C/D/E MIL-L-46152C/D/E; 15W40 / 20W20 Caterpillar TO-4 ; John Deere JDM J20C SAE 10W / 30 SAE 10W30 ® ® DEXRON IID / III, MERCON M; SAE 10W / 30 Caterpillar TO-4 ; John Deere JDM J20C SAE 10W30 Monograde engine oils – API CD / CE / CF-4 / CF / SF / SG / SH / SJ or ACEA SAE 30 (SAE 40 in hot countries) categories A / B / E Monograde engine oils in accordance with SAE 30 (SAE 40 in hot countries) ZFN 13024 Multigrade engine oils in accordance with SAE 10W40 / 15W40 ZFN 13024 Mineral oil based & semi-synthetic gear oils in accordance with ZFN 13011 Synthetic gear oils in accordance with ZFN 13011 Mineral oil based gear oils in accordance with ZFN 13011 with limited slip additives Synthetic gear oils in accordance with ZFN 13011 with limited slip additives

SAE 75W90 / 75W140 / 80W90 / 80W140 / 85W90 / 85W140 / 90 SAE 75W90 / 75W140 SAE 75W90 / 75W140 / 80W90 / 80W140 / 85W90 / 84W140 / 90 SAE 75W90 / 75W140

Tractor transmissions and hydraulic lifts

Class 06A

Engine oils – API CD / CE / CF-4 / CF / SF SG / SH / SJ or ACEA categories A / B / E STOU in accordance with ZFN 13022 (braking test) STOU in accordance with ZFN 13022

Class 06B Class 06C TE-ML 07

Viscosity Grades SAE 80W / 80W85W / 80W90 / 85W90 / 90

SAE 20W20 SAE 10W30 / 10W40 / 15W30 / 15W40 / 20W40 SAE 10W30 / 10W40 / 15W30 / 15W40 / 20W40

Hydrostatic & mechanical drives & electric drive systems

Class 07A

Gear oils in accordance with ZFN 13016

Class 07B

STOU in accordance with ZFN 13022

Class 07C

Lubricating oils in accordance with ZFN 13012 Engine oils – API CD / CE / CF-4 / CF / SF / SG / SH / SJ or ACEA categories A/B/E

Class 07D

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SAE 80W85 / 80W90 / 80W140 / 85W90 / 85W140 / 90 SAE 10W30 / 10W40 / 15W30 / 15W40 / 20W40 SAE 10W30 / 10W40 / 15W30 / 15W40 SAE 20W20 / 30/ 5W30 / 5W40 / 10W30 / 10W40 / 15W30 / 15W40 for powershift transmissions SAE 10W40 / 15W40 for mobile mixer drives

ZF Specifications: Master List ZF List

Description

TE-ML 08

Steering systems (non-power assisted) for cars, commercial vehicles & off-road vehicles

Class 08A TE-ML 09

TE-ML 11

Manual and automatic transmissions for cars

TE-ML 12

Axles for cars, commercial vehicles and buses. Axles, differentials, wheel heads & wheel hubs - 12A,12B,12C,12D Axles & differentials with multi disc self locking differentials – 12C & 12D

Class 12A

Class 12C Class 12D

SAE 75W80 / 75W85 / 75W90 / 80W / 80W85 / 80W90

Steering system with ZF Vane pump – ATF Other versions – ATF API CD / CE / CF/ SF / SG, MIL-L2104C SAE 20W20 (10W & 30 grade /D/E, MIL-L46152C/D/E for hot (>-10°C) or cold (<-10°C) ambient conditions for 3 DS 18 + WSK 244 * S5-28 & S5-31 : Esso ATF D21065 * S5-31 & S5-39 : Esso Gear Oil 304 * 3HP22&22Q;4HP14Q,18FL,18FLA, 18FLE,18Q,22,22EH,22HL,24&24A: Approved ATFs under 11A & 11B * 4HP20;5HP18,19FL,19FLA,19HLA, 24,24A&30: LT71141

ZF assemblies in special purpose vehicles Automatic transmissions for commercial vehicles

Class 14A

Mineral oil based ATFs in accordance with ZFN 13015 Semi-synthetic ATFs in accordance with ZFN 13015 Synthetic ATFs in accordance with ZFN 13015 Recommended alternatives from the passenger car application : Mineral oil based ATFs in accordance with ZFN 13015

Class 14B Class 14C Class 14D

TE-ML 15

Gear oils (API GL-4, MIL-L-2105)

Mineral oil based & semi-synthetic gear oils in accordance with ZFN 13016 Synthetic gear oils in accordance with ZFN 13016 Mineral oil based gear oils in accordance with ZFN 13016 with limited slip additives Synthetic gear oils in accordance with ZNF 13016 with limited slip additives

Class 12B

TE-ML 14

Viscosity Grades

Steering systems and oil pumps for cars, commercial vehicles & off-road vehicles

Class 09A Class 09B TE-ML 10 Transmatic for cars and commercial vehicles

TE-ML 13

Required Performance

Brake systems for special vehicles

04/02 - Driveline

SAE 75W90 / 75W140 / 80W90 / 80W140 / 85W90 / 85W140 / 90 SAE 75W90 / 75W140 SAE 75W90 / 75W140 / 80W90 / 80W140 / 85W90 / 85W140 / 90 SAE 75W90 / 75W140

Viscosity Ranges for AGMA Lubricants

AGMA 9005 - D94 Rust and Oxidation Inhibited Gear Oils

Viscosity Range

AGMA Lubricant No. 1 2 3 4 5 6 *7 Compounded *8 Compounded *8A Compounded

cSt (mm2/s) @ 40°C 41.4 to 50.6 61.2 to 74.8 90 to 110 135 to 165 198 to 242 288 to 352 414 to 506 612 to 748 900 to 1100

Notes: Viscosity Ranges for AGMA Lubricant numbers will henceforth be identical with those of the ASTM system. * Oils compounded with 3% to 10% fatty or synthetic fatty oils.

04/02 - Driveline

Equivalent ISO Grade

Extreme Pressure Gear Lubricants AGMA Lubricant No.

46 68 100 150 220 320 460 680 1000

2 EP 3 EP 4 EP 5 EP 6 EP 7 EP 8 EP 8A EP

Viscosity Ranges for AGMA Lubricants

AGMA 9005 - D94 Rust and Oxidation Inhibited Gear Oils

Viscosity Range

AGMA Lubricant No. 1 2 3 4 5 6 *7 Compounded *8 Compounded *8A Compounded

cSt (mm2/s) @ 40°C 41.4 to 50.6 61.2 to 74.8 90 to 110 135 to 165 198 to 242 288 to 352 414 to 506 612 to 748 900 to 1100

Notes: Viscosity Ranges for AGMA Lubricant numbers will henceforth be identical with those of the ASTM system. * Oils compounded with 3% to 10% fatty or synthetic fatty oils.

04/02 - Driveline

Equivalent ISO Grade

Extreme Pressure Gear Lubricants AGMA Lubricant No.

46 68 100 150 220 320 460 680 1000

2 EP 3 EP 4 EP 5 EP 6 EP 7 EP 8 EP 8A EP

Specification for R & O Gear Oils including Compounded Gear Lubricants

AGMA 9005 - D94 Property

Test Procedure

Criteria for Acceptance

Viscosity Viscosity Index Oxidation Stability

ASTM D-445 ASTM D2270 ASTM D-943 *Hours to reach a neutralisation number of 2.0 mg KOH/g ASTM D-665 B ASTM D-130 ASTM D-892

As specified 90 min.

Rust Protection Corrosion Protection Foam Suppression

Demulsibility

ASTM D-2711

Cleanliness

None

AGMA Grade Hours (minimum) 1.2 1500 3.4 750 5.6 500 No rust after 24 hours with synthetic sea water Class 1 after 3 hours @ 121°C Max. Vol. of Foam (ml) after 5 Minutes Blow 10 Minutes Rest Sequence I 75 10 Sequence II 75 10 Sequence III 75 10 Max. % water in oil after 5 hours 0.5 Max. cuff after centrifuging, ml 2.0 Min. total free water collected during entire test, ml 30.0 Must be free of visible suspended or settled contamination

Note: * The Criteria for acceptance indicated for Oxidation Stability and Demulsibility are not applicable to Compounded Gear Oils.

04/02 - Driveline

Specification for Extreme Pressure Gear Lubricants

AGMA 9005 - D94 Property

Test Procedure

Criteria for Acceptance

Viscosity

ASTM D-445

As specified

Viscosity Index Oxidation Stability Rust Protection Corrosion Protection Foam Suppression

ASTM ASTM ASTM ASTM ASTM

Demulsibility

ASTM D-2711

Cleanliness EP Property

None Timken Test (ASTM D2782) FZG Test (DIN 51354) None

Additive Solubility

04/02 - Driveline

D-2270 D-2893 D-665B D-130 D-892

90 min. Viscosity increase after 312 hours @ 121°C, 6% max. No rust after 24 hours with synthetic sea water Class 1 after 3 hours @ 100°C Max. Vol. of Foam (ml) after 5 Minute Blow 10 Minute Rest Sequence I 75 10 Sequence II 75 10 Sequence III 75 10 AGMA Grades 2EP to 7EP 8EP to 13EP Max. % water in oil after 5 hours 2.0 2.0 Max. cuff after centrifuging (ml) 1.0 4.0 Min. total free water collected during 80 50 entire test (start with 90ml of water) (ml) Must be free of visible suspended or settled contamination 60lb OK load > Load Stage 12 (A/8.3/90°C) Must be filterable to 25 microns (wet or dry) without loss of EP additive

22.07/ 1998 Rev 0

Flender Suitability Proof for Oils used in Flender Gear Units Test

Requirement

Company Mineral Oil

Flender Foam Test Original Oil Contaminated with 2% and 4% running-in oil (Castrol Alpha SP220S) Compatibility with Internal Coating (P22-8050) Compatibility with Elastomer Seals (72 NBR 902 and 75 FKM 585) Static Test (DIN 53521) Dynamic Test (DIN 3761) Compatibility with Sealing Compound (Loctite 128068) FZG Micropitting Test (FVA 54) Flender Grey Staining Test FZG Scuffing Load Test (A/16.6/90) Worm Gear Test Notes: I For cylindrical and bevel gearing II For worm gearing Not Required A Absolutely required B Required after agreement B3 Required for new additives

04/02 - Driveline

A.F. Flender AG Carl Diederichs Carl Freudenberg Loctite Various Flender Various RUB

Synthetic Oil

I

II

I

II

A A B3

A B3

A A A

A A

A B3 A B B -

A B B3 A

A B B3 A B B -

A B3 A

David Brown Number S1.53 101

January 1985

DBGI Specification for Mineral Based Lubricating Oils for use in Industrial Enclosed Gear Units. Scope:

This specification covers the requirements for ten grades and three classifications of mineral based lubricating oils for use in DAVID BROWN enclosed gear units. The grades are numbered 0 to 9 and will be associated with a classification character. M - straight mineral oils A - anti-wear or mild EP additive oils E - industrial extreme pressure additive oils

Description:

The lubricants shall be stable homogeneous blends of highly refined mineral oils and additives. They should not contain any grit, abrasives, sediments or other impurities. The lubricants should be branded products on general sale or intended to be so.

Classification:

For mineral based lubricant the following general classifications will be used: Type M These lubricants will usually contain additives to reduce corrosion, oxidation and foaming. They may contain other additives designed to improve their performance in service. They should not contain additives which will adversely affect the performance of sprag holdback (or similar) devices. Type A These lubricants will usually contain anti-wear or mild extreme pressure additives which improve the load carrying properties of the base oil. Type E These lubricants will contain additives which are designed to improve the load carrying properties of the base oil. They should not contain any lead or lead based additives. The requirements for all three lubricant types are the same or similar in all respects except for carrying capacity.

04/02

Driveline

David Brown Requirements for a Mineral Based Lubricant Title

Test Method

Kinematic Viscosity mm2/s

IP 71, ASTM D445

Viscosity Index Pour Point (°C) Load Carrying Capacity

IP 226, ASTM 2270 IP 15, ASTM D97 IP 334, A/8.3/90 (Visual method)

Corrosion

IP 154, ASTM D130

Corrosion

IP 135, ASTM D665

Oxidation Stability

04/02 - Driveline

ASTM D2893, (@ 95°C)

DBGI Lubricant Grade Conditions

Limit

0

1

2

3

4

5

6

7

8

9

@ 40°C @ 40°C @ 100°C

min. max. min. min. max.

24.5 36.0 5.1 90 -6

36.0 52.8 6.4 90 -6

52.8 77.6 8.1 90 -6

77.6 114 10.5 90 -6

114 167 13.6 90 -6

167 245 17.4 90 -3

245 360 22.3 90 -3

360 528 28.5 90 0

528 776 36.5 90 0

776 1140 46.2 90 0

min. min. min.

5 7 11

5 7 11

6 8 12

6 8 12

6 8 12

6 9 12

7 9 12

7 9 > 12

7 10 > 12

7 10 > 12

max.

1b

1b

1b

1b

1b

1b

1b

1b

1b

1b

10

10

FZG Load Stage at which damage occurs Lubricant Type M Lubricant Type A Lubricant Type E Copper Strip Classification after 3 hrs. @ 100°C Rust Prevention in the presence of water for 24hrs. Lubricant Type M Lubricant Types A & E % Change in Kinematic Viscosity @ 100°C

Pass Pass Report max.

PROCEDURES A AND B PROCEDURE A DEGREE OF RUSTING - PROCEDURE B 10

10

10

10

10

10

10

10

David Brown Requirements for a Mineral Based Lubricant

Title Foam Tendency/Stability

Test Method IP 146, ASTM D892

Air Release

IP 313

Demulsibility

ASTM D2711

ASTM D2711 Appendix 12

04/02 - Driveline

Conditions Volume of Foam (ml) Sequence I (24°C) After 5 mins blow After 10 mins rest Sequence II (93°C) After 5 mins blow After 10 mins rest Sequence III (24°C) After 5 mins blow After 10 mins rest Minutes @ 50°C Minutes @ 90°C Lubricant Types M & A Water in Oil (%) Emulsion (ml) Total Free Water (ml) Lubricant Type E Water in Oil (%) Emulsion in Oil (ml) Total Free Water (ml) (Report average result)

Limit

0

1

2

DBGI Lubricant Grade 3 4 5 6

7

8

9

max. max.

75 10

75 10

75 10

75 10

75 10

75 10

75 10

75 10

75 10

75 10

max. max.

75 10

75 10

75 10

75 10

75 10

75 10

75 10

75 10

75 10

75 10

max. max. max. max.

75 10 9 -

75 10 10 -

75 10 12 -

75 10 18 -

75 10 30 -

75 10 9

75 10 10

75 10 12

75 10 16

75 10 24

max. max. min.

0.5 2.0 30.0

0.5 2.0 30.0

0.5 2.0 30.0

0.5 2.0 30.0

0.5 2.0 30.0

0.5 2.0 300

0.5 2.0 30.0

0.5 2.0 30.0

0.5 2.0 30.0

0.5 2.0 30.0

max. max.

1.0 2.0

1.0 2.0

1.0 2.0

1.0 2.0

1.0 2.0

1.0 2.0

1.0 2.0

1.0 4.0

1.0 4.0

1.0 4.0

min.

60.0

60.0

60.0

60.0

60.0

60.0

60.0

50.0

50.0

50.0

September 1989

DIN 51517 Part 3 - Antiwear Circulating Oils Grade

CLP46

CLP68

CLP100

CLP150

CLP220

CLP320

CLP460

CLP680

ISO Viscosity Grade Flash Point (COC), °C, min. ISO 2592 Pour Point, °C, max. ISO 3016 Steel Corrosion (DIN 51355) FZG A/8.3/90, Load Stage Fail, min.

VG46 175

VG68 185

VG100 200 -12

VG150 VG220 200 200 -9 CLASS 0 - METHOD A 12

VG320 200 -6

VG460 200

VG680 200 -3

Notes: To be agreed as necessary:

To be undetectable:

04/02 - Driveline

-15

Density @ 15°C g/ml. (DIN 51757) Neutralisation no., mg. KOH/g (DIN 51558 Part 1) Sulphated Ash, %m. (DIN 51575) Copper Corrosion 3 hrs. @ 100°C (DIN 51759) Oxidation Stability (DIN 51586/ASTM D2893) NBR Compatibility, 168 hrs. @ 100°C (DIN 53538 Part 3) Water, %m. (DIN ISO 3733)

AISE (US Steel) Requirements No. 224 Lead Free E.P. Gear Oil Test API Gravity, D-287 Viscosity Index, D-567 Precipitation Number, D-91 Pour Point, D-97 C.O.C. Flash Point, D-92 ISO Grade 150 and up ISO Grade 68 and 100 3 Hour Copper Strip Corrosion, D-130 Rust Test (A & B), D-665 S-200 Oxidation - 312 hours @ 121.1°C (250°F) Viscosity Increase @ 98.9°C (210°F) Precipitation Number After Test Demulsibility, D-2711 Free Water Emulsion H2O in Oil Four Ball E.P. Test, D-2783 Load Wear Index Weld Point Four Ball Wear Test, D-2266 20 kg. @ 1800 rpm for 1 hour Timken Load Arm Test, D-2782 FZG - Four Square Gear Test

04/02 - Driveline

Limits 25 min. 95 min. Trace -9°C max. (based on viscosity) 232.2°C min. 203.4°C min. 1b max. Pass 6% max. 0.1% max. 80.0 ml min. 1.0 ml max. 2.0% max. 45 kg min. 250 kg min. Scar Diameter -0.35 mm max. O.K. 60 lbs min. 11th stage min.

Comparison of Industrial Gear Oil Specifications

Load Carrying Capacity Timken OK Load (ASTM D2782) lbs, min. FZG A/8.3/90, Pass Stage, min. 4-Ball (ASTM D2783), Weld Point, kg, min. LWI, min. 4-Ball (ASTM D2266) 20kg/1800 rpm/1 hr. Mean Wear Scar Diameter, mm, max. Corrosion Protection ASTM D130, 3 hrs/100°C, max. ASTM D 665, min. Oxidation Stability ASTM D2893, (121°C), % viscosity increase, max. S200, % viscosity increase, max. Precipitation Number, max. Foam Suppression, ASTM D892, Tendency/Stability, ml, max. Sequence I Sequence II Sequence III Demulsibility, ASTM D2711, Free Water, ml, min. Emulsion, ml, max. Water in Oil, %, max. Miscellaneous Seal Compatibility Notes: (1) Limits dependent upon viscosity grades (2) Limits to be agreed as necessary

04/02 - Driveline

AGMA 9005 - D94 EP

DIN 51517 Part 3 (CLP)

(AISE) 224

60 12

11

60 11

-

-

250 45

-

-

0.35

1b Pass B

(2)

Pass A

1b Pass A & B

6 -

(2)

-

6 0.1

75/10 75/10 75/10

-

-

50-80 (1) 1-4 (1) 2

-

80 1 2

-

(2)

-

Caterpillar TO - 4 Transmission and Drive Train Fluid Requirements

Physical Properties Rust Control Copper Corrosion Fluid Compatibility Homogeneity Foam, tendency/stability, mls

Flash Point Fire Point Elastomer Compatibility Fluoroelastomer

Allison C-4 Elastomer Test Oxidation Test Thermal Oxidation Stability (THOT) Sludge/varnish on parts, Total Acid Number Increase, Carbonyl Absorbance diff Further inspection

Requirements

Test Method

Less than 6 rust spots per linear inch on two out of three test specimens 1a max. No sedimentation or precipitation

Modified International Harvester BT-9 (175 hours under dynamic humidity conditions) ASTM D130 (2 hours at 100°C) Mix 50 mls test oil with 50 mls reference oil; heat to 204°C, cool to ambient; centrifuge for 30 min at 6000G Test oil held at -32°C for 24h, warmed to ambient, centrifuged ASTM D892 Part 1: No water added Part 2: 0.1% water in oil

No sedimentation or precipitation Sequence I - 25/0 Sequence II - 50/0 Sequence III - 25/0 160°C min. 175°C min. Av. Elongation of elastomer in aged test oil must not be greater than Av. Elongation with reference oil ∆ Elongation with test oil must be less than or equal to ∆ Elongation with reference oil + 10% See Allison C-4 Specification

ASTM D92 ASTM D92

ASTM D471 (240 hours; 150°C)

See Allison C-4 Specification

See Allison C-4 Specification Nil 4.0 max. 0.75 max. Fluoroelastomer input seal should not fail. Copper bushings should not undergo mechanical failure due to corrosion attack. Cooler will not be graded.

Viscosity after test Kinematic Viscosity, mm2/s Viscosity, mPa.s Viscosity, mPa.s Viscosity, mPa.s, 150°C, 106s-1 Note: * At the max. temperature specified in Section 4 for the appropriate viscosity grade. 04/02 - Driveline

Report Report Report Report

GM 6137 October 1990, Appendix E (ie DEXRON® IIE) (Fluoroelastomer input seal, production cooler, 35% silver)

ASTM D445 ASTM D2983* ASTM 4684* ASTM D683

Caterpillar TO - 4 Transmission and Drive Train Fluid Requirements

Physical Properties Rust Control Copper Corrosion Fluid Compatibility Homogeneity Foam, tendency/stability, mls

Flash Point Fire Point Elastomer Compatibility Fluoroelastomer

Allison C-4 Elastomer Test Oxidation Test Thermal Oxidation Stability (THOT) Sludge/varnish on parts, Total Acid Number Increase, Carbonyl Absorbance diff Further inspection

Requirements

Test Method

Less than 6 rust spots per linear inch on two out of three test specimens 1a max. No sedimentation or precipitation

Modified International Harvester BT-9 (175 hours under dynamic humidity conditions) ASTM D130 (2 hours at 100°C) Mix 50 mls test oil with 50 mls reference oil; heat to 204°C, cool to ambient; centrifuge for 30 min at 6000G Test oil held at -32°C for 24h, warmed to ambient, centrifuged ASTM D892 Part 1: No water added Part 2: 0.1% water in oil

No sedimentation or precipitation Sequence I - 25/0 Sequence II - 50/0 Sequence III - 25/0 160°C min. 175°C min. Av. Elongation of elastomer in aged test oil must not be greater than Av. Elongation with reference oil ∆ Elongation with test oil must be less than or equal to ∆ Elongation with reference oil + 10% See Allison C-4 Specification

ASTM D92 ASTM D92

ASTM D471 (240 hours; 150°C)

See Allison C-4 Specification

See Allison C-4 Specification Nil 4.0 max. 0.75 max. Fluoroelastomer input seal should not fail. Copper bushings should not undergo mechanical failure due to corrosion attack. Cooler will not be graded.

Viscosity after test Kinematic Viscosity, mm2/s Viscosity, mPa.s Viscosity, mPa.s Viscosity, mPa.s, 150°C, 106s-1 Note: * At the max. temperature specified in Section 4 for the appropriate viscosity grade. 04/02 - Driveline

Report Report Report Report

GM 6137 October 1990, Appendix E (ie DEXRON® IIE) (Fluoroelastomer input seal, production cooler, 35% silver)

ASTM D445 ASTM D2983* ASTM 4684* ASTM D683

Caterpillar TO - 4 Transmission and Drive Train Fluid Requirements Requirements Viscometric Properties

SAE J300 requirements plus additional low temp. and high temp. high shear requirements as shown opposite Caterpillar does not recommend oils that contain viscosity improvers in this application Wear Properties Gears Pumps

Friction Properties Link Model 1158 Oil/Friction Test Machine Dynamic Coefficient of Friction Static Coefficient of Friction Energy Capability Wear Properties - (7 friction disc-steel reaction plate combinations evaluated separately - 3 paper, 2 sintered bronze, 2 fluroelastomer friction discs.)

04/02 - Driveline

Test Method

SAE J300 Viscosity Grade

ASTM D2983 Maximum Temperature (°C) for Brookfield Viscosity of 150,000 mPa.s

ASTM D4684 Low Temp. Pumpability (MRV TP-1) 30,000 Centipoise Max, Temp. °C

ASTM D4683 (or Equiv) High Temp High Shear Viscosity at 150°C and 6 -1 10 s min. mPa.s

0W 5W 10W 20W 30 40 50 60

-55 -40 -35 -30 -25 -20 -15 +5

-45 -35 -25 -15 -15 -10 -5 +10

2.4 2.4 2.4 2.4 2.9 3.7 4.5 5.7

Average of three separate runs 100mg max. No single run with more than 150 mg weight

ASTM D4998 (FZG Machine - ‘A’ gears, low speed, 100 rpm, 121°C, load stage 10, 20 hours)

Total weight loss for all vanes from individual cartridges (not including intravanes), < 15 mg Ring weight loss, from individual cartridge, < 75 mg Pump parts, especially rings, should not have evidence of unusual wear or stress in contact areas.

Vikers pump test procedure for mobile systems as defined in publication form M-2952-S.

The results of each friction disc-reaction plate combination for the candidate oil must be within the allowable range of variation from the reference test oil.

Caterpillar VC 70 Standard Test Method

Ford MERCON® Specification Test Miscibility New Fluid Viscosity 100°C mm 2/s -10°C, mPa.s -18°C, mPa.s -20°C, mPa.s -30°C, mPa.s -40°C, mPa.s Evaporation loss, 150°C, 1 hr (Noack), % wt Viscosity after Noack, -40°C, mPa.s Flash Point °C, ASTM D92 Copper Strip, ASTM D130, 150°C, 3h Rust, ASTM D665A, 24h Vane Pump Wear (80°C/1000psi/100h), mg Colour, ASTM D 1500 Friction Durability Midpoint Dynamic Coef of Friction Low Speed Dynamic Coef of Friction Static Breakaway Coef of Friction (0.25s) Engagement Time, s Ratio of Low Speed to Dynamic Torque (S1/D) Ratio of Static Breakaway Torque to Midpoint, Dynamic Torque (S2/D) Notes: (1) Introduced February 1987 - now obsolete (2) Revised September 1992

04/02 - Driveline

Old Limit(1)

Current Limit(2)

No separation or colour change

No separation or colour change

6.8 min. 1700 max. 50000 max. 177 min. 1b max. No rust 15 max. 6.0 - 8.0

6.8 min. Rate & Report 1500 max. Rate & Report 20000 max. Rate & Report Rate & Report 177 min. 1b max. No rust 10 max. 6.0 - 8.0

120 to 150Nm. (between 5 & 4000 cycles) 155 Nm. max. at 5 & 200 cycles 90 to 130Nm (between 200 & 4000 cycles) 0.8 to 1.0 (between 5 & 4000 cycles) 0.90 to 1.0 (at 200 cycles)

0.13 to 0.16 (between 25 & 15000 cycles) 0.12 to 0.16 (between 25 & 15000 cycles) 0.10 to 0.15 (between 100 & 15000 cycles) 0.75 to 1.0 (between 25 & 15000 cycles) 0.90 to 1.0 (between 100 & 15000 cycles)

-

Rate & Report

Ford MERCON® Specification Old Limit(1)

Test Antifoaming Properties ASTM D892 Sequence I Sequence II Sequence III Sequence IV Elastometer Compatibility ATRR-100, Vol. Change, % Hardness Change, Pts ATRR-200, Vol. Change, % Hardness Change, Pts ATRR-300, Smear Test ATRR-400, Vol. Change, % Hardness Change, Pts ATRR-500, Vol. Change, % Hardness Change, Pts Aluminium Beaker Oxidation Test (ABOT) Pentane Insolubles, % TAN Change, 250h Diff IR Absorbance Change, 250h % Viscosity Increase, 40°C, 250h Viscosity, -40°C, mPa.s, 300h Volatility, % wt. Loss,300h Copper Strip Rating, 50h 300h Aluminium Strip Rating, 300h Sludge, 300h Turbo Hydra-matic Cycling Test (THCT) Shift Feel Test

Tendency 100 100 100 100

Stability 0 0 0 0 +1 to +6 -5 to +5 +3 to +8 -5 to +5 No reversion -

200 hr, < 1 5.0 max. 50 max. 50 max. 3b max. 3b max. No varnish No sludge As per GM DEXRON® Specification Shift performance equal to reference fluid

Notes: (1) Introduced February 1987 - now obsolete (2) Revised September 1992 04/02 - Driveline

Current Limit(2) Tendency 100 100 100 100

Stability 0 0 0 0 +1 to +6 -5 to +5 +3 to +8 -5 to +5 No reversion Rate & Report Rate & Report Rate & Report Rate & Report

250 hr, < 1 4.0 max. 40 max. 40 max. Rate & Report Rate & Report 3b max. 3b max. No varnish No sludge As per GM DEXRON® Specification Shift performance equal to reference fluid

C-4 Heavy Duty Transmission Fluid Specification

Allison Transmission Division General Motors Test Chemical Analysis Metals Content Barium Boron Calcium Magnesium Phosphorus Silicon Sodium Zinc Nonmetals Content Chlorine Nitrogen Sulphur Total Acid Number Total Base Number Infrared Spectrum Physical Properties Flash Point, °C min. Fire Point, °C min. Viscosity Characteristics Kinematic Viscosity @ 40°C Kinematic Viscosity @ 100°C Apparent Viscosity Brookfield Viscosity Stable Pour Point

Requirements

Test Method

Report Report Report Report Report Report Report Report

Emission spectroscopy: ICP Emission spectroscopy: ICP Emission spectroscopy: ICP Emission spectroscopy: ICP Emission spectroscopy: ICP Emission spectroscopy: ICP Emission spectroscopy: ICP Emission spectroscopy: ICP

Report Report Report Report Report Report

ASTM D808 ASTM D3228 ASTM D4951 or ASTM 129 ASTM D664 ASTM D4739 or D2896 ASTM E168

170 185

ASTM D92 ASTM D92

Report * Report * Report * Report Temperature at 3500 mPa.s Report *

ASTM D445 ASTM D445 ASTM D2602 ASTM D2983 ASTM D97

Note: * Fluids shall meet SAE J300 Viscosity grades and in addition ATFs must meet DEXRON® III and MERCON® requirements.

04/02 - Driveline

C-4 Heavy Duty Transmission Fluid Specification

Allison Transmission Division General Motors

Bench Tests Foaming Tendency Foam at 95°C, max. Foam at 135°C, mm max. Break time at 135°C, secs. max Copper Corrosion Corrosion/Rust Protection Rust Protection Elastomer Compatibility Nitrile: Volume difference, % Hardness difference, points Polyacrylate: Volume difference, % Hardness difference, points Silicone: Volume difference, % Hardness difference, points Fluoroelastomer: Volume difference, % Hardness difference, points Ethylene Acrylic: Volume difference % Hardness change, points Oxidation Stability, C-4 Oxidation Test (THOT) Viscosity Increase, 40°C, %, max. Viscosity Increase, 100°C, %, max. TAN Increase, max. Carbonyl Absorbance, max. Wear protection C-4 Vane Pump Wear Test, Total Weight Loss, mg, max. Clutch Frictional Characteristics C-4 Graphite Clutch Test C-4 Paper Clutch Friction Test

04/02 - Driveline

Requirements

Test Method

Nil 10 23 No blackening or flaking No visible rust on test pins No rust or corrosion on any test surface Limits are adjusted for each new elastomer batch -1.5 to + 6 -5 to + 5 0 +10 -5 to 0 +1.5 to 6.5 - 10 to 0 0 to + 4 -4 to + 4 +12 to + 28 -6 to -18

GM 6297-M,Test M

100 60 4.0 0.75

ASTM D130, 3 hours at 150°C ASTM D665, procedure “A” for 24 hours ASTM D1748, 98% humidity, 50 hrs at 40°C GM 6137-M, test J1, total immersion GM 6137-M, test J2, dip cycle GM 6137-M, test J1, total immersion GM 6137-M, test J1, total immersion GM 6137-M, test J1, total immersion

GM 6297-M (Appendix E)

15

ASTM D2882 mod. (a) 80 ± 3°C (b) 6.9 mPa

Mid-point dynamic co efficient and slip time must surpass limits set with minimum performance reference oil

Allison C-4 graphite clutch friction test Allison C-4 paper clutch friction test

A Comparison of GM DEXRON® II, IIE & III Specification Requirements General Motors ATF Specification GM 6137-M

DEXRON® II

DEXRON® IIE

DEXRON® III (GM 6417 - M)

Test

Method

Requirement

Requirement

Requirement

Colour Elemental Analysis

ASTM D1500

Not required

ASTM D4951

Not required

ASTM ASTM ASTM ASTM

Not Not Not Not

6.0 - 8.0 Report ppm: Ba, B, Ca, Mg, P Si, Na, Zn, Cu, S, Al, Fe, Pb Report, ppm: Cl Report, ppm: N Report, ppm: S Report No separation or colour change at end of test using reference fluid

6.0 - 8.0 Report ppm: Ba, B, Ca, Mg, P, Si, Na, Zn, Cu, S, Al, Fe, Pb Report, ppm: Cl Report, ppm: N Report, ppm: S Report No separation or colour change at end of test using reference fluid

Infrared Spectrum Miscibility

D808 D3228 D129 OR D 4951 E168

FTM 791C Method 3470.1

No separation or colour change at end of test

ASTM D445

Not Required 5.5 cSt min during and at end of oxidation and cycling tests

ASTM D92 ASTM D92

160°C min. 175°C min.

160°C min. 175°C min.

170°C min. 185°C min.

ASTM D2983

4000 mPa.s (4.0 Pa.s) max. at -23.3°C 50,000 mPa.s (50.0 Pa.s) max. at -40°C

Report Viscosity, mPa.s at -10°C 1,500 mPa.s max. at -20°C 5,000 mPa.s max. at -30°C 20,000 mPa.s max. at -40°C

Report, mPa.s at -10°C 1,500 mPa.s max. at -20°C 5,000 mPa.s max. at -30°C 20,000 mPa.s max. at -40°C

Kinematic Viscosity at 40°C at 100°C Flash Point Fire Point Brookfield Viscosity

04/02 - Driveline

required required required required

Report

Report

A Comparison of GM DEXRON® II, IIE & III Specification Requirements General Motors ATF Specification GM 6137-M

DEXRON® II

DEXRON® IIE

DEXRON® III (GM 6417 - M)

Test

Requirement

Requirement

Requirement

No blackening with flaking

No blackening with flaking

1b

No rust on test pins

Pass

Pass

No rust or corrosion on test panels

No rust or corrosion on any test surface

No rust or corrosion on any test surface

No foam at 95°C 10 mm max. at 135°C 23 s max. break-time at 135°C

No foam at 95°C 6mm at 135°C

No foam at 95°C 5mm max. height at 135°C

15 s max. break-time at 135°C

15 s max. collapse time at 135°C

Copper Strip Test Corrosion Test Rust Protection

Foam Test

Fluid Effect on Seals

Method ASTM D130 Mod 3 hr at 150°C ASTM D665 Procedure A ASTM D 1748 Mod Sandblasted Surface Temp. at 40°C Test Time of 50 hours GM

GM Method

Elastomers Nitrile Polyacrylate Silicone

Procedure 1 - Total Immersion Elastomer A (Polyacrylate) B (Nitrile)

The limits are assigned by GM for each batch of elastomer

C (Polyacrylate)

5 to 12

Hardness pts.

Change in Elastomer

Vol.,%

Hardness pts.

-8 to +1

A (Polyacrylate)

5 to 12

8 to + 1

0.5 to 5

-3 to +6

B (Nitrile)

1 to 6

-3 to + 6

2 to 7

-4 to + 4

2 to 7

-4 to +4

C (Polyacrylate)

0.5 to 5

-5 to +6

H (Fluorinated)

0.5 to 5

J (Silicone)

23 to 45

-30 to -13

J (Silicone)

23 to 45

-30 to - 13

13 to 27

-17 to -7

13 to 27

-17 to - 7

Acrylic)

04/02 - Driveline

Vol., %

H (Fluorinated) R (Ethylene/

Note: * Tensile strength and elongation are now required to be reported but no limits have been set yet.

Procedure 1 - Total Immersion*

Change in

R (Ethylene/ Acrylic)

-5 to + 6

A Comparison of GM DEXRON® II, IIE & III Specification Requirements General Motors ATF Specification GM 6137-M Test Method

DEXRON® II Requirement

Saginaw Power Steering Pump Test

GM Method

Parts condition to be equal to or better than that obtained with reference fluid

Vane Pump Wear Test

ASTM D2882 Mod 80+/-3°C 6.9 MPa GM Method

HEFCAD - Plate Clutch Test

DEXRON® II uses SD-715 Clutch Plates DEXRON® IIE uses SD-1777 Clutch Plates

DEXRON® III uses SD-1777 Clutch Plates

04/02 - Driveline

DEXRON® IIE Requirement

DEXRON® III (GM 6417 - M) Requirement

weight loss < 15mg

weight loss < 15mg

Satisfactory operation for 100 hours No unusual wear or flaking on test parts Between 20 and 100 hours of operation:150Nm < Midpoint Dynamic Torque <180Nm

Satisfactory operation for 100 hours No unusual wear or flaking on test parts Between 10 and 100 hours of operation:150Nm < Midpoint Dynamic Torque < 180Nm

Delta Torque < 14Nm

Maximum Torque > 150Nm

Maximum Torque > 150Nm

0.45s < Engagement Time < 0.75s

Delta Torque < 30Nm

DeltaTorque < 30Nm

Stop time between 0.45 and 60s

Stop time between 0.50 and 0.60s

Report End Torque Nm

Report End Torque Nm

Satisfactory operation for 100 hours No unusual clutch plate wear or flaking Between 24 and 100 hours of operation:115Nm < Midpoint Dynamic Torque < 175Nm

A Comparison of GM DEXRON® II, IIE & III Specification Requirements General Motors ATF Specification GM 6137-M

DEXRON® II

DEXRON® IIE

DEXRON® III (GM 6417 - M) Requirement

Test

Method

Requirement

Requirement

Band Clutch Test

GM Method Uses 3T40

Not Required

Satisfactory operation for 100 hours

Satisfactory operation for 100 hours

No unusual wear or flaking on test parts

No unusual wear or flaking on test parts

Between 20 and 100 hours of operation:-

Between 20 and 100 hours of operation:-

Band & Drum

145Nm < Midpoint Dynamic

Torque < 225Nm

End Torque > 170Nm

End Torque > 170Nm

Delta Torque < 80Nm

Delta Torque < 80Nm

Stop time between 0.40 and 0.60 s

Stop time between 0.35 and 0.55 s

Report Maximum Torque, Nm THOT - Oxidation Test

GM Method

Satisfactory operation for 300 hours

180Nm < Midpoint Dynamic

Torque < 220Nm

Report Maximum Torque, Nm

Satisfactory operation for 300 hrs.

Satisfactory operation for 300 hours

THM-350

Transmission parts cleanliness and physical

Transmission parts cleanliness & physical

Transmission parts condition must

DEXRON® II uses

condition must be equal to or better than

condition must be equal to or better than

be equal to or better than that

Transmission

that obtained with Reference Fluid

that obtained with Reference Fluid

obtained with Reference Fluid

Total Acid Number Increase, 7.0 max.

Total Acid Number Increase < 4.5

Total Acid Number Increase < 3.25

DEXRON® IIE and III

Carbonyl Absorbance Increase, 0.8 max.

Carbonyl Absorbance Increase < 0.55

Carbonyl Absorbance Increase < 0.45

use Hydra-matic 4L60

Min. O2 content of transmission effluent gas 2%

Min O2 content of transmission effluent gas 4%

Report effluent gas O2 content

Used Fluid Viscosity at -20°C < 3,000 mPa.s

Used Fluid Viscosity at -20°C < 2000 mPa.s

Used Fluid Viscosity at 100°C > 5.5 mm2/s

Used Fluid Viscosity at 100°C > 5.5 mm2/s

No cooler braze alloy corrosion

No cooler braze alloy corrosion

Transmission

Used Fluid Viscosity at - 23.3°C 6000mPa.s max;- 40°C Report Used Fluid Viscosity at 100°C, 5.5 mm2/s min. Cooler braze alloy condition shall be acceptable

No expulsion of ATF from Vent

04/02 - Driveline

A Comparison of GM DEXRON® II, IIE & III Specification Requirements General Motors ATF Specification GM 6137-M

DEXRON® II

DEXRON® IIE

DEXRON® III (GM 6417 - M)

Test

Method

Requirement

Requirement

Requirement

THCT - Cycling Test

GM Method

Satisfactory operation for 20,000 cycles

Satisfactory operation for 20,000 cycles

Satisfactory operation for 20,000 cycles

DEXRON® II uses THM 350 transmission

Transmission parts cleanliness & physical condition must be equal to or better than that obtained with the Reference Fluid

Condition of transmission parts must be equal to or better than that obtained with the Reference Fluid

Condition of transmission parts must be equal to or better than that obtained with the Reference Fluid

DEXRON® IIE and III

0.35s < 1-2 Shift Time < 0.70s

Total Acid Number Increase < 2.50

Total Acid Number Increase < 2.0

use Hydra-matic 4L60

0.20s < 2-3 Shift Time < 0.55s

Carbonyl Absorbance Increase < 0.35

Carbonyl Absorbance Increase < 0.30

transmission

Total Acid Number Increase, 6.0 max.

1-2 Shift Time between 0.35 and 0.75s

1-2 Shift Time between 0.30 and 0.75s

Carbonyl Absorbance Increase, 0.7,max.

2-3 Shift Time between 0.30 and 0.75s

2-3 Shift Time between 0.30 and 0.75s

Report 3-4 Shift Time, s

Report 3-4 Shift Time, s

Used Fluid Viscosity at 100°C 5.5 mm2/s min. 2

during and at end of test

Used Fluid Viscosity at 100°C, > 5.0 mm /s Used Fluid Viscosity at -20°C < 2000 mPa.s

Vehicle Performance Test ECCC Vehicle Performance Test Sprag Wear Test

04/02 - Driveline

Used Fluid Viscosity at 100°C, > 5.0 mm2/s Used Fluid Viscosity at -20°C < 2000 mPa.s

GM Method

Shift performance essentially equal to that obtained with the Reference Fluid

Shift performance essentially equal to that obtained with the Reference Fluid

No expulsion of ATF from Vent Shift performance essentially equal to thatobtained with the Reference Fluid

GM Method

Not Required

Not Required

Equal to or better than Reference Fluid

GM Method

Not Required

Not Required

Maximum Weight Loss - 60 mg

Industrial

Contents

Industrial

Hydraulic: AFNOR NF E 48-603 Parts 1 and 2 DIN 51524 Part 1 Specification DIN 51524 Part 2 Specification SEB 181222 Specification US Military Specifications MIL-L-17331H and MIL-L-17672D US Steel 126 and 127 Specifications VDMA 24568 Vegetable Oil, Synthetic Ester and Polyglycol Requirements Summary of Hydraulic Pump Test Conditions Comparison of Major OEM Hydraulic Oil Specifications

Compressor: DIN 51506 Standard [VB, VC, VBL, VCL and VDL Grades] ISO / DP 6521 Standard

Turbine: British Standard BS 489 DIN 51515 Specification General Electric GEK 32568-C Specification

Slideway: Cincinnati Machine P-47, P-50 and P-53 Specifications

French Hydraulic Lubricant Standards AFNOR NF E 48-603 (Part 1) Test

Requirements Category HM Class

Requirements Category HR Class

10 15 22 32 46 68 100 150 Kinematic Viscosity 9 13.5 19.8 28.8 41.4 61.2 90 135 2 at 40°C, mm /s 11 16.5 24.2 35.2 50.6 74.8 110 165 Viscosity Index ≥ 95 ≥ 90 Neutralisation + No. mg KOH/g Water Content, ≤ 0.05 % mass Foam, ml Tendency Stability Sequence I ≤ 100 ≤ 10 Sequence II ≤ 100 ≤ 10 Sequence III ≤ 100 ≤ 10 Flash Point, °C ≥ 100 140 ≥ 160 ≥ 180 Air Release, minutes

≤5

Aniline Point, °C

≥ 90

Copper Corrosion Rust Prevention Method A Flow Point, °C Anti-Wear Demulsibility, ml/min Shear Stability

≤7

10 9 11

15 13.5 16.5

22 19.8 24.2

32 46 28.8 41.4 35.2 50.6 ≥ 130

Requirements Category HV Class 68 61.2 74.8

100 90 110

150 135 165

10 9 11

15 13.5 16.5

22 32 46 68 100 150 19.8 28.8 41.4 61.2 90 135 24.2 35.2 50.6 74.8 110 165 ≥ 130

+

+

≤ 0.05 Tendency ≤ 100 ≤ 100 ≤ 100 ≥ 100 ≥ 140

≥ 160

Method

NFT 60-112

≤ 0.05 Stability ≤ 10 ≤ 10 ≤ 10 ≥ 180

Tendency ≤ 100 ≤ 100 ≤ 100 ≥ 100 ≥ 140

≥ 160

NFT 60-100 NFT 60-136

NFT 60-113 Stability ≤ 10 ≤ 10 ≤ 10 ≥ 180

≤ 10

NFT 60-129 NFT 60-118 NFE 48-614/ NFT 60-149 (for mineral oils)

≥ 95

≥ 90

≥ 95

<2

< 2

Pass ≤ -18 ≤ -15 ≤ -12 ≤ -9 Method to be defined by agreement between supplier and user on the basis of information by supplier 40.37.3/30

Pass ≤ -42

≤ -36

≥ 90

≥ 95 <2

NFM 07-021 NFM 07-015 (3hrs @ 100°C)

NFE 48-616 NFT 60-151 Pass Method A ≤ -30 ≤ -21 ≤ -12 ≤ -42 ≤ -36 ≤ -30 ≤ -21 ≤ -12 NFT 60-105 Method to be defined by agreement between supplier and user on the basis of a file provided by supplier

+ Variation of Viscosity @ 40°C < 10%

Variation of Viscosity @ 40°C < 10%

NFT 60-125* DIN 51382 for 250 cycles

Note: * Take 82°C +/- 1°C as the temperature of the heating bath for the products of which the degree of viscosity is ≥ 100, and 25°C for the products of which the degree of viscosity is ≤ 32. + Denotes that it may be useful to know the actual value for the characteristic and that the supplier should supply this. No minimum value is required however.

04/02 - Industrial

French Hydraulic Lubricant Standards AFNOR NF E 48-603 (Part 2) Test

Requirements Category HH Class 10

15

22

32

46

Requirements Category HL Class 68

100

150

10

15

22

32

46

Requirements Category HG Class 68

100

150

Kinematic Viscosity 9 13.5 19.8 28.8 41.4 61.2 90 135 9 13.5 19.8 28.8 41.4 61.2 90 135 2 @ 40°C, mm /s 11 16.5 24.2 35.2 50.6 74.8 110 165 11 16.5 24.2 35.2 50.6 74.8 110 165 Viscosity Index ≥ 95 ≥ 90 ≥ 95 ≥ 90 Neutralisation ≤ 0.05 + No. mg KOH/g Water Content, ≤ 0.05 ≤ 0.05 % mass Foam, ml Tendency Stability Sequence I ≤ 100 ≤ 10 Sequence II ≤ 100 ≤ 10 Sequence III ≤ 100 ≤ 10 Flash Point, °C ≥ 100 ≥ 140 ≥ 160 ≥ 180 ≥ 100 ≥ 140 ≥ 160 ≥ 180 Air Release, ≤5 ≤ 7 ≤ 10 minutes Aniline Point, °C ≥ 90 ≥ 95 ≥ 90 ≥ 95 Copper Corrosion Rust Prevention Method A Flow Point, °C

<2

<2

≤ -6

≤ -15 ≤ -12 ≤ -9

Demulsibility, ml/min Shear Stability

40.37.3/30

28.8 35.2

61.2 74.8 ≥ 95 +

NFT 60 - 112

0.05 Tendency ≤ 100 ≤ 100 ≤ 100 ≥ 160

NFT 60 - 113 Stability ≤ 10 ≤ 10 ≤ 10 ≥ 180

+ ≥ 95

≤ -9 Method to be defined by agreement between supplier and user on the basis of a file provided by supplier +

NFT 60 - 100 NFT 60 - 136

Pass ≤ -6

Anti-Wear

68

<2

Pass ≤ -15 ≤ -12 ≤ -9

Method

32

NFT 60 - 129 NFT 60 - 118 NFE 48 - 614/ NFT 60 - 149 NFM 07 - 021 NFM 07 -015 (3hrs @ 100°C) NFE 48 - 616 NFT 60 - 151 Method A NFT 60 - 105 As agreed NFT 60 - 125* DIN 51382 for 250 cycles

Note: * Take 82°C +/- 1°C as the temperature of the heating bath for the products of which the degree of viscosity is ≥ 100, and 25°C for the products of which the degree of viscosity is ≤ 32. + Denotes that it may be useful to know the actual value for the characteristic and that the supplier should supply this. No minimum value is required however.

04/02 - Industrial

Rust and Oxidation Protected Hydraulic Oils

DIN 51524 Part 1 (June 1987) Grade ISO Viscosity Class (DIN 51519) Kinematic Viscosity @ 0°C/(-20°C), mm2/s, max. Kinematic Viscosity @ 100°C, mm2/s, min. Pour Point, °C, max. (ISO 3016) Flash Point (COC), °C, min. (ISO 2592) Steel Corrosion, max. (DIN 51585) Copper Corrosion, max. (DIN 51759) Air Release, 50°C, minutes, max. (DIN 51381) Demulsibility, 54°C, minutes, max. (DIN 51599/ASTM D1401) Oxidation Stability, Acidity max. mg KOH/g @ 1000 hrs. (DIN 51587/ASTM D943) Behaviour towards the Relative SRE-NBR 1 sealant specified Change % in DIN 53538 Part 1, after 7 in volume days ± 2h @ 100 ± 1 °C Change in Shore A hardness Foam Volume, ml, max Sequence I DIN 51566 Sequence II Sequence III

04/02 - Industrial

HL10

HL22

VG10 90 (600) 2.4 -30 125

VG22 300 4.1 -21 165

HL32

HL46

VG32 VG46 420 780 5.0 6.1 -18 -15 175 185 Class 0 - Method A Class 2 - 100°C for 3 hours

5 30

HL68

HL100

VG68 1400 7.8 -12 195

VG100 2560 9.9 -12 205

10 40

14 60

2.0

0 to 18

0 to 15

0 to 12

0 to 10

0 to -10

0 to -8

0 to -7

0 to -6

150/0 75/0 150/0

Anti-Wear Hydraulic Oils

DIN 51524 Part 2 (June 1987) Grade ISO Viscosity Class (DIN 51502) Kinematic Viscosity @ 0°C/ (-20°C), mm2/s, max. Kinematic Viscosity @ 100°C, mm2/s, min. Pour Point, °C, max. (ISO 3016) Flash Point (COC), °C, min. (ISO 2592) Steel Corrosion, max. (DIN 51585) Copper Corrosion, max. (DIN 51759) Air Release, 50°C, minutes, max. (DIN 51381) Demulsibility, 54°C, minutes, max. (DIN 51599/ASTM D1401) FZG A/8.3/90: Load Stage Fail, min. Vane Pump Wear, mg, max. (DIN 51389/2) Ring Vanes Oxidation Stability, Acidity max. mg KOH/g @ 1000 hrs (DIN 51587/ASTM D943) Behaviour towards the Relative SRE-NBR 1 sealant specified Change % in DIN 53538 Part 1, after 7 in volume days ± 2h @ 100 ± 1 °C Change in Shore A hardness Foam Volume, ml, max Sequence I DIN 51566 Sequence II Sequence III

04/02 - Industrial

HLP10

HLP22

VG10 90 (600) 2.4 -30 125

VG22 300 4.1 -21 165

HLP32

HLP46

VG32 VG46 420 780 5.0 6.1 -18 -15 175 185 Class 0 - Method A Class 2 - 100°C for 3 hours

5 30

HLP68

HLP100

VG68 1400 7.8 -12 195

VG100 2560 9.9 -12 205

10 40

14 60

-

10

-

120 30 2.0

0 to 18

0 to 15

0 to 12

0 to 10

0 to -10

0 to -8

0 to -7

0 to -6

150/0 75/0 150/0

December 1997

German Steel Industry Specifications SEB 181222 Hydraulic Oil Type

HLP 22 2

Kinematic Viscosity, mm /s.

@ 0°C, max. @ 40°C ± 10% @ 100°C, min.

Pour Point, °C, max. Flash Point, °C, min. Water Content Rust Prevention, max. Copper Corrosion (3 hrs @ 125°C), max. Oxidation Stability, Acidity max. mg KOH/g @ 1000 hrs (DIN 51587/ASTM D943) Behaviour towards the SRE-NBR 1 sealant specified in DIN 53538 part 1, after 7 days ± 2 hrs @ 100 ± 1°C Contents of undisolved matter, % mass Air Release, @ 50°C, minutes, max Foam volume, ml, max. Sequence I Sequence II Sequence III Demulsibility @ 54°C, time to 40ml oil, minutes, max. FZG Gear Testing (A/8.3/90) Load Stage Fail, min. Work Related Weight Change, mg/ KWh Vane Pump Wear, mg, max. Ring Vanes Density @ 15°C, g/ml Ash % mass Neutralisation No., mg KOH/g Filterability Dry, %, min. Wet (0.2%, H2O), %, min.

04/02 - Industrial

300 22 4.1 -24 180

HLP 46

HLP 68

700 1260 46 68 6.2 8.0 -21 -18 200 220 Below the limit of quantative detectability Rating 0 Method B Rating 1 2,0

Relative change 0 to +8 in volume, % max. Shore A hardness, max. 0 to -6 Below the limit of quantative detectability 5 10 15 100/0 50/0 100/0 20 30 10

12 To be specified by supplier 60 15 Is to be specified by supplier Is to be specified by supplier Is to be specified by supplier 60 60

HLP 100 2200 100 10.2 -18 220

Test Method DIN 51550 + DIN 51562 DIN 51597 DIN/ISO 3016 DIN/ISO 2592 DIN/ISO 3733 DIN 51585 DIN EN ISO 2160 DIN 51587 DIN 53521 DIN 53505 DIN 51592 DIN 51381 DIN 53566 DIN 51599 DIN 51354 Part 2

DIN 51389 Part 2 DIN 51757 DIN 51575 DIN 51558 CETOP G6.15.37.GB

Major US Military Hydraulic Oil Specifications Military Specification Product Description

MIL-L-17331H Hydraulic, steam turbine

MIL-L-17672D Hydraulic, light turbine

74-97 8.0 0.3 204 40/37/3 65/0 65/0 65/0

32, 46, 68 Report 0.2 157, 163, 171 40/37/3 65/0 65/0 65/0

100 100 100 1000 1b Pass 2200

100 100 100 1000 1b Pass -

ASTM D130 ASTM D665B (Mod) ASTM D1947

0.33 Pass Pass

-

-

Performance Viscosity @ 40°C, mm2/s Viscosity @ 100°C, mm2/s, min. Total Acid No., mg KOH/g, max. Flash Point, °C, min. Demulsibility, 30 minutes Foam Test,Sequence I Sequence II Sequence III Oil Oxidation Test after 1000 hrs Total Sludge, mg, max. Total Iron, mg, max. Total Copper, mg, max. Time to reach TAN = 2.0, hrs, min. Copper Corrosion, max. Rust Test Ryder Gear Test P.P.I. min. 4-Ball Wear (15kg/80°C/600 rpm/2hrs) MWSD, max., mm Bearing Compatibility Valve Sticking

04/02 - Industrial

Test Method ASTM D445 or equiv. ASTM D974 ASTM D92 ASTM D1401 ASTM D892

ASTM D943

US Steel Hydraulic Standards US Steel 126 & 127 Performance Requirements Viscosity, D88 Viscosity Index, D567 COC Flash Point, D92 Hydraulic Pump Test, D2882 (100 hours @ 2000 psi) Four Ball Wear Test, D2266 (40 Kg, 1800 rpm, 130°F, 1 hr) Rotary Bomb Oxidation, D2272 Low Temp Cycling Test (U.S. Steel method) Water Emulsion Test, D1401 @ 130°F Rust Prevention Test, D665 A

04/02 - Industrial

126 Suitable for specified application 80 min. 375°F min. 0.05% Total Wear (450 mg max.) 0.80 mm scar diameter max. 120 minutes min. Must pass @ 15°F ml oil ml water ml emulsion minutes 40 37 3 ≤ 30 No rust

127

ml oil 40

Suitable for specified application 90 min. 375°F min. 0.01% Total Wear (90 mg max.) 0.50 mm scar diameter max. 120 minutes min. Must pass @ 15°F ml water ml emulsion minutes 37 3 ≤ 30 No rust

VDMA 24568 - Vegetable Oil Requirements ISO Viscosity Class Kinematic viscosity, DIN 51550, mm2/s @ -20°C @ 0°C, max. @ 40°C, max. @ 40°C, min. @ 100°C, min. Low Temperature Fluidity after 72 hrs ASTM D2532, °C Pour Point DIN ISO 3016, °C Flash Point DIN ISO 2592, °C Insolubles Contents DIN ISO 5884, % Water Content DIN 51777, max., mg/kg Steel Corrosion Test DIN 51585, max. Copper Corrosion Test DIN 51759, max. Baader Oxidation Test 95°C/72hrs, increase of Viscosity @ 40°C DIN 51554 Part 3, max., % Behaviour towards Sealing Materials after 1000hrs @ 80°C, CETOP R81H Change in Shore A hardnesss Relative Volume Change max. % Elongation max. % Force max. % Air Release at 50°C DIN 51381, max., minutes Foam Test ml ASTM D892 Sequence I max. Sequence II max. Sequence III max. Demulsification in minutes DIN 51599, @ 54°C FZG Gear Test load stage fail DIN 51354 Part 2 Mechanical Testing in the Vane Pump Test (mg wear) DIN 51389 Part 2 Ring max. Vane max. Density @ 15°C DIN 51757, kg/m3 Ash Content (oxides) DIN EN 7, % Neutralisation Value DIN 51558 Part 1 mg KOH/g

04/02 - Industrial

HETG 22 ISO VG 22

Requirements HETG 32 HETG 46 ISO VG 32 ISO VG 46

300 24.2 19.8 4.1

shall be given by the supplier 420 780 35.2 50.6 28.8 41.4 5.0 6.1

HETG 68 ISO VG 68

1400 74.8 61.2 7.8

shall be given by the supplier

165

shall be given by the supplier 175 185 below limit of quantification 1000 degree of corrosion 0-A degree of corrosion 2-100A3 20 HNBR, FPM, NBRI, AU ± 10 -3/ +10 30 30 7

10

150/0 75/0 150/0 shall be given by the supplier 10

120 30 shall be given by the supplier shall be given by the supplier shall be given by the supplier

195

VDMA 24568 - Synthetic Ester Oil Requirements ISO Viscosity Class Kinematic Viscosity, DIN 51550, mm2/s @ -20°C @ 0°C, max. @ 40°C, max. @ 40°C, min. @ 100°C, min. Pour Point DIN ISO 3016, °C Flash Point DIN ISO 2592, °C Insolubles Content DIN ISO 5884, % Water Content DIN 51777, max., mg/kg Steel Corrosion Test DIN 51585, max. Copper Corrosion Test DIN 51759, max. Baader Oxidation Test 110°C/72h increase of Viscosity at 40°C DIN 51554 Part 3, max, % Behaviour towards sealing materials after 1000h CETOP, R81H Temperature °C Change in shore A hardness Relative Volume Change max., % Elongation max., % Force max., % Air Release at 50°C DIN 51381, max, minutes Foam Test ASTM D892, ml, max Sequence I Sequence II Sequence III Demulsification @ 54°C, DIN 51599, minutes FZG Gear Test load stage fail DIN 51354 Part 2 Mechanical Testing in the Vane Pump Test (mg wear) DIN 51389 Part 2 Ring max. Vane max. Density @ 15°C DIN 51757, kg/m3 Ash Content (oxides) DIN EN 7, % Neutralisation Value DIN 51558 Part 1 mg KOH/g

04/02 - Industrial

Requirements HEES 32 HEES 46 HEES 68 ISO VG 32 ISO VG 46 ISO VG 68

HEES 22 ISO VG 22

300 24.2 19.8 4.1 -21 165

shall be given by the supplier 420 780 35.2 50.6 28.8 41.4 5.0 6.1 -18 -15 175 185 below limit of quantification 1000 degree of corrosion 0-A degree of corrosion 2-100A3

1400 74.8 61.2 7.8 -12 195

20

80 °C FPM, 80 °C FPM, NBR1, AU NBR1, AU ±10 -3/+10 30 30 7

100 °C FPM

10

150/0 75/0 150/0 shall be given by the supplier 10

120 30 shall be given by the supplier shall be given by the supplier shall be given by the supplier

VDMA 24568 - Polyglycol Requirements ISO Viscosity Class Kinematic Viscosity, DIN 51550, mm2/s @ -20°C @ 0°C, max. @ 40°C, max. @ 40°C, min. @ 100°C, min. Pour Point DIN ISO 3016, °C Flash Point DIN ISO 2592, °C Insolubles Contents DIN ISO 5884, % Water Content DIN 51777, max. mg/kg Steel Corrosion Test DIN 51585, max. Copper Corrosion Test DIN 51759, max. Ageing Test Neutralisation No. increase after 1000hrs DIN 51587, mg KOH/g Behaviour towards sealing materials CETOP RP81H Temperature, °C Change in Shore A hardness Relative Volume Change max. % Elongation max. % Force max. % Air Release @ 50°C DIN 51381, max. minutes Foam Test ASTM D892, ml, max Sequence I, Sequence II, Sequence III, FZG Gear Test load stage fail DIN 51354 Part 2 Mechanical Testing in the Vane Pump Test (mg wear) DIN 51389 Part 2 Ring max. Vane max. Density @ 15°C DIN 51757, kg/m3 Ash Content (oxides) DIN EN 7, % Neutralisation Value DIN 51558 Part 1 mg KOH/g

04/02 - Industrial

HEPG 22 ISO VG 22

300 24.2 19.8 4.1 -21 165

Requirements HEPG 32 HEPG 46 HEPG 68 ISO VG 32 ISO VG 46 ISO VG 68 shall be given by the supplier 420 780 35.2 50.6 28.8 41.4 5.0 6.1 -18 -15 175 185 below limit of quantification 5000 degree of corrosion 0-A degree of corrosion 2-100A3

1400 74.8 61.2 7.8 -12 195

2.0

60 °C HNBR, 80 °C HNBR, 100 °C HNBR, FPM FPM, NBR1 FPM, NBR1 ±10 -3/+10 30 30 5 10 300/0 300/0 300/0 10

120 30 shall be given by the supplier shall be given by the supplier shall be given by the supplier

Hydraulic Oil Pump Test Conditions Test

Pump Model

D-2882

Vickers 104C/105C Vane Pump

Denison HP Vane Pump

Model T5D-42

DIN 51389/2

Vickers 104C

Denison HP Piston Pump

Racine Vane Type

Model P-46 Axial Piston Model 35VQ25 Mobile Application Industrial Application Model S Variable Displacement

Denison HP Vane Type

Model T6C 020

Vickers HP Vane Pump

Volume (Litres per Min.)

Speed (RPM)

Time (Hrs)

Temp (°C)

28.4 @ 1000 PSI

1200

100

329

2400

24-30

1440

25

416

2400

60 @ 71.1 40 @ 98.9

227

2400

65.5 or 79.4 60 @ 71.1 40 @ 98.9

150(1)

Viscosity Dependant

93.3

Reservoir (Litres)

Pressure (Bar)

Filter (µm)

11.3 or 57

136

25

227

170

10

57

140

25

227

340

10

251

Appearance of Bronze on Shoes, Wear Plate & Port Plate

227

204

10

123

Ring & Vane Wt. Loss:

Pass/Fail Criteria

Ring & Vane Wt. Loss 50 mg. max. 121

Vane Contour Increase 0.015 in. max Ring & Vane Wt. Loss: Ring, 120 mg. max Vanes, 30 mg. max

Ring, 75 mg. max. 1800

73.9

Vanes, 15 mg. total

38

1775

1000

65.5 to 76.7

113

0 to 68 cycling

10

Ring & Vane Wt. Loss 45 mg. max.

114.8

1800

300 dry 300 wet (1% water)

80± 5

150

250

6

Visual Assessment

Note: (1) 3 x 50 hour tests using the same oil, but a new cartridge in each test. If one test fails, two additional tests must be run.

04/02 - Industrial

Input (kW)

Major OEM Hydraulic Oil Specifications Performance

Sludge & Metal Corrosion (1000 hr D943) Neutralisation No. (D974), mg KOH/g Sludge, mg Copper, mg Iron, mg. C.M. Thermal Stability Test (Procedure A) Results After Test Viscosity (D445, D2161), % change Neutralisation No. (D664), change Sludge or Precipitate, mg/100 ml Condition of Steel Rod Visual Deposits (per 200 ml), mg Metal Removed (per 200 ml), mg Condition of Copper Rod Visual (CM) Metal Removed (per 200 ml), mg Hydrolytic Stability (ASTM D2619) Copper Wt. Loss (mg/cm2) H2O Acidity (mg KOH/g)

Denison HF-2

Denison HF-0

1.0 max. 100 max. 200 max. 100 max.

1.0 max. 100 max. 200 max. 50 max.

100 max.

Report 10.0 max.

Report 10.0 max.

0.2 max. 4.0 max.

0.2 max. 4.0 max.

Note: Other bench testing is also required for Denison HF-2 and HF-0.

04/02 - Industrial

100 max.

Vickers

Cincinnati Machine P-68, P-69, P-70

Denison HF-1

Rust and Oxidation Cincinnati Machine P-38, P-54, P-55, P-57

100 max.

5 max. ± 50% max. 25 max.

5 max. 0.15 max. increase 25 max.

No discoloration 3.5 max. 1.0 max.

No discoloration 3.5 max. 1.0 max.

5 max. 10.0 max.

5 max. 10.0 max.

Major OEM Hydraulic Oil Specifications Performance

Pump Wear Test (ASTM D2882) Total wt. loss @ 100 hrs, mg Denison Axial Piston & Vane Pump Wear Tests (1) Vickers HP Vane Pump Test Weight Loss, mg Filterability (Denison procedure) Filtration Time without water Filtration Time with water

Rust Test (ASTM D665) 24 hrs Foam (ASTM D892) After 10 minutes Neutralisation No. (ASTM D664) mg KOH/g

Denison HF-2

Denison HF-0

Vickers

Denison HF-1

Rust and Oxidation Cincinnati Machine P-38, P-54, P-55, P-57

50 max. T6C 020

P-46 T6C 020

P-46 Ring - 75 max. Vanes - 15 max.

600 secs max. Not to exceed two times the filtration rate w/o water Procedure A & B

600 secs max. Not to exceed two times the filtration rate w/o water Procedure A & B

No Foam

No Foam

Note: (1) Both of these tests will be conducted in cooperation with Denison when deemed necessary.

04/02 - Industrial

Cincinnati Machine P-68, P-69, P-70

Procedure A

Procedure A & B

Procedure A

No Foam 1.5 max.

0.2 max.

Table 1 September 1985

Air Compressor Lubricant Standard DIN 51506

Oil Classification VDL VC VCL VB VBL Note: (1) Some types of compressors up to 180°C with VCL or engine oils.

04/02 - Industrial

Compressed Air Temperature °C maximum For compressors on moving equipment For compressors with storage tanks for brakes, signals and tippers and pipe network systems 220

220

220

160(1)

140

140

Table 2 Part 1: VB, VC, VBL and VCL Grades

Air Compressor Lubricant Standard DIN 51506 Lube Oil Group

VB and VBL

ISO Viscosity Class ISO ISO ISO ISO ISO ISO (DIN 51519) VG22 VG32 VG46 VG68 VG100 VG150 Kinematic Viscosity min. 19.8 28.8 41.4 61.2 90 135 (DIN 51561) to to to to to to max. 24.2 35.2 50.6 74.8 110 165 @ 40°C, mm2/s 4.3 5.4 6.6 8.8 11 15 @ 100°C, mm2/s, min. Flash Point, °C (COC) min. 175 195 205 210 (ISO 2592) Pour Point, °C, max. (ISO 3016) -9 -3 Ash, % m/m, max. (DIN 51675) VB & VC: 0.02 oxide ash Water soluble Acids (DIN 51558) TAN, mg KOH/g max. VB & VC: 0.15 (DIN 51558 Part 1) Water, % Mass (ISO 3733) % Mass CRC max. after air 2.0 ageing (DIN 51352 Part 1) % Mass CRC max. of 20% Not required distillation residue (DIN 51356) Note: Grades VB and VC are pure mineral oils. Grade VDL contains additives to increase ageing resistance. Grades VBL and VCL are HD type Engine oils which are used as mineral oils.

04/02 - Industrial

VC and VCL ISO VG220 198 to 242 19

ISO VG320 288 to 352 23

225

ISO VG460 414 to 506 30

ISO VG32 28.8 to 35.2 5.4

255

175

ISO VG46 41.4 to 50.6 6.6

ISO VG68 61.2 to 74.8 8.8 195

ISO VG100 90 to 110 11

ISO VG150 135 to 165 15

205

210

0 -9 VBL, VCL sulphated ash to be specified by supplier

-3

Neutral VBL, VCL to be specified by supplier 0.1 max. 2.5

1.5

2.0

0.3

0.75

Table 2 Part 2: VDL Grades

Air Compressor Lubricant Standard DIN 51506 Lube Oil Group ISO Viscosity Class (DIN 51519) Kinematic Viscosity (DIN 51561) @ 40°C, mm2/s @ 100°C, mm2/s, min. Flash Point, °C (COC) min. (ISO 2592) Pour Point, °C, max. (ISO 3016) Ash, % mass, max. (DIN 51575) Water soluble acids (DIN 51558) TAN, mg KOH/g, max. (DIN 51558 Part 1) Water, % mass (ISO 3733) % mass CRC max. after air ageing (DIN 51352 Part 1) % mass CRC max. after air/Fe2O3 ageing (DIN 51352 Part 2) % mass CRC max. of 20% distillation residue (DIN 51356) Kinematic Viscosity @ 40°C max. of 20% distillation residue mm2/s (DIN 51356)

04/02 - Industrial

VDL ISO VG32

ISO VG46

ISO VG68

ISO VG100

ISO VG150

28.8 to 35.2 5.4

41.4 to 50.6 6.6

61.2 to 74.8 8.8

90 to 110 11

135 to 165 15

205

210 -3

175

195 -9 Sulphated ash to be specified by supplier Neutral To be specified by supplier 0.1 max. Not required 2.5

3.0 0.3 Maximum of five times the value of the new oil

0.6

Draft - 1983

Air Compressor Lubricant Standard ISO/DP 6521 Mineral Oil-Based Lubricants for Reciprocating Compressors Category

ISO-L-DAA

Viscosity Grades Kinematic Viscosity @ 40°C, mm2/s ± 10%

68

100

150

32

46

68

100

150

32

46

68

100

150

32

46

68

100

150

@ 100°C, mm /s Pour Point(1), °C max. Copper Corrosion, max. Rust

To be stated -9 lb

To be stated -9 lb

No rust

No rust 54

82 30

15

1.5

ISO 3448 ISO 3104 (IP71) ISO 3016 (IP15) ISO 2160 (IP154) ISO/DP 7120A (IP135A)

No requirement 60

No requirement

ISO/DP 6614 (ASTM D1401)

ISO/DP 6617 Part 1 (DIN 51352)

2.0 Not applicable

20 2.5

Not applicable

Note: (1) When VG32 or VG46 oils are used in cold climate, pour points lower than -9°C are required.

04/02 - Industrial

Test Method

46

2

Emulsion Characteristics Temperature, °C Time (minutes) to 3 ml Emulsion, max. Oxidation Stability after ageing @ 200°C Evaporation loss, %, max. Increase in Conradson Carbon residue, %, max. after ageing @ 200°C Evaporation loss, %, max. Increase in Conradson Carbon Residue, %, max. Distillation Residue (20% vol) Conradson Carbon Residue, %, max. Ratio of Viscosity of residue to that of new oil, max.

ISO-L-DAB

32

ISO/DP 6617 Part 2 (DIN 51352)

3.0

0.3

0.6

5

ISO/DP 6616 with ISO/DP 6615 and ISO 3104

Draft - 1983

Air Compressor Lubricant Standard ISO/DP 6521 Mineral Oil-Based Lubricants for Rotary Screw Compressors Category

ISO-L-DAH

Viscosity Grades Kinematic Viscosity @ 40°C, mm 2/s ±10% Pour Point(1), °C max. Copper Corrosion, max.

ISO-L-DAG

Test Method

32

46

68

100

150

32

46

68

100

150

ISO 3448

32

46

68

100

150

32

46

68

100

150

ISO 3104 (IP71)

Rust

-9 1b

-9 1b

No rust

No rust

ISO 3016 (IP15) ISO 2160 (IP154) ISO/DP 7120A (IP135A)

Characteristics(2)

Emulsion Temperature, °C Time (minutes) to 3 ml Emulsion, max. Foaming Characteristics Sequence I Tendency, ml, max. Stability, ml, max. Oxidation Stability Evaporation Loss, %, max. Increase in Viscosity, % Increase in Acidity, % Sludge, % weight

54

82

82

30

30

300 nil

300 nil

To be decided

To be decided

Note: (1) When VG32 or VG46 oils are used in cold climate, pour points lower than -9°C are required. (2) Required only in those applications where condensation of atmospheric moisture is a problem. Where this does not apply, oils with dispersant additives, which tend to have poor water separating properties, may be used satisfactorily.

04/02 - Industrial

54

ISO/DP 6614 (ASTM D1401)

ISO/DP 6247 (IP146)

To be established

British Standard Specification BS 489: 1999 R & O Turbine Oils Test ISO Viscosity grade (BS 4231) Kinematic Viscosity, @ 40°C, mm 2/s min. max. Viscosity Index, min. Flash Point (COC), °C, min. Pour Point, °C, max. Demulsification number, seconds, max. Copper Corrosion Classification Acid Number mgKOH/g, max.

TO

TO

TO

32

46

68

100

BS reference

Technically identical with

28.8 35.2

41.4 50.6

61.2 74.8

90 110

BS EN ISO 3104

IP71

BS 2000: Part 226

IP 226/77

185

BS EN 22592

IP 34

-6

BS 2000: Part 15

IP 15

BS 2000: Part 19

IP 19

1

BS EN ISO 2160 (3 hr. at 100°C)

0.45

BS 2000 : Part 177

Pass

BS 2000 : Part 135 Procedure B (24 hr test), as amended by appendix A

IP 154 (3 hr. at 100°C) IP 1 Method A IP 135 procedure B (24 hr test), as amended by appendix A

BS2000: Part 146

IP 146

BS 2000: Part 313

IP 313

BS 2000: Part 280

IP 280

90

300

300

Rust-Preventing Characteristics Foaming Characteristics: Foaming Tendency, ml Sequence I, max. Sequence II, max. Sequence III, max. Foam Stability after 10 minutes, ml Sequence I, max. Sequence II, max. Sequence III, max. Air Release Value, minutes to 0.2% air content at 50° C, max. Oxidation Characteristics: Total Oxidation Products (TOP) % (m/m), max. Sludge % (m/m), max.

04/02 - Industrial

Test MethodsMethods

TO

360

360

400 50 400

400 50 400

400 100 400

400 100 400

Nil Nil Nil

Nil Nil Nil

20 10 20

30 10 30

5

6

7

10

0.70 0.30

0.80 0.35

0.80 0.35

0.80 0.35

DIN 51515 R & O Turbine Oils (L-TD) Test Lubricating Oil Group ISO Viscosity Grade Kinematic Viscosity at 40°C mm2/s min. max. Flash Point (COC), °C, min. Density at 15°C g/ml, max. Pour Point, °C, max. Neutralisation No., mg KOH/g Ash (oxide ash), % mass Water Content, % mass Content of solid foreign matter, % mass Water separation ability after steam treatment, seconds, max. Air Release Property at 50°C, minutes, max. Copper Corrosion 3 hrs at 100°C, rating, max. Corrosion Protection Properties with Steel Ageing Behaviour: Increase in Neutralisation No. after 1000 hours, mg KOH/g, max.

04/02 - Industrial

Limits

Test Methods

TD32

TD46

TD68

TD100

ISO VG 32

ISO VG 46

ISO VG 68

ISO VG 100

28.8 35.2 160

41.4 61.2 50.6 74.8 185 205 To be specified by supplier -6 To be specified by supplier To be specified by supplier Below the quantitative detectability limit

90.0 110 215

DIN 51 519 DIN 51 550 plus DIN 51 561 or DIN 51 562 ISO 2592 DIN 51 757 ISO 3016 DIN51 558 Part 1 DIN EN 7 ISO 3733

Below the quantitative detectability limit 300 5

5

DIN 51 589 Part 1

2 No rust

6

No value specified

DIN 51 381 DIN 51 759 DIN 51 585 A

2.0

DIN 51 587

GEK 32568-E Test Gravity (°API) Colour, max Pour Point (°F), max Viscosity 98.9°C (mm2/s) 40°C (mm2/s) Viscosity Index, min Neutralization No. (mg KOH/g), max Rust Prevention - B (24 hours) Flash Point (COC) (°F/°C), min Copper Corrosion, max Carbon Residue Ramsbottom, %, max Foam, ml, max

Sequence I Sequence II Sequence III

Turbine Oil Oxidation Test (hours, min) Oxidation Stability by rotating bomb (minutes), min Oxidation Stability by rotating bomb (modified) Air Release, (minutes), max

04/02 - Industrial

Recommended Value

ASTM Test Method No.

29-33.5 2.0 +10

D287 D1500 D97

5.1 to 5.7 28.8 to 35.2 95 0.20 Pass 420/215 1B 0.10 50/0 50/0 50/0 3000 500 > 85% of time in original test 5

D445 D2270 D974 D665 D92 D130 D524 D892 D943 D2272 D2272 D3427

Cincinnati Machine Slideway Specifications Chemical and Physical Properties API Gravity at 60°F Viscosity Grade SUS @ 100°F Kinematic Viscosity @ 40°C, mm2/s Colour, max Flash (C.O.C.), °F min. Flash (C.O.C.), °F min. Neutralisation No. (mg KOH/g oil), max Frictional Test Thermal Stability Method B Results after test Neutralisation No., mg KOH/g Precipitate or Sludge Condition of Steel Rod Condition of Copper Rod

04/02 - Industrial

P-47 (G-68) Heavy-Medium Way Oil

P-50 (G220) Heavy Way Oil

P-53 (HG-32) Combination Hydraulic and Way Oil

Test Method

18 to 27 typical ISO VG 68 317 to 389

18 to 27 typical ISO VG 220 1047 to 1283

20 to 30 typical ISO VG 32 149 to 182

ASTM D287 ASTM D2422 ASTM D2161

61.2 to 74.8

198 to 242

28.8 to 35.2

ASTM D445

330 360

350 410

8 315 355

ASTM D1500 ASTM D92 ASTM D9

1.7

1.7

0.60

ASTM D664

Ratio of static to Kinetic friction 0.80 max.

Ratio of static to Kinetic friction 0.80 max.

Ratio of static to Kinetic friction 0.80 max.

CM stick-slip test

0.5 max. increase None No deposit or discolouration 5 max.

0.5 max. increase None No deposit or discolouration 5 max.

0.2 max. increase None No deposit or discolouration 5 max.

ASTM D664

CM colour class

Tractor

Contents

Tractor

STOU Specifications: Massey Ferguson CMS-M1139 Ford ESN-M2C-159B John Deere J27 Massey Ferguson CMS-M1144

UTTO Specifications: Massey Ferguson M1127A Massey Ferguson M1127B Massey Ferguson M1135 Massey Ferguson CMS-M1143 Ford ESN-M2C-86C Ford ESN-M2C-134D John Deere J20C MS-1207

(Super Tractor Oil Universal)

STOU Specifications Test

API Engine Performance Kinematic Viscosity, 100°C, mm2/s

Massey Ferguson CMS-M1139 (May 1969)

Ford ESN-M2C-159-B (July 1984)

John Deere J27 (January 1992)

CD 10.1 - 12.0

CD/CE SAE 10W-30 SAE 15W-40

Viscosity -18°C (Brookfield), mPa.s, max. Pour Point, °C, max.

8000 -30

CD/SE B1 10W-30 B2 15W-30 B3 20W-40 NR NR

Flash Point, °C, min. (ASTM D92) Shear Stability IP297/77, % loss @ 100°C, max. JDQ102, Viscosity @ 100°C, mm2/s Foaming: (ASTM D892) Sequence I, ml max. Sequence II, ml max. Sequence III, ml max. + Water: Sequence I, ml max. Sequence II,ml max. Sequence III, ml max. Copper Strip Corrosion (3 hrs @ 150°C, max.) Rust Prevention: ASTM D665A MF Rust Test JDQ22, hrs min. Oxidation Test (100 hrs @ 150°C,) Viscosity Increase @ 100°C, %, max. Sludging Seal Test (168 hrs @ 120°C) Volume change, % Hardness change (+ 21 days @ 95°C), max. Seal Test (70 hrs @ 125°C) Volume Change, % (1) Hardness Change, points 4-Ball Wear Scar Diameter (1hr, 65°C, 1500 rpm 40 kg), mm, max. Load Wear Index, kg, min. IAE Gear Rig (2000 rpm, 110°C, 1pt/min.) Scuff Load, kg, min. Water Sensitivity (0.5% v/v) Sediment, ml, max. Water Separation, max. Additive Loss (% mass), max. Wet Brake Tests, various IPTO Clutch Tests, various Transmission Test

NR

190

NR -33 (10W-30) -30 (15W-40) NR

NR NR

10 NR

NR 7.1

NR NR NR

20/0 50/0 20/0

100/0 100/0 100/0

NR NR NR

NR NR NR

1a

1b

NR

NR Pass -

No Rust NR -

NR NR 100

10 None

10 NR

10 None

0 to +5

NR

NR

+10

NR

NR

NR NR

0 to +10 ± 10

NR

Note: (1) 180° bend test on itself - No cracks. 04/02 - Tractor

25/0 50/0 25/0

(30 sec. break time)

0.4

0.4

NR

55

NR

NR

52

NR

NR

NR NR Pass Pass Pass

0.1 Trace Pass Pass Pass

0.1 NR 15 Pass Pass Pass

STOU Specifications Test SAE Classification, J300D

Massey Ferguson CMS-M1144 5W-30 10W-30 10W-40 15W-30 15W-40 20W-40

Engine Performance API CCMC Kinematic Viscosity at 100°C after shearing, CEC L14A78 (250 Cycles), mm2/s. Flash Point (COC), NFT 60-118°C Copper Corrosion (3hrs @ 100°C), NF M 07-015 Rating Four Ball Wear (1h/40daN), ASTM D4172 Scar Diameter, mm Four Ball EP Test, ASTM D2783 Load Wear Index (LWI), kg FZG Test (A/8.3/90), CEC L07A85 Fail Stage Vickers V104C Vane Pump Test, NF E 48-617, 140 bar/250h/1460 rpm Ring and Vane Weight Loss, mg Rust Protection, ASTM D665B Rating Oxidation Test, CEC L48T94, 192h/150°C KV 100°C Change, % Total Acid Number Change, % Deposits Friction Test Dry Filterability (mod. AFNOR) Wet Filterability (mod. AFNOR) Pour Point, °C Foam -18°C Brookfield Viscosity

04/02 - Tractor

CD or CE D4 or D5 9.0 min. 200 min. 1a max. 0.4 max. 45 min. 9 min.

80 max. No Rust 25 max. 75 max. None Pass 1.5 max. Report 10°C below pumpability limit, max. Report Report

UTTO Specifications Test M1127A (October 1980) (U.S.A) Kinematic Viscosity, 100°C, mm2/s Viscosity -18°C, cP (Brookfield) Pour Point, °C Shear Stability, 100°C, mm2/s (ASTM D2603) Viscosity Index Copper Corrosion (3 hrs @ 150°C) (3 hrs @ 121°C) Foaming (+ water): Sequence I, ml Sequence II, ml Sequence III, ml Seal Test (168 hours/120°C): Volume % change Hardness (+21 days @ 95°C) Viscosity Stability on Heating; 100hrs @ 150°C % increase @ 100°C Sludge Steel Corrosion (MF methods): Time to fail, hrs Corrosion 4 Ball Wear: MWSD, mm (1 hr/65°C/1800 rpm/40 kg) MWSD, mm (1 hr/65°C/1500 rpm/40 kg) 4 Ball (ASTM D2783): LWI Weld Point, kg IAE Gear Rig (2000 RPM/110°C/1 pint per min.): Scuff Load, lb MF Four Square Rig Functional Tests Note: (1) Test as low temperature grade.

04/02 - Tractor

Massey Ferguson M1127B

M1135 (May 1969) (Europe)

11.0 max. 6000 max. - 30°C max.

9.6 max. 4000 max. - 30 max.

10.3 - 11.7 (99°C) 10000 max. - 26 max.

8.8 min.

7.3 min.

-

120 min. 1b max.

95 min. 1a max. 1a max.

50/0 max. 50/0 max. 50/0 max.

100/0 max. 100/0 max. 100/0 max.

0.5 to 10 10 IRHD max.

-2 to 5 10 IRHD max.

0 to 5 nil

10 max. nil

100 min. -

nil

0.5 max.(1) -

0.4 max.

30 min.(1) 200 min.(1)

-

Pass

135 min. Pass Pass

UTTO Specifications Test Kinematic Viscosity at 100°C, NFT 60-100, mm2/s Kinematic Viscosity at 100°C after shearing, CEC L14A78 (250 Cycles) KV 100, mm2/s Dynamic Viscosity at -18°C ASTM D2983, mPa.s Pour Point, NFT 60-105, °C Flash Point, (COC), NFT 60-118, °C Foaming Tendency/Stability NF T60-129 Sequence I (24°C), ml/ml Sequence II (93°C), ml/ml Sequence III (24°C), ml/ml Copper Corrosion (3h/100°C), NF M07-015 Rating Four Ball Wear (1h/40 daN), ASTM D4172 Scar Diameter, mm Four Ball EP Test, ASTM D2783 Load Wear Index (LWI), kg FZG Test (A/8.3/90), CEC L07A85 Fail Stage Vickers V104C Vane Pump Test, NF E 48-617, 140 bar/250h/1460 rpm Ring and Vane Weight Loss, mg Rust Protection, ASTM D665B Rating Oxidation Test, CEC L 48T94, 192h/150°C KV 100°C change, % Total Acid Number Change, % Deposits Elastomer Compatibility, CEC L39T87 RE1 (150°C): Fluoro-elastomers Var. in hardness DIDC, point Var. in tensile strength, % Var. in elongation rupture, % Var. in volume, % RE2 (150°C): ACM Var. in hardness DIDC, point Var. in tensile strength, % Var. in elongation rupture, % Var. in volume, % RE3 (150°C): Silicone Var. in hardness DIDC, point Var. in tensile strength, % Var. in elongation rupture, % Var. in volume, % RE4 (150°C): NBR Var. in hardness DIDC, point Var. in tensile strength, % Var. in elongation rupture, % Var. in volume, % Friction Test Dry Filterability (mod. AFNOR) Wet Filterability (mod. AFNOR)

04/02 - Tractor

Massey Ferguson CMS-M1143

9.0 min. 4000 max. -34 max. 200 min. 50/0 max. 50/0 max. 50/0 max. 1a max. 0.4 max. 45 min. 9 min.

80 max. No Rust 25 max. 75 max. None

0/+5 -50/0 -60/0 0/+5 -5/+5 -15/+10 -35/+10 -5/+5 -25/0 -30/+10 -20/+10 0/+30 -5/+5 -20/0 -50/0 -5/+5 Pass 1.5 max. Report

UTTO Specifications(2) Test

Kinematic Viscosity, 100°C, mm2/s Viscosity -20°C (D2602) mPa.s Viscosity -30°C (D2602) mPa.s Viscosity -18°C (Brookfield) mPa.s, max. Viscosity -35°C, mPa.s, max. Viscosity Index Pour Point, °C, max. Flash Point, °C, min. Shear Stability % change, max. Aniline Point Foaming: Sequence I, ml max. Sequence II, ml max. Sequence III, ml max. Foam Break Time (secs): + Water: Sequence I, ml. max. Sequence II, ml. max. Sequence III, ml. max. Copper Strip Corrosion 3 hrs @ 150°C Rust Prevention ASTM D665A Humidity Cabinet (min.) Oxidation Test (100 hrs @ 150°C) Viscosity Increase @ 100°C, % max. Oxidation Stability (JDQ 23) Evaporation Loss (%) Viscosity Increase (%) Sludge Formation Additive Separation Seal Test (70 hrs @ 125°C) Volume Change, % Hardness Change 180° bend 4-Ball MWSD, mm (1 hr/65°C/1500 rpm/40 kg) max. Water Sensitivity Sediment, ml. (% volume), max. Additive Loss (% mass), max. Water Separation, max. Compatibility 50/50 mix Wet Brake Tests Various IPTO Clutch Tests Various Transmission Tests Various Hydraulic Pump Tests Various Drive Line Durability Various Gear Wear Filterability

Ford ESN-M2C-86C (European)

Ford ESN-M2C-134D (November 1989) (U.S.A.)

John Deere J20C(1) (Revised) (Sept. 1992)

9.0 min. NR NR 4000 NR NR -37 190 -16 (D3945) NR

9.0 min. NR NR 4000 NR NR -37 190 -16 (D3945) NR

9.1 min. NR NR NR 70000 NR -36 200 7.1 (JDQ102) NR

6.2 min. 3500 max. 15000 max. NR NR 95 - 115 -37 195 NR

20/0 50/0 20/0 NR

20/0 50/0 20/0 NR

25/0 50/0 25/0 30 max.

50/10 50/10 50/10 NR

NR NR NR 2b max.

NR NR NR 2b max.

NR NR NR

50/10 50/10 50/10 NR

Pass NR

Pass NR

NR 100 hrs.

NR 100 hrs.

10

10

NR NR NR NR

NR NR NR NR

5.0 max. 10.0 max. None None

NR NR NR NR

0 to +10 ± 10 No cracks

0 to +10 ± 10 No cracks

NR NR

Various Various

0.4

0.4

NR

NR

0.1 NR Trace Pass Pass Pass Pass Pass NR Pass NR

0.1 NR Trace Pass Pass Pass Pass Pass Pass Pass NR

0.1 15 NR Pass Pass Pass Pass Pass NR Pass NR

91 - 110

Special Case Test

Notes: (1) J20D low viscosity UTTO for cold climates. Earlier UTTO specification versions on file. (2) UTTO = Universal Tractor Transmission Oil (not for tractor engines).

04/02 - Tractor

MS 1207 (Nov. 1986)

Special Case Test Pass Pass NR Pass NR Pass Pass Pass

Engine Tests

Contents

Engine Tests

European Tests: LEF/MAN 535 Mercedes Benz M111 Fuel Economy Test Mercedes Benz M111 Sludge Mercedes Benz OM 364LA Mercedes Benz OM 441LA Mercedes Benz OM 602A MWM KD 12E (MWM-B) Peugeot TU3M High Temperature Test Peugeot TU3M Valve Train Scuffing Peugeot XUD 11 BTE VW 1302 VW Intercooled T/C Diesel VW TDi Diesel

US Tests: Caterpillar 1G-2 Caterpillar 1H-2 Caterpillar 1K Caterpillar 1M-PC Caterpillar 1N Caterpillar 1P CRC L-38 Cummins M11 Detroit Diesel 6V-92TA Mack T-6 Mack T-7 Mack T-8/T-8E Mack T-9 Roller-Follower Wear Test Sequence IID Sequence IIIE Sequence VE Sequence VI

LEF/MAN 535 CEC L-50-T-99 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder, LEF/MAN 5305, turbocharged diesel engine. 2.0 litres, 43 kW (58.5 BHP).

Evaluation of SHPD oils against MAN QC 13-017 Specification.

Duration, hrs.

200

Speed, rpm.

2200

Oil Sump Temp., °C

115

Coolant Out Temp., °C

95

Fuel

CEC RF-90-A-92

Bore polishing, piston cleanliness and oil consumption rated.

Engine Tests

LEF/MAN 535 CEC L-50-T-99 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder, LEF/MAN 5305, turbocharged diesel engine. 2.0 litres, 43 kW (58.5 BHP).

Evaluation of SHPD oils against MAN QC 13-017 Specification.

Duration, hrs.

200

Speed, rpm.

2200

Oil Sump Temp., °C

115

Coolant Out Temp., °C

95

Fuel

CEC RF-90-A-92

Bore polishing, piston cleanliness and oil consumption rated.

Engine Tests

Mercedes Benz M111 Fuel Economy Test CEC L-54-T-96 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Standard production Mercedes Benz 2.0L gasoline injection with four valves per cylinder.

To evaluate the performance of engine oils in respect of fuel economy.

The test procedure is based upon the ECE R15-04 and EUDC emissions test cycles. It uses flying flush oil systems to compare oils against a base line calibration oil.

Fuel consumption through the test cycle is compared against that of a base line calibration oil. Reduction in fuel consumption is expressed as a % fuel economy benefit.

Engine Tests

Mercedes Benz M111 Sludge CEC L-53-T-95 Equipment Used:

Mercedes Benz M111 E20, four cylinder 2.0L gasoline injection with four valves per cylinder. Special engine required (bearings, piston rings, tappets, cams, timing chain, timing cover - cylinders differ in hardware set up). Modified gear box by-passed by one piece main shaft arrangement or standard gear box is used.

Purpose:

Test Conditions:

Method of Rating:

04/02

To evaluate the performance of engine oils to control the formation of black sludge on engine internal surfaces. Also measured are piston deposits and cam wear.

No run in. Phase 1:

48 hours of cyclic cold stage (includes 6 starts at -40°C ambient air temperature 25°C).

Phase 2:

1 hour power curve.

Phase 3:

75 hour alternating stage (21/2 min. 3750 rpm. W.O.T.; 21/2 min. 3850 rpm. W.O.T.).

Phase 4:

100 hours full cyclic stage based on M102E procedure with 10 steps of varying speed, load and temperature.

Fuel:

RF-86-A-96.

Black sludge (CRC Manual No.12). Cam wear. Piston cleanliness (DIN 51361 Part No. 2).

Engine Tests

Mercedes Benz OM 364LA CEC L-42-T-99 Equipment Used: Purpose:

Test Conditions:

Mercedes Benz OM 364LA, 4 litre turbocharged, intercooled diesel engine.

To evaluate piston deposits, wear, sludge, varnish, oil consumption.

The engine is run according to a cyclic procedure. Total duration 300 hours consisting of 3 x 100 hour phases of 20 x 21/2 hour cycles plus 50 hours steady state. Stage 1

Stage 2

Stage 3

Stage 4

Duration, hrs.

1.5

0.5

0.5

50

Speed, rpm.

2400

1500

1000

2400

Power, kW (bhp).

102 (137)

70 (94)

30 (40)

102 (137)

Coolant Outlet Temp., °C

30

Oil Temperature, °C

126

Oil Charge, kg. Fuel Specification

Method of Rating:

04/02

105

Intake Air Temp., °C

5.2 RF 90-A-92 (0.25 to 0.30% S)

Pistons rated for cleanliness, cylinder liners rated for bore polish and wear. Cams and followers rated for wear. Oil consumption reported.

Engine Tests

Mercedes Benz OM 441LA CEC L-52-T-97 Equipment Used:

Purpose:

Test Conditions:

Mercedes Benz OM 441LA EURO II V6, turbocharged, intercooled 250 kW engine with electronically controlled fuel pump.

To evaluate the performance of engine oils in respect of performance in low emission high performance diesel engines.

400 hour test programme. 50 hours cyclic (4 stages) followed each time by 50 hours constant speed/load.

Stage 1

Stage 4

Constant Speed

1900

1330

1140

2120

1900

Duration, hrs.

1.0

0.5

0.5

0.5

50

Power, kW (bhp).

250 (335) 210 (281) 185 (248) 2 (3) 105

Intake Air Temp., °C

25

Oil Temperature, °C

> 123

Oil Charge, kg. Fuel Specification

04/02

Stage 3

Speed, rpm.

Coolant Outlet Temp., °C

Method of Rating:

Stage 2

Piston cleanliness. Bore polish. Cylinder wear. Oil consumption. Sludge. Inlet system deposits. Turbocharger boost pressure drop.

Engine Tests

16.1 RF 93-T-95 (0.05 % S)

250 (335)

Mercedes Benz OM 602A CEC L-51-A-98 Equipment Used: Purpose:

Test Conditions:

Mercedes Benz OM602A indirect injection, five cylinder in-line, turbocharged.

To evaluate the performance of engine oils in respect of cam and cylinder wear under a combination of stop and go, medium speed and high speed operating conditions.

Complex test cycle of 60 mins., which is repeated 200 times giving a test duration of 200 hours. Currently 23 stages per cycle which includes 16 ramps. Max. oil temperature 142°C. Min. oil temperature 52°C.

Method of Rating:

04/02

Cylinder and cam wear. Oil viscosity increase. Piston cleanliness. Bore polish. Sludge.

Engine Tests

MWM KD 12E (MWM-B) CEC L-12-A-76, DIN 51361 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

MWM KD 12E, single cylinder, naturally aspirated 850cc diesel engine. Compression ratio 22 to 1.

To assess high performance diesel engine oils with respect to their influence on piston cleanliness.

Duration, hrs.

50

Speed, rpm.

2200

Power, kW (bhp).

10.7 (14.3)

Coolant Out Temp., °C

110

Oil Sump Temp., °C

110

Fuel Sulphur, %(1)

1

The three ring grooves and the first and second lands are assessed for deposits. Reporting of piston skirt and piston undercrown is optional. The piston rings are also checked for ring sticking. A final piston cleanliness rating is determined based on the five individual ring zone assessments.

Note:

04/02

(1) To CEC RF-91-A-81 specification.

Engine Tests

Peugeot TU3M High Temperature Test CEC L-55-T-95 Equipment Used:

Purpose:

Test Conditions:

Peugeot TU3M OHC four cylinder, 1360cc gasoline engine with mono-point fuel injection.

To evaluate the ability of a lubricant to control piston deposits, ring sticking and oil thickening during sustained high temperature running conditions.

The test comprises 96 hours of maximum speed and load running at elevated temperatures. Every 12 hours the engine is stopped for an automatic forced oil make up of 600g. Test

Oil Make Up

Duration, hrs.

96

10 (mins)

Engine (r/min).

5500

Idle/stopped

Power, kW (bhp).

50 Minm

0

Oil

150

Record

Coolant Out Temp., °C

110

Record

Fuel Cons. kg/hr.

16.5

-

Ignition advance is increased 2° and fuelling by 15% to increase test severity.

Method of Rating:

Note:

04/02

CEC M 02-A-78.

A replacement test based on the Peugeot TU5 engine should become available in 2000. It is unlikely to have any oil top-ups.

Engine Tests

Peugeot TU3M Valve Train Scuffing CEC L-38-A-94 Equipment Used:

OHC Peugeot TU3M, four cylinder gasoline engine, 1360cc, fitted with batch approved cams and followers.

Purpose:

The method is used to evaluate the performance of engine oils in respect of valve train scuffing in a combination of hot and cold running conditions.

Test Conditions:

The test comprises two individual sequences run under different test conditions. Total Duration, 100 hrs. Part A

Part B

Duration, hrs.

40

60

Engine Speed, rpm.

1500

3000

Engine Torque, Nm.

10

35

Oil Temp., °C

40

100

Coolant Out Temp., °C

45

90

Fuel Consumption, kg/hr.

1.5

4.0

Fuel: RF 83-A-91

Method of Rating:

04/02

The data is reported as ratings of the rocker pads according to the CEC M-02-A-78 test method and cam nose wear.

Engine Tests

Peugeot XUD 11 BTE CEC L-56-T-95 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Peugeot 2088cc, turbo-charged, indirect injection diesel engine with EGR pollution control system and electronic fuel injection.

To evaluate the performance of engine oils in respect of control of combustion soot. The evaluations are based on piston cleanliness and increase of viscosity.

Engine set-up balances fuel rate, fuel timing and boost pressure to achieve exhaust temperature of 800±20°C and Bosch smoke of 2.0±0.2; 75 hours of 2 mins idle; 27 mins. 4300 rpm. (2 x 30 sec ramps). Power from zero to above, kW

80

Coolant Out Temp., °C

100

Oil Gallery Temperature, °C

110

Fuel

RF 90-A-92

Forced Oil Make-up

every 8.5 hours

Oil viscosity increase at 3% soot content

CEC L-83-A-97

Soot content

CEC L-82-A-97

Piston cleanliness

CEC M-02-A-78

Engine Tests

VW 1302 DKA 6/79 Equipment Used: Purpose:

Test Conditions:

Method of Rating:

VW 1302, aircooled, four cylinder Boxer gasoline engine, 1.3 litre.

To evaluate gasoline crankcase oils with respect to engine wear, piston cleanliness and oil consumption.

Duration, hrs.

50

Speed, rpm.

4200 (wide open throttle)

Power, kW (bhp).

32.8 (44)

Oil Sump Temperature, °C

100

Oil Levelling

Every 10 hours

Fuel

Premium Leaded Gasoline DIN 51600

Oil consumption measured. Main, camshaft and big end bearings and piston rings are measured for wear. Piston lands, grooves, undercrown and skirt are assessed for deposits (100 merit = clean), according to the DIN procedure. NB. Skirt rating includes a lead paint deposit assessment.

04/02

Engine Tests

VW Intercooled T/C Diesel CEC L-46-T-93 Equipment Used: Purpose:

Test Conditions:

Method of Rating:

04/02

VW four cylinder, 1.6 litre, turbocharged and intercooled diesel engine.

Diesel detergency test for passenger car turbocharged diesel engines run under high load conditions.

Duration, hrs.

50

Speed, rpm.

4500

Power, kW (bhp).

55 (75)

Oil Temperature, °C

130

Water Temperature, °C

90

Fuel Sulphur, %

0.3

Pistons rated for groove and land deposits and for ring sticking.

Engine Tests

VW TDi Diesel CEC L-78-X-99, P-VW 1452 Equipment Used:

Purpose:

Test Conditions:

VW four cylinder, 1.9 litre, turbocharged, intercooled diesel engine with direct injection.

Diesel detergency test for passenger car diesel engines run under high load conditions.

Duration, hrs.

54

Speed, rpm.

4500

Power, kW (bhp).

82 (110)

Oil Temperature, °C

145

Water Temperature, °C

90

Fuel Sulphur, %

0.3

Test oil fill 4.5 Ltrs. No oil additions permitted.

Method of Rating:

04/02

Pistons rated for groove and land deposits and for ring sticking.

Engine Tests

Caterpillar 1G-2

Equipment Used: Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder supercharged diesel engine (1Y73).

Evaluation of ring sticking, ring and cylinder wear and piston deposits.

Duration hrs.

480

Speed, rpm.

1800

Power, kW (bhp).

42

Coolant Out Temp., °C

88

Fuel Sulphur, %

0.37 – 0.43

Engine rated for total piston demerits, top groove carbon filling and ring side clearance loss.

Engine Tests

Caterpillar 1G-2

Equipment Used: Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder supercharged diesel engine (1Y73).

Evaluation of ring sticking, ring and cylinder wear and piston deposits.

Duration hrs.

480

Speed, rpm.

1800

Power, kW (bhp).

42

Coolant Out Temp., °C

88

Fuel Sulphur, %

0.37 – 0.43

Engine rated for total piston demerits, top groove carbon filling and ring side clearance loss.

Engine Tests

Caterpillar 1H-2 ASTM STP 509A (Pt.II), FTMS 791C-FTM 346.2 Equipment Used: Purpose:

Test Conditions:

Single cylinder supercharged diesel engine (1Y73).

Diesel detergency test for high speed, medium severity supercharged conditions.

Duration, hrs.

480

Speed, rpm.

1800

Power, kW (bhp).

24.6 (33)

Oil Temperature, °C

82

Oil Charge

6 qts. (US)(≈ 5kg)

Fuel Sulphur, %

0.4

Oil Make Up

Forced make-up every 12 hours Oil change every 120 hours

Method of Rating:

Piston rated for deposits (grooves, lands, skirt) ring stick and ring side clearance. Calculated Total Weighted Demerit and Top Groove Fill (%) are the ratings of main importance.

04/02

Engine Tests

Caterpillar 1K ASTM RR: D-2-XXXX Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder supercharged diesel engine (1Y540) using one piece aluminium piston.

Diesel detergency test for high speed, severe supercharged conditions.

Duration, hrs.

252

Engine Speed, rpm.

2100

Power, kW (bhp).

67 (91)

Coolant Out Temp., °F

200

Inlet Air, °F/°C

260/127

Exhaust Gas, °F

1025

Inlet Air Pressure (in Hg).

71.1

Coolant Flow (galls. min).

17.3

Air Fuel Ratio

28.0

Fuel Injection Pressure (psi).

15,000

Fuel Sulphur, %

0.35 min.

Parameters assessed include piston deposits, oil consumption, piston ring projections and wear, liner polish and wear, and oil deterioration.

Engine Tests

Caterpillar 1M-PC

Equipment Used: Purpose:

Test Conditions:

Single cylinder supercharged diesel engine (1Y73).

Evaluation of ring sticking, ring and cylinder wear and piston deposits.

Duration, hrs.

120*

Engine Speed, rpm.

1800

Power kW, (bhp).

42

Coolant Out Temp., °C

88

Fuel Sulphur, %

0.4

* After 1 hour run-in

Method of Rating:

04/02

Piston and liner inspected. Cylinder liner and piston ring wear determined. Piston grooves and lands rated for carbon deposits.

Engine Tests

Caterpillar 1N

Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder supercharged diesel engine (1Y540) using one piece aluminium piston.

To determine acceptability of oils for Caterpillar engines, based on evaluation of oil consumption and piston deposits.

Duration, hrs.

252

Engine Speed, rpm.

2100

Power, kW (bhp).

67 (91)

Coolant Out Temp., ºC

93

Fuel Injection Pressure (psi).

15,000

Fuel Sulphur, %

0.05

Piston deposits rated to include top groove fill (TGF) %, top land heavy carbon (TLHC) % and weighted deposits (WDK). No stuck piston rings or piston, ring or liner distress are allowed. Average oil consumption measured.

Engine Tests

Caterpillar 1P

Equipment Used: Purpose:

Test Conditions:

Method of Rating:

04/02

Single cylinder, non-intercooled 1Y3700 engine.

Evaluation of piston deposits and oil consumption when using two-piece pistons with forged steel crown and aluminium skirt.

Duration, hrs.

360

Power, kW (bhp).

55 (74)

Engine Speed, rpm.

1800

Inlet Air Temp., °C

60

Oil Temp., °C

130

Fuel Injection Pressure, (psi)

28,000

Fuel Sulphur, %

0.03 – 0.05

Total Weighted Piston Deposits (WDP), Top Groove and Top Land Carbon (TGC and TLC) and oil consumption rated.

Engine Tests

CRC L-38 FTM 791C-FTM 3405.2, ASTM STP 509A Pt. IV Equipment Used: Purpose:

Test Conditions:

Labeco CLR laboratory oil test engine. Single cylinder, 0.69 litre, spark ignition.

To evaluate copper/lead corrosion, oxidation and deposit formation tendencies under high speed/high temperature conditions. Can also be used to assess shear stability.

Duration, hrs.

40

Speed, rpm.

3150

Power, kW (bhp).

Not controlled

Coolant Out Temperature, °C

93

Oil Temperature, °C

143*

*135°C for SAE 10W only.

Method of Rating:

Weight loss of bearings is measured. Engine parts are rated for varnish and sludge deposits. Shear stability data are obtained by measuring viscometric changes of samples taken at 10 hour intervals.

04/02

Engine Tests

Cummins M11

Equipment Used: Purpose:

Test Conditions:

1994 Cummins, 11 Litre in-line, six cylinder engine.

To evaluate soot abrasive wear of the valve train, oil filter plugging and sludge formation on the rocker covers.

Duration, hrs.

200*

Power, kW (bhp).

254 (341) - 275 (370)

Engine Speed, rpm.

1600 - 1800

Torque, Nm.

1340 - 1660

Coolant Out Temp., °C

88

Oil Gallery Temp., °C

115

* May run for 30 hours according to application. Engine runs 15% over-fuelled with alternate 50 hour cycles of retarded and standard timing.

Method of Rating:

04/02

Weight losses of valve cross-heads, sludge and differential pressure across oil filter are rated.

Engine Tests

Detroit Diesel 6V - 92TA

Equipment Used: Purpose:

Test Conditions:

Detroit Diesel 6V-92TA, six cylinder, two stroke turbocharged diesel engine.

Evaluation of ability of lubricant to protect critical cylinder components under typical conditions of use.

Duration 100 hrs, consisting of six cycles. Half of running at full load, other half at full rated power. Load Mode

Method of Rating:

04/02

Power Mode

Speed, rpm.

1200

2300

Power, kW (bhp).

300 – 320

490 – 510

Oil Sump Temp., °C

112 – 119

123 – 131

Oil Consumption, g/hr., max.

340

340

Coolant Out Temp., °C

84

84

Rings, liners, slipper bushings and piston skirts rated for distress which relates to overall engine life.

Engine Tests

MACK T-6 ASTM RR: D-2-1219, MACK 5GT 49 Equipment Used:

Purpose:

Test Conditions:

Mack ETAZ 673, six cylinder turbocharged, intercooled diesel engine. 11.0 litres.

High severity diesel detergency and ring wear test.

Total Duration,hrs.

600 (50 x 12 hr cycles) Phase 1

Phase 2

Phase 3

Time, hrs.

4

4

4

Speed, rpm.

1400

1800

2100

Power, kW (bhp).

141 (191)

168 (228)

174 (237) 113

Oil Sump Temp., °C max.

113

113

Coolant Out Temp., °C

88

88

88

Fuel Flow, lbs/hr.

91.6

110.1

122

Fuel Sulphur, %

0.1 – 0.3

12 samples are taken during the test for used oil analysis.

Method of Rating:

04/02

The five parameters as described in the Mack Merit Rating System are rated, reported and awarded a Merit Rating. The sum of the five ratings gives the total Mack Merit rating. See Section C.

Engine Tests

MACK T-7 ASTM RR: D-2-1220, MACK 5GT 57 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Mack EM6-285, six cylinder turbocharged, intercooled diesel engine. 11.0 litres, 283 bhp.

Evaluation of viscosity increase of lubricants in medium speed, turbocharged, intercooled four-cycle diesel engines.

Duration, hrs.

150 at full load

Speed, rpm.

1200

Power, kW (bhp).

132 (180)

Oil Sump Temp., °C

113

Coolant Out Temp., °C

85

Fuel Sulphur, %

0.5 max.

Viscosity increases from used oil analysis are measured.

Engine Tests

MACK T-8 / T-8E MACK 5GT 82 Equipment Used:

Purpose:

Test Conditions:

Method of Rating:

04/02

Mack E7-350, six cylinder turbocharged, intercooled diesel engine. 12.0 litres, 350 BHP.

Evaluation of viscometric performance and soot loading of engine oils in turbocharged and intercooled diesel engines.

Duration, hrs.

250 at full load (T-8) 300 at full load (T-8E)

Speed, rpm.

1800

Torque, lb/ft.

1010 – 1031

Oil Sump Temp., °C

102 – 107

Coolant Out Temp., °C

85

Fuel Sulphur, %

0.03 – 0.05

Viscosity increases from used oil analysis are measured. Test method also stipulates max. oil consumption of 0.0005 lbs/BHP/hr.

Engine Tests

MACK T-9

Equipment Used: Purpose:

Test Conditions:

1994 Mack, 12 Litre VMAC 11, in-line, six cylinder engine.

Evaluation of bearing, piston ring and cylinder liner wear.

Duration, hrs.

500

Power, kW (bhp).

265 (356) – 290 (390)

Engine Speed, rpm.

1250 – 1800

Oil Temp., °C

99 – 107

Coolant Out Temp., °C

85

First 75 hours of test with retarded timing to generate 1.5 – 2.0% soot. Remaining 425 hours at peak torque, 15% over fuelled to produce ring and liner wear.

Method of Rating:

04/02

Top ring weight loss, cylinder liner wear and increase in lead concentration (new/used oil) are measured.

Engine Tests

Roller-Follower Wear Test

Equipment Used: Purpose:

Test Conditions:

04/02

GM 6.5 Litre diesel engine.

Evaluation of valve train wear not related to soot.

Engine Speed, rpm.

1000

Power, kW (bhp).

30 (41) - 34 (46)

Coolant Out Temp., °C

120

Engine Tests

Sequence IID ASTM STP 315H Part 1 Equipment Used: Purpose:

Test Conditions:

5.7 litre Oldsmobile V8 gasoline engine with no exhaust gas recirculation.

Measures ability of oil to protect valves train components against rusting or corrosion under low temperature, short-trip service conditions.

Duration, hrs.

28

2

0.5

Speed, rpm.

1500

1500

S/D

3600

Power, kW (bhp).

18.6 (25)

18.6 (25)

S/D

74.6 (100)

Oil Temp., °C

49

49

S/D

127

43

49

S/D

Coolant Out Temp., °C Fuel

2

ASTM Approved Leaded Gasoline

Note: S/D = shutdown

Method of Rating:

04/02

Hydraulic valve lifter mechanisms are evaluated for rust and sticking.

Engine Tests

93

Sequence IIIE ASTM STR 315H Part 2 Equipment Used:

Purpose:

Test Conditions:

3.8 litre (231 CID) Buick V6. 8:1 compression ratio.

Evaluates an engine oil for its ability to minimise high temperature oxidation and thickening, sludge and varnish deposits, and wear.

Duration, hrs.

64

Speed, rpm.

3000

Power, kW (bhp).

50 (68)

Oil Temp., °C

149

Oil Pressure, (psi).

30

Blowby Rate, cfm.

16.5

Fuel

Leaded Gasoline (GMR 995) - 375 gallons

04/02

Engine Tests

Sequence VE

Equipment Used:

2.3 litre Ford four cylinder fast burn engine with electronic fuel injection, 9.5:1 compression ratio.

Purpose:

This test evaluates an engine oil for its ability to protect against sludge, varnish deposits and valve train wear.

Test Conditions:

Simulates severe field service characterised by a combination of low speed, low temperature “stop/go” city driving and moderate motorway operation. Total Duration, hrs.

04/02

288

Stage 1

Stage 2

Stage 3

Duration, mins.

120

75

45

Speed, rpm.

2500

2500

750

Power, kW (bhp).

25 (33.5)

25 (33.5)

0.75 (1.0)

Oil Temp., °C

68.3

98.9

46.1

Coolant Out Temp., °C

29.4

85.0

29.4

Fuel

Unleaded Gasoline (Phillips J)

Engine Tests

Sequence VI ASTM RR: D-2-1204 Equipment Used: Purpose:

Test Conditions:

04/02

Buick V6, 3.8 litre Gasoline Engine.

To evaluate Equivalent Fuel Economy Improvement (EFEI) of an oil.

Total Duration, hrs.

65

Stage 1

Stage 2

Stage 3

Duration, hrs.

13

32

20

Speed, rpm.

1500

1500

1500

Power, kW (bhp).

6 (8)

6 (8)

6 (8)

Coolant Out Temp., °C

54

93

110

Oil Temp., °C

66

107

135

Engine Tests

Rig Tests

Contents

Rig Tests

European Tests: CEC Tractor IPTO Test Denison T6C Hydraulic Vane Pump Test Ford Tractor Wet Brake Test Four-Ball Extreme Pressure Test Four-Ball Wear Test FZG Load-Carrying Capacity Test FZG Low Speed Test FZG Micropitting Test IP High Torque Test MB Planetary Gear Rig Schmidt/Ethyl Tribo Tester Slideway Oil Test Shear Stability Test - Kurt Orban The Brugger Test Timken Extreme Pressure Test VW Shear Stability Test ZF Synchroniser Rig

US Tests: Gear Oil Corrosion Test High Speed Axle Test High Speed Shock Test High Torque Axle Test Thermal Oxidation Stability Test

CEC Tractor IPTO Test

Scope:

Assesses the performance of a lubricant in maintaining the function of an IPTO (Independent Power Take-Off) wet clutch under conditions representing the most severe field operation.

Equipment:

A Ford New Holland 4600 tractor, with a modified hydraulic system and suitable instrumentation, is fitted with a new sintered bronze IPTO clutch pack.

Method:

Powered by the tractor engine, the IPTO clutch is stalled 100 times, in a continuously operated test taking approximately 3.5 hours, against a fixed stop. The time for each stall is recorded.

Rating:

The time for each stall is plotted against the stall number and the clutch pack is examined for wear and distortion.

Significance:

The test is required for a Ford New Holland tractor transmission and STOU lubricant approvals. Typical criteria are: Minimum number of complete stalls: 100. Mean stall time, secs: 1-3 at start, rising to not more than 4.5 through the test.

04/02

Rig Tests

CEC Tractor IPTO Test

Scope:

Assesses the performance of a lubricant in maintaining the function of an IPTO (Independent Power Take-Off) wet clutch under conditions representing the most severe field operation.

Equipment:

A Ford New Holland 4600 tractor, with a modified hydraulic system and suitable instrumentation, is fitted with a new sintered bronze IPTO clutch pack.

Method:

Powered by the tractor engine, the IPTO clutch is stalled 100 times, in a continuously operated test taking approximately 3.5 hours, against a fixed stop. The time for each stall is recorded.

Rating:

The time for each stall is plotted against the stall number and the clutch pack is examined for wear and distortion.

Significance:

The test is required for a Ford New Holland tractor transmission and STOU lubricant approvals. Typical criteria are: Minimum number of complete stalls: 100. Mean stall time, secs: 1-3 at start, rising to not more than 4.5 through the test.

04/02

Rig Tests

Denison T6C Hydaulic Vane Pump Test

Scope:

Equipment:

Method:

Rating:

Specification:

04/02

To evaluate the wear and filter blocking performance of hydraulic fluids in controlled conditions with and without water contamination.

Denison T6C Vane Pump Rig which circulates fluid while cycling the pump output pressure and maintaining fluid flow.

The same fluid is used for 2 305-hr test phases, first with < 0.05% water then with 1% water. A new pump cartridge is used for each phase.

Rating is carried out by Denison at their factory in Vierzon, France.

Denison Specification TP-30283.

Rig Tests

Ford Tractor Wet Brake Test

Scope:

Method:

The method evaluates the performance of oils in respect of noise control when used in tractor oil immersed brakes.

A Ford 6610, total weight of 9600 lbs (4355 kg), is used for a three part procedure which reflects noise provoking and brake stress conditions occuring in service. PART (A)

Deceleration/Stopping from maximum speed, both with a laden tractor and with tractor only.

PART (B)

Brake assisted spin turns.

PART (C)

A drag or fade test to simulate downhill running with continuous brake application.

The tractor is instrumented to record brake pedal effort deceleration, brake noise and brake oil temperature during each part of the test.

Rating:

Significance:

04/02

Tabulated and graphical results of the recorded data are presented, together with a subjective noise report.

The test is required for a Ford New Holland tractor transmission and STOU lubricant approvals.

Rig Tests

Four-Ball Extreme-Pressure Test ASTM D2783 Scope:

Covers two determinations of the load-carrying properties of lubricating fluids: (a) Load-Wear Index (formerly Mean Hertz load), and (b) Weld Point.

Equipment:

Method:

Load-Wear Index:

Weld Point:

Specifications:

04/02

A standardised machine design is used.

The four-ball EP tester is operated with one steel ball rotating against three steel balls held stationary in the form of a cradle. The lubricant under test covers the lower three balls. The speed of rotation is 1780 rpm. A series of tests of 10 seconds duration are made at increasing load until welding occurs.

An index of the ability of the lubricant to prevent wear at applied loads. The equation for load-wear index reflects the ability of a lubricant to carry a high load without welding and to allow only relatively small wear scars at loads below the weld point.

The lowest load in kilograms at which the rotating ball welds to the three stationary balls.

The user should determine to his own satisfaction whether the results correlate with field performance or other bench test machines.

Rig Tests

Four-Ball Wear Test ASTM D4172 Scope:

Equipment:

Method:

Specifications:

04/02

Covers a procedure for making a preliminary evaluation of anti-wear properties of fluid lubricants. Evaluation of greases using the same machine is detailed in Method D2266.

A standardised machine design is used.

Three 12.7 mm diameter steel balls are clamped together and covered with the lubricant under test. A fourth half-inch steel ball is pressed with a force of 147 or 392 N into the cavity formed by the three balls for the “three-point contact”. The temperature of the test lubricant is regulated at 75°C and the top ball is rotated at 1200 rpm for 60 minutes. Lubricants are compared by using the average size of the scar diameters worn on the lower three clamped balls.

The user of this method should determine to his own satisfaction whether the results of this procedure correlate with field performance or other bench test machines.

Rig Tests

FZG Load-Carrying Capacity Test IP334/DIN 51354 Scope:

Equipment:

Assess the relative load-carrying capacities of oils when used to lubricate steel/steel spur gears.

The FZG spur gear test rig consists of a closed power circuit with drive and test gears connected by two torsion shafts. One of the shafts has a positive clutch for application of the load.

Method:

Special gear wheels are run in the lubricant under test at a constant speed for a fixed time. The initial oil temperature is controlled but allowed to rise freely during each stage of the test. Loading is raised in stages. The test is continued until the damage load stage is reached, but if no damage occurs at load stage 12 the test is terminated.

Ratings:

The gears are inspected visually, without removal, at the end of each load stage. The failure load stage is determined by the summation of deep scoring, seizure lines or seizure areas on any of the gear teeth.

Results:

The load stage in which failure occurs is reported together with the test conditions; e.g. A/8.3/90, where A = gear type, 8.3 = pinion speed at pitch circle in m/sec, and 90 = initial temperature in oil sump in °C. These are the usual conditions, but they can be changed as required.

Specifications:

Results are reported in terms of the highest pass stage for the IP method or the first fail load stage, for the DIN Method.

04/02

Rig Tests

FZG Low Speed Test

Scope:

Method:

Results:

Note:

04/02

Based on a test originally developed by Chevron, this new procedure has been adopted by ASTM D 4998-89 for the evaluation of final drive lubricants for use in agriculture tractors and similar off-road applications.

Using the same test equipment and gear wheels as for the FZG load-carrying capacity test, this procedure requires a fixed load durability run to the following conditions. Lubricant Temp., °C

121

Load Stage

10

Motor Speed, r/min.

100 ± 3

Duration, Revolutions

120,000

The data is reported as total weight loss for both test gears, together with the total number of teeth exhibiting wear. The precision of the method has not been determined.

CEC test method development working group has abandoned the method until further research studies are completed. This is due to poor discrimination.

Rig Tests

FZG Micropitting Test

Scope:

Equipment:

Evaluates the ability of gear lubricants to resist micropitting.

A FZG gear rig is specially adapted to supply spray lubrication at a given rate and temperature to both the slave and spur gear boxes.

Method:

The two part procedure comprises a load stage test followed by an endurance test. During the load stage test, the ability of the gear lubricant tribological systems to resist micropitting is determined. The endurance test provides information on the progress of the damage after a higher number of load cycles.

Results:

The gears are examined for weight loss, area of micropitting involute profile deviation.

04/02

Rig Tests

IP High Torque Test IP232 Scope:

Method:

Specifications:

04/02

Assess the ability of a lubricant to prevent tooth surface distress in a hypoid automotive axle under conditions of high torque - low speed at an an oil temperature of 107°C (Procedure A) or 135°C (Procedure B).

A Standard Vanquard Phase I Hypoid rear axle is operated in a special test rig under conditions of high torque - low speed. The performance of the oil is evaluated by the examination of the axle components for tooth surface distress, corrosion and deposits.

CS3000B requirements (Procedure B) are that the gear teeth be free from evidence of scuffing, rippling, ridging, pitting or wear and that there is no corrosion or rusting of the half shafts or axle housing.

Rig Tests

MB Planetary Gear Rig

Scope:

Equipment:

Method:

To assess the relative EP/antiwear and anti-pitting properties of gear oils under low speed - high torque non steady state conditions.

The MB Planetary Gear rig is based upon a Mercedes-Benz screening rig using vehicle hub reduction units.

The test cycle below is repeated until a tooth breaks, excessive noise is heard, or the iron content of the oil sample, taken every second cycle, shows a significant increase. DURATION

SPEED

TORQUE

(sec)

(rpm)

(KNm)

154

420

-2.0

288

480

8.6

154

420

-2.0

88

420

9.4

154

420

-2.0 10.3

46

420

154

420

-2.0

24

420

11.1

58

420

-2.8

17

360

11.9

25

420

-3.7

4

360

12.8

6

420

-4.5

3

360

13.6

1

420

-5.4

5

300

14.4

154

420

-2.0

30

0

0

446

480

7.0

154

420

-2.0

414

480

7.8

Inlet oil temperature controlled at 100°C Rating Method:

04/02

The two sun gears and ten planetary gears are inspected for amount of pitting and wear on the teeth.

Rig Tests

Schmidt/Ethyl Tribo Tester Slideway Oil Test

Scope:

Method:

The method evaluates oil in respect of static friction and stick slip behaviour when used in machine slideway applications.

A slideway supporting a sliding block is lubricated with the test oil. The slideway is gradually inclined until the sliding block begins to move. The angle at which the block moves 20 µm is used to calculate the ‘Schmidt Coefficient of Friction’ which uses a calculation developed by the Hans Schmidt Tribology Laboratory for their original slideway test machine. The method uses two combinations of test materials: (a) Grey Cast Iron on Grey Cast Iron (b) SKC 3 plastic on Grey Cast Iron 300 run-in cycles are carried out with the SKC 3 plastic test and 400 with the Grey Cast Iron test. After completing the run-in, 10 test cycles are carried out to determine the ‘Schmidt Coefficient of Friction’ of the oil.

Results:

04/02

Graphical plots of all the run-in and test cycles are presented along with the calculated results of the 10 test cycles.

Rig Tests

Shear Stability Test - Kurt Orban CEC L-14-A-88 Scope:

Equipment:

Method:

04/02

To correlate shear stability with the permanent viscosity drop expected in field service.

Kurt Orban Injector rig.

A sample of oil is subjected to 30 or 250 cycles of a two cylinder diesel injection pump and injector nozzle set to a pressure of 175 bar.

Rig Tests

The Brugger Test

Scope:

Equipment:

The Brugger Test determines the load capacity of industrial, transmission and hydraulic lubricants. The test provides a useful technique for evaluating the wear protection of a lubricant under conditions of minimal lubrication.

A Müller Weingarten Brugger Test Machine is used.

Method:

A 25 mm diameter steel friction roller is rotated at 940 rpm (1.2 m/sec) against an 18 mm diameter fixed steel cylinder roller with a force of 400 N applied by a lever mechanism for 30 seconds. The surfaces are lubricated with a 5 ml sample poured over the assembly one minute before the start of the test

Results:

The result is reported in N/sqmm, calculated from the measurement of the wear scar.

Specifications:

Significance:

04/02

Typical pass criteria are: Hydraulic Oil

≥ 30 N/sqmm

Transmission Oil

≥ 50 N/sqmm

Grease

≥ 30 N/sqmm

The user should determine to his own satisfaction whether the results correlate with field performance or other bench test machines.

Rig Tests

Timken Extreme-Pressure Test ASTM D2782 Scope:

Covers the determination of load-carrying capacity of lubricating fluids by means of the Timken Extreme-Pressure Tester.

Equipment:

The test uses the Timken Wear and Lubricant Testing Machine, in which a pivoted test block is applied to the periphery of a rotating cylinder (cup) in such a way that the pressure of application can be controlled.

Method:

The machine is operated with the steel cup rotating at 800 r/min. Two determinations are made: the minimum load that will rupture the lubricant film and cause scoring or seizure; and the maximum load (OK load) that will not rupture the lubricant film. Testing is initiated at an applied load of 30 lbs and increased in increments of 10 lbs until scoring occurs. The load is then reduced by 5 lbs to determine the final score load and OK load values. Each load stage is run for a 10 minute duration and the lubricant temperature is brought to 38°C at the start of each stage.

Specifications:

04/02

The method is widely used for specification purposes and is used to differentiate between lubricants having low, medium or high extreme-pressure characteristics. The results may not correlate with results from service.

Rig Tests

Volkswagen Shear Stability Test PV1437 Taper Roller Bearing Rig Scope:

Method:

Determination of the mechanical shear stability of lubricants containing polymer additives such as gearbox, shock-absorber, automatic transmission and engine oils.

An adaptor, containing a standard single row taper roller bearing, is installed in a Four-Ball test machine. 40ml of test oil is introduced into a cup surrounding the bearing and the machine is run at 1500 r/min. with a 5 KN bearing axial load, for test durations of 4, 8 and 20 hours. The oil temperature is held at 60°C. The percentage loss in kinematic viscosity of the oil after each test run is plotted against time.

Significance:

Note:

The method is being standardised for specification purposes and is a rapid means of assessing the shear stability of a wide range of lubricants.

Limited service correlation of data from this test method is available. It is anticipated that this test will be introduced into Volkswagen lubricant specifications as they become due for revision.

04/02

Rig Tests

ZF Synchroniser Rig

Scope:

Equipment:

Method:

To evaluate the relative performance of gear lubricants in a synchromesh transmission system.

ZF Synchroniser Testing rig. The main component is a two-speed synchromesh gearbox.

50,000 cycles (100,000 changes). Each cycle consists of an up and down change. Input Speed

1700 rpm

Output Speed

1700 rpm and 2787 rpm

Oil Temperature

Results:

04/02

85 ± 5°C

After 50,000 cycles completed the coefficient of friction is calculated. The synchromesh cones are measured to calculate wear. They are also visually inspected for degradation.

Rig Tests

Gear Oil Corrosion Test L-33 Formerly FTMS 791B Method 5326.1 Scope:

Equipment:

Evaluates the rust and corrosion inhibiting properties of a gear lubricant when subjected to water contamination and elevated temperature.

The test utilises an unloaded Dana Model 30 hypoid differential unit mounted on a test stand which enables the unit to be motored over with heat lamps playing on the outer surface. Additionally, an environmentally controlled box is used to store the test unit at elevated temperature.

Method:

The unit is thoroughly cleaned, including shotblasting, internally and assembled with care. The unit is filled with 1200 ml of oil and 30 ml of water and motored for 4 hours at 82.2°C. On completion of this phase, the whole differential unit is stored for 162 hours at 51.7°C in the environmental box.

Rating:

Specifications:

04/02

At the end of storage, the unit is disassembled and rated for corrosion, sludge and other deposits.

Lubricant performance to API GL-5 and MIL-L-2105C requires no rusting on any working surface and up to 3.2 cm2 of rust on the cover plate as a maximum.

Rig Tests

Gear Oil Corrosion Test L-33 Formerly FTMS 791B Method 5326.1 Scope:

Equipment:

Evaluates the rust and corrosion inhibiting properties of a gear lubricant when subjected to water contamination and elevated temperature.

The test utilises an unloaded Dana Model 30 hypoid differential unit mounted on a test stand which enables the unit to be motored over with heat lamps playing on the outer surface. Additionally, an environmentally controlled box is used to store the test unit at elevated temperature.

Method:

The unit is thoroughly cleaned, including shotblasting, internally and assembled with care. The unit is filled with 1200 ml of oil and 30 ml of water and motored for 4 hours at 82.2°C. On completion of this phase, the whole differential unit is stored for 162 hours at 51.7°C in the environmental box.

Rating:

Specifications:

04/02

At the end of storage, the unit is disassembled and rated for corrosion, sludge and other deposits.

Lubricant performance to API GL-5 and MIL-L-2105C requires no rusting on any working surface and up to 3.2 cm2 of rust on the cover plate as a maximum.

Rig Tests

High Speed Axle Test L-42 Formerly FTMS 791B Method 6507.1 Scope:

Evaluates the anti-scoring characteristics of a gear lubricant under high-speed and shock loading conditions using a Spicer Model 44-1 hypoid axle.

Equipment:

The axle is driven by a 5.7 litre V8 gasoline engine which drives the test axle, a 4 speed truck transmission and two high inertia dynamometers at a rate to simulate hard acceleration to ca. 100 mph. The axle during testing is periodically shock loaded through a dynamometer.

Method:

After break-in, the axle is accelerated through the gears to a speed of 1050 r/min; then decelerated to 530 r/min. The cycle is repeated 5 times. This high speed sequence is followed by 10 shock loadings - the shock sequence.

Results:

Each new batch of gears is referenced against two industry standardised oils; RGO-110 (low-scoring) and RGO-108 (scoring). At least a 15% difference in the metal score characteristics is required.

Specifications:

Lubricant performance to API GL-5 and MIL-L-2105D requires scoring to be equal to or better than reference oil RGO-110. (Only the coast side of the gear is rated. The drive side score is only considered if there is a large amount of scoring).

The drive gear and pinion are rated for coast side scoring. The drive side score is only considered if scoring is significant.

04/02

Rig Tests

High Speed Shock Test CS3000B ANNEX D Scope:

Method:

Assess the ability of the oil to lubricate a hypoid automotive axle at high sliding speed, and with high impact loading, without surface distress to the gears.

An automotive hypoid rear axle is fitted into the test vehicle (Avenger) which is operated on a laboratory inertia roller rig. The severity level of the rig is adjusted so that the requirements of the axle are such that, using the CRC reference oil 10/90, the area of scuffing on the coast side of the pinion teeth is not less than 25%. The performance of the oil under test is evaluated by examination of the axle components for tooth distress, corrosion and deposits.

Specifications:

04/02

CS3000B requires the oil to have performance equal to or better than that of the reference oil.

Rig Tests

High Torque Axle Test L-37 Formerly FTMS 791B Method 6506.1 Scope:

Equipment:

Evaluates the load carrying, wear and extreme pressure characteristics of gear lubricants in a hypoid axle under high speed - low torque and low speed - high torque operation.

A Dana Model 60 hypoid axle (5.86 ratio) fitted with uncoated drive gear and pinion is set up to drive 2 dynamometers from an 8 cyclinder, 5.7 litre gasoline truck engine.

Method:

The axle is fitted with the test oil and driven under varying conditions. A high speed - low torque is first run for 100 minutes and the gears visually assessed via an inspection plug. A low speed - high torque sequence is then run for a further 24 hours.

Results:

A complete inspection of the gears is made and any deposits or discolouration of the bearings also noted.

Specifications:

04/02

Lubricant performance to API GL-5 and MIL-L-2105D is assessed on the basis of tooth surface rippling, ridging, pitting and wear, together with any deposits or discolouration.

Rig Tests

CRC L-60 Thermal Oxidation Stability Test L-60 FTM 2504 Gear TOST Scope:

Determines the deterioration of lubricants under severe oxidation conditions.

Method:

A measured sample of test oil is placed in a special gear case with two spur gears and a copper catalyst strip. The test is run for 50 hours, at 163ºC, whilst the gears are being driven at 1725 rpm and air is being bubbled through the sample.

Results:

Viscosity increase and pentane and toluene insolubles are determined.

Specifications:

04/02

The gears are rated for carbon, varnish and sludge deposits.

Rig Tests